CN101311495A - X-ray tool for an oilfield fluid - Google Patents

X-ray tool for an oilfield fluid Download PDF

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Publication number
CN101311495A
CN101311495A CNA2008100985351A CN200810098535A CN101311495A CN 101311495 A CN101311495 A CN 101311495A CN A2008100985351 A CNA2008100985351 A CN A2008100985351A CN 200810098535 A CN200810098535 A CN 200810098535A CN 101311495 A CN101311495 A CN 101311495A
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ray
fluid
instrument
target
fluid line
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CNA2008100985351A
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CN101311495B (en
Inventor
罗德·沙姆派因
乔尔·L·格罗夫斯
安东尼·德科斯基
艾蒂恩·瓦利
彼得·赖特
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Schlumberger Canada Ltd
Prad Research and Development Ltd
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Prad Research and Development Ltd
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Priority claimed from US11/751,727 external-priority patent/US20080069307A1/en
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Abstract

The invention provides an x-ray tool for an oilfield fluid. The tool may include a generator portion housing a collimator about a target from which x-rays are emitted. In this manner x-rays may be attenuated right at the target such that a majority of shielding otherwise necessary for safety concerns may be eliminated. Rather, by employing the target within the collimator, shielding of the generator may be limited to a single shielding plate within the generator portion that is positioned parallel to the target at the opposite end of an x-ray tube therebetween. As a result of this configuration, an x-ray tool for analysis of oilfield fluids may be provided with a minimum weight of shielding material. Thus, hand-held user friendly embodiments may be safely employed at the oilfield.

Description

The X ray instrument that is used for oilfield fluid
Technical field
The present invention relates to analyze the aid of oilfield fluid.Especially, the present invention relates to compactness and X ray instrument very flexibly.
Background technology
Be usually directed to adopt the various application of oilfield fluid from the field produces hydro carbons.For example, for extract hydro carbons from the oil field, a large amount of main equipments may be transported to the oil field.These application may relate to by the well that pierces the stratum in the oil field adds oilfield fluid to obtain hydro carbons.Then, can hydro carbons be extracted out from well with the oilfield fluid that is added in some cases.
The DRILLING APPLICATION that is used for forming at first well relates to add a kind of application of oil well fluid, wherein drilling mud in drilling process circular flow to and flow out drill bit.The another kind of oilfield fluid is used and can be comprised that the completion application is to give well construction integrality and navigability.This completion is used the cementing that can be included in the well bore casing district in the well, wherein pumps into cement in the well and is squeezed in the well bore casing district and all the other expose between boreholes wall.
Except that mud and cement, also other fluid can be introduced in the well.For example can under high pressure fracturing fluid be introduced in the well, to form the crack of passing the borehole wall and entering the stratum in the production wellblock.Also can from well, reclaim the fracturing fluid of certain percentage subsequently.Similarly, dosage and other application may relate to Xiang Jingzhong interpolation oilfield fluid.
The characteristic of aforesaid oilfield fluid is most important for the effect of the application that utilizes oilfield fluid.Thereby the way of monitoring oilfield fluid character is very general closely in the use.For example, under the situation that pressure break is used, the density the when fracturing fluid of monitoring injection well injects usually.The information of the support dosage that provides in well in the relevant processing procedure can be provided of the fracturing fluid density.Consider that the type of proppant and the formation of measuring for above-mentioned crack are generally key factor, these information may be very important.In fact, in many cases, the owner of well is according to the expense of the support dosage payment fracturing operation that pumps into the down-hole.Thereby the accuracy of described measuring density may be very important.Particularly it is practical with regard to typical pressure break is used the fact that may relate to about 0.5 million pounds~about 2,000,000 pounds of proppants.Thereby, industrially require of the fracturing fluid measuring density to be accurate in 1% usually.
Density when pumping in the well for the precise monitoring fracturing fluid is used various radioactive density meters usually in the oil field.Radioactive density meter connects along the pipeline that leads to from fracturing pump device or house steward the well.Densometer comprises the radioactive source that is positioned at a place on the described pipeline, and for example radiocesium (is generally Cs 137).The opposite side that detector is positioned at described pipeline is used to detect the gamma ray that caesium sends.Outside the exception pipeline material itself, of the fracturing fluid density will determine the testing result that detector is final in the pipeline.Thereby, the effect of drain wire material, the information that the indication of the fracturing fluid density that in-line flows relatively will be provided of the amount of the gamma ray that radioactive source sends and the detected amount of detector.The radioactive density meter of Ying Yonging is accurate to usually and is better than in about 1% by this way.
Disadvantageously, above-mentioned radioactive density meter relates to the on-the-spot dangerous radioactive substance that uses.Densometer must manually be placed and use with manual mode, thereby makes the user stand to be exposed to the great risk of hazard class radiation.In order to eliminate the potential risk of using radioactive substance at operating position, densometer is set to mainly the part of the main equipment made by shielding material usually.Thereby, sacrificed the flexibility of radiation density counter device basically.In addition, also there is the possibility of shield partial failure, even only the inefficacy of minimum degree also can be to the your healthy danger greatly that constitutes in scene.
For solving the harm of using radioactive source, as described in the series application No.11/532236 that is called " Apparatusand Method for Well Services Fluid Evaluation Using X-Rays " that submitted on September 15th, 2006, can adopt the photon generator of X-ray density meter form.By this way, be similar to above-mentioned radioactive density meter, X ray seen through be used for the pipeline that detector detects.Under the situation of X-ray density meter, the intensity of the X ray of being launched still is enough to see through fully pipeline, but this intensity is starkly lower than the gamma ray that radioactive density meter is launched.In addition, when not using, the X-ray density meter can simply cut out, thereby can not stay the huge hidden danger of harmfulness emission.
The above-mentioned advantage of X-ray density meter is very remarkable, particularly considers and has eliminated on-the-spot harmfulness radioactive source fully.Yet can to launch a large amount of densities of infection lower but still have the X ray of potential danger for the X-ray density meter in operating process.Thereby, still need enough shieldings, with near being perfectly safe of user guaranteeing.Thereby the X-ray density meter is still quite inflexible device of 150~250 pounds of weighing.Thereby the assembled on site of this device, location and dismounting are still great challenge for the user.
Summary of the invention
Be provided for measuring the X ray instrument of oilfield fluid character.This X ray instrument can comprise to being connected target on the X-ray tube provides the generator of electron beam, and target is used to receive electron beam and the corresponding X ray that sends.Collimater can be arranged on the collimation that is used for X ray on every side of target.
Description of drawings
Fig. 1 is the sectional view that is connected the oil field X ray execution of instrument scheme on the oilfield fluid pipeline.
Fig. 2 is the part enlarged drawing along the oil field shown in Figure 1 X ray instrument of section line 2-2 intercepting.
Fig. 3 is the general view of the oilfield operations of employing oil field shown in Figure 1 X ray instrument.
Fig. 4 is the part enlarged drawing of the alternate embodiment of oil field X ray instrument.
Fig. 5 is the part enlarged drawing of another embodiment of oil field X ray instrument.
The specific embodiment
With reference to certain X ray instrument that in the oil field, is used for the pressure break application embodiment is described.Yet other field use also can be utilized the described X ray execution of instrument of the application scheme.For example, cementing and DRILLING APPLICATION can be used the described X ray execution of instrument of the application scheme.Which kind of situation no matter, the included X ray instrument of the described embodiment of the application need be not more than about 25lb or following shield is used safely for the user.In fact, following oil field X ray instrument can have less than the gross weight of about 50lb and have configuration flexibly, is used in user friendly ground, oil field hand-held and placement.
Refer now to Fig. 1, show the oil field X ray execution of instrument scheme 100 that is connected on the oilfield fluid pipeline 150.Oilfield fluid pipeline 150 is set, in the well 310 in oil field 301 shown in Figure 3, to carry oilfield fluid 160.Especially, embodiment shown in discloses the oilfield fluid 160 of the fracturing fluid form that is used for the pressure break application.Provide support the high pressure pressure break of agent 165 by fluid 160 with auxiliary stratum.Yet, in other embodiments, can use the oilfield fluid and the application of other type, comprise the drilling mud and other suitable fluid and the application that are used for cemented cement paste or are used for drilling well.
The oil field X ray instrument 100 of Fig. 1 is set, to help to determine the information of oilfield fluid 160 character in the relevant pipeline 150.This information can relate to density, solid content, and solid phase, liquid and gas character or physical state character, material are formed or other character.In addition, even integrated unnecessary X ray shield, instrument 100 still can be gross weight less than about 50lb and preferably less than the equipment of the hand-held of about 30lb, manual positioning, easy operating.
In conjunction with reference to figure 2, show oil field X ray instrument 100 with generator part 125, this generator part 125 is connected on the detector portion 175 by anchor clamps or the big envelope 110 around the oilfield fluid pipeline 150.The size of ruling big envelope 110 is so that the testing agency 177 of detector portion 175 is aimed in the outlet 135 of generator part 125.In one embodiment, testing agency 177 has the scitillating material that joins with the interface with photocathode and electron multiplier, detects to realize indication.Further describe as the application, the X ray 250 that generator part 125 is sent can pass fluid line 150, is impaired to a certain degree by oilfield fluid 160, and detected then mechanism 177 is detected.By this way, but the identification oilfield fluid to the weakening of X ray 250 so that relevant information of being passed through oilfield fluid 160 character to be provided.In one embodiment, the low-intensity scattered x-ray that can collimate and to pass oilfield fluid 160 once in a while indirectly testing agency 177 to avoid detecting.This X ray may be harmless, but does not have informedness substantially, or even potential obstacle effective and accurately definite oilfield fluid characteristic.
Shown in fluid line 150 can be wall thickness and be nominally 15000lb or above steel pipe for about 0.5 inch.Thereby X ray instrument 100 can have the high energy that produces X ray 250 between about 450kV at about 100kV and dispose, with fluid line 150 shown in passing effectively.Yet this still is starkly lower than the intensity of above-mentioned radioactive source, the shield 145 that still can be provided with to a certain degree as described below.
Still in conjunction with Fig. 2 with reference to figure 1, generator part 125 is set, guiding electron beam 200 into target 101, thereby produce the X ray 250 that passes fluid line 150 as mentioned above.In the illustrated embodiment, generator part 125 can comprise conventional filament 137 feeding electric current by conventional methods, thereby discharges electronics.Filament 137 can be connected on the X-ray tube that nickel or other suitable material make or be arranged in the described X-ray tube, so that electronics is with the form directive target 101 of electron beam 200.Target 101 can be made and be had enough thickness and keep off electron beam 200 to cut by gold, copper or other suitable material.Yet, in this process, the x-ray photon of target 101 emission X ray forms (for example 250).
X-ray tube 130 can be arranged in the dielectric material space 140, and this dielectric material space 140 is full of sulfur hexafluoride, transformer oil or other suitable inertia and does not preferably have the medium of gas.In addition, in the illustrated embodiment, X-ray tube 130 is an end ground connection relative with filament 137.Yet, in other embodiments, X-ray tube 130 can be near filament 137 ground connection.In addition, the X-ray tube of generator part 125 130 and other internal work unit are installed in the rigid casing 127, shown in this rigid casing 127 directly is connected on the big envelope 110.In the illustrated embodiment, an end of X-ray tube 130 is supported by the pillar 139 that is connected on the shield 145, and shield 145 is fixed on the sidewall of rigid casing 127 in turn.Consider the high energy of X ray instrument 100, shield 145 can be made by having certain thickness lead, gold, tungsten or other suitable material.
As mentioned above, shield 145 is separated by by pillar 139 and filament 137 and X-ray tube 130.In one embodiment, spacing distance can be about 2~5 inches.In the end of the X-ray tube 130 that has filament 137 as shown in the figure is under high voltage and the unearthed situation, may need described interval.Yet, by making the X-ray tube 130 end ground connection relative, can directly be close to and closely place collimaters 131, and collimater 131 has limited size around X-ray tube 130 with filament 137, the following collimator effect that further describes is provided simultaneously.
X-ray tube 130 ends relative with filament 137 are connected on the collimater 131, and collimater 131 is fixed on the gripper shoe 133 in turn.Collimater 131 can be made and as described below usually by with shield 145 identical materials or even make with target 101 identical materials by lead, gold, copper, tungsten or other suitable shielding material.In addition, gripper shoe is fixed on the sidewall of rigid casing 127, thereby fixedly positioning the internal work unit of generator part 125.As mentioned above, outlet 135 can be arranged on rigid casing 127 and the side plate 133.As shown in Figure 2, outlet 135 can be the weakened region of described supporting structure 127,133, and multi x-ray 250 passes to allow more.
Reference detector 134 can be connected near the above-mentioned outlet 135, to detect outgoing X ray 250 before passing through fluid line 150, is used for comparing at the detected X ray of fluid line 150 opposite sides with testing agency 177.In one embodiment, reference detector 134 has the above-mentioned testing agency 177 essentially identical structures with detector portion 175.In addition, reference detector 134 can link to each other by lead with the processing mechanism that their data are analyzed with testing agency 177.In addition, testing agency 177 itself can be contained in the outer rigid housing 179 that directly is connected on the above-mentioned big envelope 110.Also outer rigid housing 179 can be set, with to detector 175 part provide the structural supports, outer rigid housing 179 also holds and shields from generator part 125 and penetrates thereon remaining X ray simultaneously.
Now continue with reference to figure 1 and Fig. 2, describe the structure of generator part 125 in detail.Particularly, the embodiment of generator part 125 is described, wherein make X ray instrument 100 be used safely in manually to place effectively and use desired shield gross weight obviously to reduce (for example being reduced to the weight of shield 145).In fact, as mentioned above, based on the structure shown in Fig. 1 and Fig. 2, the weight of entire tool 100 can be not more than about 30lb.
In the embodiment of Fig. 1 and Fig. 2, collimater 131 is arranged on around the target 101.Promptly target 101 is not clipped between X-ray tube 130 and the adjacent collimator 131, but with target 101 actual being arranged in the collimater 131.By this way, the X ray 250,251,275,276 that target 101 is produced directly collimates, so that the actual amount of leaving collimater 131 zones is substantially limited in the particular range that the shunt X ray 250,251 that is limited as angle α and α ' arrives target 101 either sides.Form those X ray that drop on outside angle α and the α ' scope by X ray 275,276.Describedly also avoid it to leave collimater 131 zones substantially by X ray 275,276 direct conductively-closeds.Except that above-mentioned X ray 250,251,275,276, a small amount of low-intensity X ray (not shown) can near scattering generator part 125 inside.Yet rigid casing 127 can be made by conventional stainless steel, thereby has got rid of the possibility that this low-intensity X ray leaves generator part 125 and the user constituted harm basically.Should be noted in the discussion above that this sleeve pipe with prior art is opposite, promptly X-ray tube, target and collimater structure arranged in a straight line requires whole sleeve pipe to be made by shielding material in the prior art.
Because above-mentioned collimater 131 and target 101 structures, X ray instrument 100 is used safely in manually to use the amount of desired shield obviously to reduce.In fact, suppose to fail to leave collimater 131 zones, with regard to shielding, only pay close attention to X ray 250,251 along separate routes by the X ray 275,276 that ends outside angle α and α ' that target 101 penetrates.Yet angle is that the shunt X ray 250 of α is intended to leave generator part 125 and advance to detector portion 175 as mentioned above, weakens naturally thereby follow inbound path.Thereby the X ray shielding potential safety hazard of only depositing is that relative angle is the shunt X ray 251 of α ' those X ray (for example towards filament 137) back to above-mentioned electron beam 200 sources.
Angle is that the shunt X ray 251 of α ' can fully be shielded by the shield 145 that is parallel to target 101, so that shunt X ray 251 is still between target 101 and shield 145.Thereby, the minimum dimension of shield can with angle [alpha] ' and target 101 and shield 145 between distance directly related.For example, in the illustrated embodiment, shield 145 is separated by with target 101 by X-ray tube 130, filament 137 and pillar 139.Thereby the size of these parts can determine that cut-off angles is the size of the required shield 145 of all X ray 251 of α '.Yet,, can obviously reduce the weight and/or the size of X ray instrument 100 by shield 145 shown in whole shield is restricted to.
With reference to said structure, in one embodiment, the weight of shield 145 can be less than about 25lb, and the weight of whole X ray instrument 100 is not more than about 50lb.As a comparison, otherwise the shield of whole X ray instrument 100 can make tool and 100 surpass about 150lb.Perhaps, said structure makes X ray instrument 100 can have the flexibility, hand-holdable of improvement, thereby than large-scale X-ray equipment easy operating more, described large-scale X-ray equipment does not adopt the target 101 that places in the collimater 131, thereby for the obvious shield of purpose of safety needs, even may be greater than the shield of 100lb greater than 50lb.
Continuation is with reference to figure 2, and simultaneously with reference to figure 1, view 2-2 shows the amplifier section of X ray instrument 100.In this view, the end of X-ray tube 130 is in the collimater 131 of contiguous target 101.Collimater 131 is used to carry out described collimation around the end of X-ray tube 130 and target 101.In fact, suppose that collimater 131 and target 101 can be made by identical materials, in one embodiment, in fact collimater 131 and target 101 have single or overall structure.
Illustrate electron beam 200 to leave the end of X-ray tube 130 shown in Figure 2 and clashed into target 101, made a large amount of X ray 250,251,275,276 from target, penetrate.X ray 250,251,275,276 can weaken by collimated device 131, if it is interior then cast out from collimater 131 perhaps to drop on above-mentioned proper angle α, α '.Can angle [alpha], α ' be set according to the size and target 101 location therein of collimater 131.For example, in one embodiment, target 101 places near collimater 131 mid points, angle [alpha], α ' is equated substantially and very narrow, according to the length of collimater 131 between about 1 °~about 10 °.Yet, in other embodiments, can adopt other angle [alpha], α ' scope, so that X ray 250,251 penetrates along separate routes from collimater 131.
Leave collimater 131 directive fluid lines 150 shunt X ray 250 can by shown in the outlet that reduces of structural thickness 135 penetrate.Yet identical X ray 250 also can reach reference detector 134, and to read the X ray 250 that passes through before the fluid line 150, the X ray testing result that is used for obtaining with testing agency 177 after X ray passes fluid line 150 is compared.In one embodiment, the real-time feedback mechanism of processor can utilize the reading of reference detector 134 to adjust the X ray output of instrument 100.In another embodiment, processor can be compared the reading of analyzing reference detector 134 and testing agency 177.In addition, the out of Memory about the data of known chemical material and relative fluid 160 that may type can be stored in the processor.By this way, can set up the benchmark of X ray information, to determine the X ray attenuation degree in the fluid line 150.Thereby, can obtain the more accurate density or the out of Memory of relevant oilfield fluid 160.
In alternate embodiment, as shown in Figure 4, strainer 409 can be placed on before the reference detector 134,434 decay that takes place with in analog stream fluid line 150 self material.For example, detected X ray 250 passes 1 inch thick fluid line 150 pipe wall material before detected mechanism 177 is detected, strainer 409 can by about 1 inch thick and make with fluid line 150 material identical materials.By this way, the reference line (see figure 4) that can obtain raising as described below by reference detector 134,434.Which kind of situation no matter, detector shield 136 is connected in reference detector 134 and the testing agency 177 so that residual arbitrarily X ray 250 decay.
Refer now to Fig. 3, show the fracturing device 300 in oil field 301.Fracturing device 300 is used in may surpass under the pressure of about 15000PSI fracturing fluid 360 is imported in the well 310.By this way, fracturing fluid 360 producing region 375 that can permeate the ground, thus form pressure break district 370.Thereby can impel in producing region 375 and obtain hydro carbons.In order to arrive well 310, fracturing fluid 360 can be imported fluid lines 330 and arrive the well head 340 at well 310 tops.One group of high pressure three cylinder pump or other pump, pipe summation miscellaneous equipment (not shown) can be arranged on before the fluid line 330, as mentioned above to order about fracturing fluid 360 by fluid line 330.
The density of fracturing fluid 360 and other character may be conclusive to fracturing operation.Thereby, above-mentioned oilfield fluid X ray instrument 100 embodiments can be fixed on the fluid line 330 character when line operate of going forward side by side adds well 310 with check and monitoring fracturing fluid 360.As shown in Figure 3, the composition of fracturing fluid 360 can comprise liquid and proppant 365, and liquid and proppant 365 mix the fracturing fluid character to obtain to be scheduled in mixing tank 325.Proppant 365 can comprise sand, ceramic materials, bauxite, glass microballoon or salt and other suitable material.Which kind of situation no matter, the suitable mixture of described composition is very important to fracturing operation.Thereby, can utilize X ray instrument 100, for example by the density of monitoring fracturing fluid 360 when in fluid line 330, flowing through instrument 100, monitor the amount of the proppant 365 of supplying with well 310.
In the illustrated embodiment, other composition combination of proppant 365 and fracturing fluid 360 in the oil field.Yet, in other embodiments, can provide the fracturing fluid 360 that has wherein contained proppant 365 to the oil field.In addition, can before in well 310, carrying, carry out the premix of fracturing fluid 360.Which kind of situation no matter is suitably mixed and/or is carried in well 310 under the situation of total amount proper supporting agent 365 at fracturing fluid 360 compositions, uses the X ray instrument 100 may be very important for guaranteeing that fracturing operation carries out according to design in this way.In addition, as shown in Figure 3, because target 101 and collimater 131 have as above with reference to figure 1 and the described orientation of Fig. 2, so X ray instrument 100 is enough compact, with the hand-held of safety and manually placement.
Refer now to Fig. 4, show the internal structure of the alternate embodiment of oil field X ray instrument 400.As mentioned above, instrument 400 comprises the strainer 409 that is placed on before the reference detector 434, is used for the decay that takes place of the sidewall of fluid line 150,330 as shown in figures 1 and 3 of analog stream fluid line example.By this way, can detect the Data Base directrix by the X ray that reference detector 434 obtains to improve.Thereby, can determine character more accurately by the oilfield fluid of fluid line.The i.e. reading explanation that can obtain by reference detector substantially with irrelevant X ray 450 decay of oilfield fluid.Thereby, when when comparing analysis from the information of reference detector 434, can determine the character of fluid in the fluid line more accurately from the information of the testing agency of fluid line opposite side.
Continuation is with reference to figure 4, and the class of operation of X ray instrument 400 is similar to the X ray instrument of above-mentioned Fig. 1 and Fig. 2.Be that target 401 places in the collimater 431 with reception and by the electron beam 402 from X-ray tube 430.Electron beam 402 bump targets 401 cause and produce X ray 450,451,475,476, collimate by 431 pairs of described X ray of collimater.For falling into the interior X ray of angle α ' 451, describe in detail at Fig. 1 as above, a certain amount of shield can be provided in the opposite end of X-ray tube 430.Yet, make X ray instrument 400 be used for safely manually using desired shielding amount minimum.Thereby X ray instrument 400 can be set to the hand-held easy operating type of gross weight less than about 50lb.
As the embodiment of Fig. 1 and Fig. 2, the collimater 431 of network for location 4 and target 401 are so that a large amount of X ray 475,476 collimated device 431 before leaving this zone weakens.Other X ray 451 conductively-closeds along separate routes of penetrating back as mentioned above along the direction of electron beam 402.Yet, can will be transported to independently reference detector 403 and fluid line 407 passages from the shunt X ray 450 that X ray instrument 400 penetrates by collimation current divider 405.The suitable collimation current divider 405 of shape that the collimation material is made can be arranged in the collimater 431 and export between the gripper shoe 433 at 435 places at target 401 and instrument 400.As shown in the figure, passage 403,407 shown in the placement of collimation current divider 405 can provide.Fluid line passage 407 can lead to fluid line, as being used to estimate the character of oilfield fluid wherein as described in the above-mentioned embodiment.In addition, the reference detector passage can pass above-mentioned strainer 409 and leads to reference detector 434.Reference detector shield 436 can be fixed on the reference detector with guarantee instrument 400 in operating process near user's safety.
Refer now to Fig. 5, show the internal structure of another alternate embodiment of oil field X ray instrument 500.In this embodiment, target 501 is arranged in the collimater 531 equally with reception with by the electron beam 502 from X-ray tube 530.Electron beam 502 bump targets 501 cause and produce X ray 550,551,575,576, collimate by 531 pairs of described X ray of collimater.Describe in detail with reference to figure 2 and Fig. 4 as above, a certain amount of shielding can be provided in the opposite end of X-ray tube 530, weaken so that drop on the interior X ray of angle α ' 551.Yet,, make the X ray instrument be used safely in manually to use desired shielding amount minimum, thereby the gross weight of not considering shield entire tool 500 can be less than 501b because target places in the collimater 531.
In the embodiment of Fig. 5, X ray 550,575 penetrates from target along the direction away from X-ray tube 530 along separate routes.Can collimate current divider 504,506 shuntings or guide a certain amount of shunt X ray by multichannel.Promptly collimating the suitable collimation current divider 504,506 of shape that material makes can be arranged in the collimater 531 between target 501 and gripper shoe 533.As shown in Figure 5, be similar to above-mentioned embodiment, the passage 503,505,507 that the placement of collimation current divider 504,506 can provide X ray 550 to pass fluid line.By this way, the multichannel that can carry out X ray 550 at the opposite side of fluid line detects.Utilize the obtainable relevant multichannel data collection (multiple data set) that passes through the oilfield fluid of fluid line, can carry out various analyses.For example, desirable multichannel detects the average of gained information, to guarantee to provide the property information in fluid representative cross section.Perhaps, multichannel detects and can compare mutually, with phase composition (phase fraction) information (for example liquid-solid composition information) that relevant fluid is provided.
In another alternate embodiment, adopt for example X ray instrument 500 of Fig. 5, can pass the diverse location of fluid line or pass the different fluid pipeline and carry out detecting corresponding to the difference of different passages 503,505,507.For example, can proppant is added be used for fracturing fluid that pressure break uses before and afterwards, pass fluid line and detect.Can pass perhaps in the DRILLING APPLICATION process that slurry conveyed fluid line carries out a kind of detection in well, can be passed in another fluid line of in the same DRILLING APPLICATION mud being derived and carry out another detection from well.
No matter adopt which kind of specific embodiments, described those embodiments of the application provide effective method, obtain information such as relevant oilfield fluid character, density in inactive mode by this method.Thereby, obviously reduced harm to the user.In addition, described X ray instrument can adopt the structure that obviously alleviates its overall weight by exempting conventional X ray instrument manually to use desired most of X ray shield.Therefore, the X ray instrument that can provide flexibility to improve.This instrument can be the portable equipment that weight is not more than about 50lb, and can manually be placed on the well operations position, and can not make the user stand to be exposed to any great risk of X ray.
Carried out above stated specification with reference to present embodiment preferred.It will be appreciated by those skilled in the art that under the situation of design that does not break away from these embodiments and scope and can improve and change said structure and method of operating.For example, main reference is described embodiment with the oilfield fluid that the fracturing fluid form adds in the well among the application.Yet, can utilize the described embodiment of the application to monitor other oilfield fluid, comprise hydro carbons that the oilfield fluid that extracts for example produced, circulating drilling mud etc. from same well.In addition, should not think above stated specification only limit to describe and the concrete structure of signal in the accompanying drawings, and should think and meet and supports to comprise its most comprehensive and claim optimized scope.

Claims (28)

1. X ray instrument that is used to measure oilfield fluid character, this X ray instrument has the generator part, and described generator partly comprises:
Shell;
Be arranged on the X-ray tube that described shell is interior, be used to guide electron beam;
With described X-ray tube end direct neighbor, the target that is used to receive described electron beam and sends X ray; And
Be arranged on around the described target, be used to collimate the collimater of described X ray.
2. the X ray instrument of claim 1, wherein said end is a first end, described generator part also comprises the shield that is contained in the described shell, the position of this shield contiguous described X-ray tube with described first end opposite second end.
3. the X ray instrument of claim 2, the weight of wherein said shield is less than about 25lb.
4. the X ray instrument of claim 2, wherein said first end ground connection, described collimater is directly extended around described first end, and about 2 inches~about 5 inches of described the second ends of described position distance.
5. the X ray instrument of claim 2, wherein said shield is the shield that material is selected from lead, gold and tungsten.
6. the X ray instrument of claim 1, wherein the part X ray penetrates from described collimater and passes a plurality of X ray and be used for the multichannel X ray along separate routes and detect.
7. the X ray instrument of claim 6, wherein said multichannel X ray detect a plurality of oilfield fluid pipelines that pass contiguous described generator part to carry out.
8. the X ray instrument of claim 6, wherein said multichannel X ray detect the fluid line that passes contiguous described generator part to carry out, to provide about one of the character of oilfield fluid in the described fluid line and average data of phase composition characteristic.
9. the X ray instrument of claim 1, wherein said character are that density, solid content, physical state and material one of are formed.
10. the X ray instrument of claim 1, wherein said X-ray tube is placed in the dielectric material space of described shell, and this dielectric material space comprises one of sulfur hexafluoride and transformer oil.
11. the X ray instrument of claim 1, wherein said collimater are the collimaters that material is selected from lead, gold, copper and tungsten.
12. the X ray instrument of claim 1, wherein said collimater and described target have the integral type overall structure.
L3. the X ray instrument of claim 1, wherein the part X ray penetrates from the end of described collimater with about 1 °~about 10 ° angular range.
14. the X ray instrument of claim 1, wherein said target are the targets that material is selected from Jin Hetong.
15. the X ray instrument of claim l, wherein said X-ray tube is made by nickel.
16. an X ray tool assembly that is used to measure oilfield fluid character, this assembly comprises:
The generator part, this generator partly comprises: shell, be arranged on the X-ray tube that described shell is interior, be used to guide electron beam, with described X-ray tube end direct neighbor, the target that is used to receive described electron beam and sends X ray, and around described target, be used for the collimater of the X ray of leader through the fluid line of oilfield fluid;
Detector portion, it is used to detect the X ray through fluid line of described part; And
Be connected the big envelope on described generator part and the described detector portion, this big envelope be used for described generator partly and described detector portion be fixed on described fluid line around.
17. the X ray tool assembly of claim 16, wherein said end are first end, described generator part also comprises the shield that is contained in the described shell, the position of this shield contiguous described X-ray tube with described first end opposite second end.
18. the X ray tool assembly of claim 17, its gross weight is less than about 50lb.
19. the X ray tool assembly of claim 16, wherein said fluid line are to be nominally the fluid line of 15000lb at least, described electron beam produces under about 100kV~about 450kV.
20. the X ray tool assembly of claim 16, wherein said generator part also comprises the reference detector of separating with described fluid line, to detect the part of the X ray that described target sends.
21. the X ray tool assembly of claim 20 also comprises placing between described target and the described reference detector to simulate the strainer of described fluid line sidewall.
22. the X ray tool assembly of claim 16, wherein said detector portion collimates.
23. the X ray tool assembly of claim 16, wherein said oilfield fluid are one of fracturing fluid, cement paste and drilling mud.
24. a method of measuring oilfield fluid character, this method comprises:
Have therein on the fluid line of oilfield fluid x ray generator is set;
Utilize the collimater that is positioned in the generator around the target that the X ray that target sends is collimated; And
Utilization is positioned at the testing agency of fluid line and described generator relative position, the X ray of test section.
25. the method for claim 24 also comprises the oilfield fluid data according to pre-stored, analyzes the data of described testing agency.
26. the method for claim 24, wherein said part are first, this method also comprises to be utilized and reference detector that described fluid line separates detects second portion in the X ray that described target sends.
27. the method for claim 26 also comprises the data according to described reference detector, analyzes the data of described testing agency.
28. the method for claim 26 comprises that also the data of utilizing described reference detector adjust the intensity of the X ray that described target sends.
CN 200810098535 2007-05-22 2008-05-22 X-ray tool for an oilfield fluid Expired - Fee Related CN101311495B (en)

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US5689540A (en) * 1996-10-11 1997-11-18 Schlumberger Technology Corporation X-ray water fraction meter
FR2764064B1 (en) * 1997-05-30 1999-07-16 Schlumberger Services Petrol FLOW SECTION FOR MEASUREMENTS CONCERNING OIL WELL EFFLUENTS AND MEASUREMENT SYSTEM INCLUDING SUCH SECTION
FR2764065B1 (en) * 1997-05-30 1999-07-16 Schlumberger Services Petrol PROCESS AND DEVICE FOR THE CHARACTERIZATION OF OIL WELL EFFLUENTS
US6130931A (en) * 1998-09-17 2000-10-10 Process Control, Inc. X-ray fluorescence elemental analyzer
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