CN101317636A - Method for reducing sulphur dioxide residual in sulphur conservation raw material of preserved fruit - Google Patents
Method for reducing sulphur dioxide residual in sulphur conservation raw material of preserved fruit Download PDFInfo
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- CN101317636A CN101317636A CNA2008100291552A CN200810029155A CN101317636A CN 101317636 A CN101317636 A CN 101317636A CN A2008100291552 A CNA2008100291552 A CN A2008100291552A CN 200810029155 A CN200810029155 A CN 200810029155A CN 101317636 A CN101317636 A CN 101317636A
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Abstract
The invention discloses a method for reducing the SO2 residue in preserved fruits sulphur-preserving raw material. The preserved fruits sulphur-preserving raw material is arranged in a sealable disposal device where ozone is pumped into for carrying out the desulfurization treatment. The invention takes the ozone treatment as the main mean and has the advantages of environmental protection, safety, effectiveness, etc. Furthermore, the method of the invention can be combined with ultrasonic treatment, and the like, thus having the effect of reducing the SO2 further; meanwhile, the method of the invention has the effect of killing the micro-organism in the raw material. Owning to the disposal, the SO2 residue of the raw material with the primary content of the SO2 less than 3,000mg/kg achieves the requirement of national standard, thus improving the quality and safety of the preserved fruits. The method of the invention has simple method, strong practicability, easy generalization and application, which has active effects on promoting the development of the preserved fruit food enterprises, reinforcing the market competitiveness, etc.
Description
Technical field
The invention belongs to food processing technology field, be specifically related to a kind of method that fruit jelly sulphur is hidden sulfur dioxide residue in the raw material that reduces.
Background technology
Food industry is the pillar industry that the national economy meta ranks first.In numerous food processing product, all kinds of traditional foods occupy a tiny space in food processing with they characteristics separately, play a part to intersperse people's dietetic life.As preserved fruit preserved fruit, fruit jelly etc., be pot foods and the characteristic typical local food that the consumer likes.Yet from product quality supervision check result and consumer's reflection in recent years, the quality safety of traditional food exists many problems, has become the hot issue that food quality safety is watched attentively, and wherein content of sulfur dioxide severe overweight problem is particularly outstanding.Fruit jelly processing is compared with other food processing, and bigger difference and special process are arranged.Longer between the preservation term of first fruit jelly raw material, process from raw material post processing to the product of gathering, usually to place 3~6 months or the longer time, for improving the keeping quality of preserving raw material, except that making salt embryo, fruit embryo through the stifling preservation of sulfur dioxide, salt down the way that the sulfite solution immersion is adopted in the preservation of soaking material more; It two is work in-processes, often needs to use sulphite as decolorizer.The covet aesthetic appearance of keeping quality and product of some producers often adds excessive sodium pyrosulfite in the production, caused the content of sulfur dioxide severe overweight of finished product, to the healthy formation harm of consumer, and becomes the underproof one of the main reasons of product.According to " the GB14884-2003 preserved fruit sanitary standard " requirement that replenishes revision, sulfur dioxide residual quantity can not surpass 0.35g/kg in the fruit jelly.Guangdong-style preserved fruits sulphur is hidden desulfurization of raw material and is handled the method that generally adopts the clear water rinsing at present, because the time that sulphur is hidden is longer, sulphite fully infiltrates in the fruits and vegetables tissue, combine closely with multiple organic matter in the fruits and vegetables, the fruit and vegetable materials that in addition has dense structure after calcification processing, only adopt the method for clear water rinsing, rinsing needs long period time, to production efficiency, fruits and vegetables tissue etc. has certain influence, and the effect of removing sulphite is limited, many products still do not reach standard-required, and sulfur dioxide residual quantity exceeds standard becomes the critical control link of Guangdong-style preserved fruits safety in production.
For improving desulfurization degree, enterprise that has and research department have carried out some researchs to the method that desulfurization is handled, the way of vacuum desulfurization has been proposed to adopt as the emerging enterprise in east, Beijing City Nutrient Source Inst food industry technique center, compare with simple infusion method, improved desulfurized effect to a certain extent and be significantly improved; Really embryo, olive, ginger etc. are experiment material to Foodstuffs Academy associate professor Huang Wei of Agricultural University Of South China with dried hawthorn embryo, plum through the sodium pyrosulfite processing, adopt distinct methods such as alkali lye, hydrogenperoxide steam generator immersion, ultrasonic wave processing, carry out desulfurization and handled research, the result shows and utilizes ultrasonic wave and dipping by lye or clear water to soak the method that combines, and can remove most of sulfur dioxide in the raw material within a short period of time.But not seeing has the ozone treatment utilized to remove the report that fruit jelly sulphur is hidden sulphite in the raw material.
Ozone (O
3) be oxygen (O
2) allotrope, form by three oxygen atoms, at normal temperature, under the normal pressure, can decompose and produce extremely strong antozone (O) and the hydroxyl (OH) of oxidability, can destroy bacterium rapidly, the internal structure of microorganisms such as virus, various pathogenic microorganisms there is extremely strong killing action, and have not can the residual harmful thing and cause the characteristics of secondary pollution, be considered to a kind of novel, desirable disinfectant, the ozone sterilization technology is as one of modern cold sterilization technology, demonstrated huge superiority, the security of using in food has obtained approval widely, but does not see have the ozone treatment utilized to remove the report that fruit jelly sulphur is hidden raw material sulphite content.
Summary of the invention
The objective of the invention is to overcome the deficiencies in the prior art, the method of content of sulfur dioxide in a kind of environmental protection, the safe and effective reduction fruit jelly raw material is provided, with ozone treatment is main means, select suitable treatment conditions according to the different material characteristic, can remove sulphite in the fruit jelly raw material to greatest extent, make the requirement that is up to state standards of product sulfur dioxide residual quantity.
Purpose of the present invention is achieved by the following technical programs:
A kind of method that reduces content of sulfur dioxide in the fruit jelly raw material is provided, may further comprise the steps:
(1) but raw material places the closed processes device;
(2) but in the closed processes device, feed ozone.
The present invention need dispose an ozone generator and prepare ozone, and the ozone generator specification of equipment is selected by the material quantity of every batch processing according to routine techniques.The ozone treatment mode is divided into gas-solid contact processing, the solution-air contact is handled gentle-liquid contact+ultrasonic wave and handled, and required auxiliary facility is different.
As one of processing scheme, adopt gas-solid contact processing mode, step (1) but described closed processes device between handling; The stainless steel diffuser is installed between described processing, and the described ozone of step (2) prepares by ozone generator; Described ozone generator bubbling air quantity delivered 1L/min, ozone generator power 100%; The described ozone feeding time is 30min~60min.Step (2) also comprises raw material water spray humidification step.
Specifically comprise following implementation step:
A. require to have between a processing that ozone output reaches and the raw material treating capacity is complementary with ozone generator, require good airproof performance between processing;
The diffuser that number row stainless steel tube is made is installed between b. handling;
C. place between handling and handle the shelf that material quantity adapts, on can place the bamboo sieve, raw material then is tiled on the bamboo sieve; Also can adopt the multiple field raw material charging carriage of belt wheel;
D. after material is put, close gateway between processing, open ozone generator, ozone is entered between processing through diffuser contact with raw material; After disposing, close ozone generator, material still continues to place to shift out behind the 24h again and carries out subsequent technique between processing and handle;
E. for improving desulfurized effect, the humidification of will spraying water before raw material is handled makes material weightening finish 20~30%, in the ozone treatment process, continues humidification with sprayer.
As two of processing scheme, adopt solution-air contact processing mode, step (1) but described closed processes device is a fermentation vat, adorn water in the pond in.Described fermentation vat bottom is equipped with the stainless steel diffuser; Diffuser top is equipped with stainless (steel) wire, and raw material places on the stainless (steel) wire.Described material quantity water yield weight ratio is 1: 20~25.
Specifically comprise following implementation step:
A. require to have a fermentation vat that adapts with every batch of raw material treating capacity, 15~20cm is equipped with stainless (steel) wire apart from the fermentation vat bottom;
B. the diffuser that number row stainless steel tube is made is installed in fermentation vat bottom, the end sealing of diffuser, the other end is connected with ozone generator, promptly the ozone by the ozone generator generation enters diffuser by tube connector, and with become Ozone Water after water contacts;
C. material is put into fermentation vat, is placed on the stainless (steel) wire, and inventory is about 1: 20 with the ratio of amount of water~and 25;
D. open ozone generator, ozone is entered in the water through diffuser contact with raw material; After disposing, close ozone generator, after material still continues to place 4~6h in former water, change water again and carry out the subsequent technique processing.
As three of processing scheme, adopt the processing of solution-air contact+ultrasonic wave, step (1) but described closed processes device is a groove type ultrasonic ripple treating apparatus, in tank, install stainless (steel) wire and diffuser additional.Step also comprises the ultrasonic wave treatment step after (2).Described raw material and water weight ratio are 1: 20~25; The described feeding ozone time is 30~60min; Described ultrasonic treatment time is 30~60min.
Specifically comprise following implementation step:
A. requiring has a groove type ultrasonic ripple treating apparatus that adapts with every batch of raw material treating capacity, installs stainless (steel) wire and diffuser in tank additional, requires identical with scheme two.
B. material is put on the stainless (steel) wire of ultrasonic wave processing treatment trough, inventory is about 1: 20 with the ratio of amount of water~and 25, open the logical ozone 30~60min of ozone generator, close ozone generator, after handling 30~60min with ultrasonic wave again, after material still continues to place 4~6h in former water, change water again and carry out the subsequent technique processing.
The invention has the beneficial effects as follows:
(1) the present invention utilizes the ozone safe, that noresidue also can be killed microorganism in the raw material simultaneously that sulphur Tibetan fruit jelly raw material is carried out the desulfurization processing, develop a kind of process that can effectively reduce sulfur dioxide residual quantity in the raw material of fruit jelly sulphur Tibetan, the sulfur dioxide residual quantity that has solved the traditional fruit or vegetable type food sustainable development of the long-term puzzlement problem that exceeds standard, thereby obviously improve the production safety technology and the product quality of this series products, promote the technology of traditional garden stuff processing food to innovate again, and have positive social benefit.
(2) the inventive method operation is simple relatively, and practicality is stronger, applies easily.
The specific embodiment
Further describe the present invention below in conjunction with specific embodiment.
Embodiment 1 gas-solid contact method (ozone exposure method) is handled the haw berry embryo
A. require to have between a processing that ozone output reaches and the raw material treating capacity is complementary with ozone generator, require good airproof performance between processing;
The diffuser that number row stainless steel tube is made is installed between b. handling;
C. place between handling and handle the shelf that material quantity adapts, on can place the bamboo sieve, raw material then is tiled on the bamboo sieve; Also can adopt the multiple field raw material charging carriage of belt wheel;
The multiple field raw material charging carriage of the sealing requirements between above-mentioned processing, the installation of diffuser, shelf, bamboo sieve and belt wheel all belongs to the simple technique of this area routine, does not have special requirement.
D. after material is put, close gateway between processing, open ozone generator, ozone is entered between processing through diffuser contact with raw material; After disposing, close ozone generator, material still continues to place to shift out behind the 24h again and carries out subsequent technique between processing and handle;
E. for improving desulfurized effect, the humidification of will spraying water before raw material is handled makes material weightening finish 20~30%, in the ozone treatment process, continues humidification with sprayer.
Hawthorn dry fruit embryo (content of sulfur dioxide is below the 3000mg/kg) can be placed between processing with the atomizing humidifier humidification during concrete operations, feed ozone 30min~60min, air quantity delivered 1L/min, ozone generator power 100%, can remove the sulfur dioxide of 60 above % behind the placement 24h, (soak time is 4~6h in conjunction with follow-up immersion treatment again, change water therebetween 2~3 times), can make the content of sulfur dioxide in the raw material be reduced to the national standard scope, and the hawthorn of simple immersion treatment, soak the 350mg/kg of the above sulfur dioxide residual quantity of 12h far above national Specification, and haw pulp soft texture.
Embodiment 2 liquid-solid contact methods are handled the haw berry embryo
A. require to have a fermentation vat that adapts with every batch of raw material treating capacity, 15~20cm is equipped with stainless (steel) wire apart from the fermentation vat bottom;
B. the diffuser that number row stainless steel tube is made is installed in fermentation vat bottom, the end sealing of diffuser, the other end is connected with ozone generator, promptly the ozone by the ozone generator generation enters diffuser by tube connector, and with become Ozone Water after water contacts;
C. material is put into fermentation vat, is placed on the stainless (steel) wire, and inventory is about 1: 20 with the ratio of amount of water~and 25;
D. open ozone generator, ozone is entered in the water through diffuser contact with raw material; After disposing, close ozone generator, after material still continues to place 4~6h in former water, change water again and carry out the subsequent technique processing.
The installation of above-mentioned fermentation vat, stainless (steel) wire, diffuser etc. all belongs to the simple technique of this area routine, does not have special requirement.
During concrete operations hawthorn dry fruit embryo (content of sulfur dioxide is below 3000mg/kg) is placed treating apparatus, add entry at 1: 25 by solid-to-liquid ratio, feed ozone (air quantity delivered 1L/min, ozone generator power 100%) 30min~60min after soaking 1h, after placing 4~6h, content of sulfur dioxide in the raw material can reduce more than 70%, after this change water again 2~3 times, soak 2~4h, the content of sulfur dioxide in the raw material can be reduced to the national standard scope.
Embodiment 3 ozone+ultrasonic wave is handled
A. requiring has a groove type ultrasonic ripple treating apparatus that adapts with every batch of raw material treating capacity, installs stainless (steel) wire and diffuser in tank additional, requires identical with (2).
B. material is put on the stainless (steel) wire of ultrasonic wave processing treatment trough, inventory is about 1: 20 with the ratio of amount of water~and 25, open the logical ozone 30~60min of ozone generator, close ozone generator, after handling 30~60min with ultrasonic wave again, after material still continues to place 4~6h in former water, change water again and carry out the subsequent technique processing.Ultrasonic wave is handled according to the existing routine techniques in this area.
During concrete operations the hawthorn of embodiment 2 after ozone treatment continued to handle 30~60min with ultrasonic wave, content of sulfur dioxide in the raw material can reduce more than 86%, the requirement that is up to state standards illustrates that ozone+ultrasonic wave handles and have the cooperative effect of good removal sulphite.
Claims (10)
1, a kind of method that reduces sulfur dioxide residue in the raw material of fruit jelly sulphur Tibetan is characterized in that may further comprise the steps:
(1) but fruit jelly sulphur hidden raw material place the closed processes device;
(2) but in the closed processes device, feed ozone.
2, hide the method for sulfur dioxide residue in the raw material according to the described reduction fruit jelly of claim 1 sulphur, it is characterized in that step (1) but described closed processes device between handling; The stainless steel diffuser is installed between described processing.
3, hide the method for sulfur dioxide residue in the raw material according to the described reduction fruit jelly of claim 2 sulphur, it is characterized in that the described ozone of step (2) is that ozone generator prepares; Described ozone generator bubbling air quantity delivered 1L/min, ozone generator power 100%; The described ozone feeding time is 30min~60min.
4, hide the method for sulfur dioxide residue in the raw material according to the described reduction fruit jelly of claim 2 sulphur, it is characterized in that also comprising raw material water spray humidification step before and after the step (2).
5, hide the method for sulfur dioxide residue in the raw material according to the described reduction fruit jelly of claim 1 sulphur, it is characterized in that step (1) but described closed processes device is a fermentation vat, adorn water in the pond in.
6, hide the method for sulfur dioxide residue in the raw material according to the described reduction fruit jelly of claim 5 sulphur, it is characterized in that described fermentation vat bottom is equipped with the stainless steel diffuser; Diffuser top is equipped with stainless (steel) wire, and raw material places on the stainless (steel) wire.
7, hide the method for sulfur dioxide residue in the raw material according to the described reduction fruit jelly of claim 5 sulphur, it is characterized in that described material quantity and water yield weight ratio are 1: 20~25.
8, hide the method for sulfur dioxide residue in the raw material according to the described reduction fruit jelly of claim 1 sulphur, it is characterized in that the described treating apparatus of step (1) is a groove type ultrasonic ripple treating apparatus, in tank, install stainless (steel) wire and diffuser additional.
9, according to the method for sulfur dioxide residue in claim 1 or the 8 described reduction fruit jelly sulphur Tibetan raw materials, it is characterized in that also comprising the ultrasonic wave treatment step after the step (2).
10, hide the method for sulfur dioxide residue in the raw material according to the described reduction fruit jelly of claim 9 sulphur, it is characterized in that described raw material and water weight ratio are 1: 20~25; The described feeding ozone time is 30~60min; Described ultrasonic treatment time is 30~60min.
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102144761A (en) * | 2011-03-04 | 2011-08-10 | 华南农业大学 | Method for removing sulfur dioxide from semifinished fruit |
ES2364478A1 (en) * | 2010-02-12 | 2011-09-05 | Unique Size España, S.L | Procedure for packaging and conservation of cut fruits and vegetables and products obtained according to such procedure (Machine-translation by Google Translate, not legally binding) |
CN102524609A (en) * | 2012-01-18 | 2012-07-04 | 王利兵 | Food safety ecological instrument |
WO2012168494A1 (en) | 2011-06-06 | 2012-12-13 | Palacios Gazules, Sergio | Method for packaging and preserving cut citrus fruits and products obtained by means of said method |
CN103565860A (en) * | 2013-11-12 | 2014-02-12 | 药都制药集团股份有限公司 | Method for removing sulfur dioxide residues on surface of traditional Chinese medicinal material |
CN108740704A (en) * | 2018-06-22 | 2018-11-06 | 仲恺农业工程学院 | New method for reducing sulfur dioxide residue by biological method and application of new method in Cantonese preserved fruit |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1327777C (en) * | 2005-09-05 | 2007-07-25 | 陕西师范大学 | Technique for conserving fresh winter date |
CN101104538A (en) * | 2007-04-23 | 2008-01-16 | 郑海平 | Sulfur dioxide degradation device and application thereof |
CN101147611B (en) * | 2007-10-15 | 2012-07-04 | 广州南联实业有限公司 | Method for processing clearing type pineapple juice |
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2008
- 2008-07-01 CN CN2008100291552A patent/CN101317636B/en not_active Expired - Fee Related
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2364478A1 (en) * | 2010-02-12 | 2011-09-05 | Unique Size España, S.L | Procedure for packaging and conservation of cut fruits and vegetables and products obtained according to such procedure (Machine-translation by Google Translate, not legally binding) |
CN102144761A (en) * | 2011-03-04 | 2011-08-10 | 华南农业大学 | Method for removing sulfur dioxide from semifinished fruit |
WO2012168494A1 (en) | 2011-06-06 | 2012-12-13 | Palacios Gazules, Sergio | Method for packaging and preserving cut citrus fruits and products obtained by means of said method |
CN102524609A (en) * | 2012-01-18 | 2012-07-04 | 王利兵 | Food safety ecological instrument |
CN103565860A (en) * | 2013-11-12 | 2014-02-12 | 药都制药集团股份有限公司 | Method for removing sulfur dioxide residues on surface of traditional Chinese medicinal material |
CN108740704A (en) * | 2018-06-22 | 2018-11-06 | 仲恺农业工程学院 | New method for reducing sulfur dioxide residue by biological method and application of new method in Cantonese preserved fruit |
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