CN1012822B - Extraction of near-cocoa oil from seed of chinese tallowtree - Google Patents
Extraction of near-cocoa oil from seed of chinese tallowtreeInfo
- Publication number
- CN1012822B CN1012822B CN 87105207 CN87105207A CN1012822B CN 1012822 B CN1012822 B CN 1012822B CN 87105207 CN87105207 CN 87105207 CN 87105207 A CN87105207 A CN 87105207A CN 1012822 B CN1012822 B CN 1012822B
- Authority
- CN
- China
- Prior art keywords
- leaching
- seed
- tallow tree
- chinese tallow
- hour
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Landscapes
- Fats And Perfumes (AREA)
Abstract
The present invention relates to a method for preparing cacao-like butter, which takes Chinese tallow tree seeds as a raw material and belongs to the field of chemical industrial techniques. The method makes use of the specific construction of the Chinese tallow tree seed particles and adopts a solvent leaching method to directly prepare the cacao-like butter. The method has the advantages of short process route and low product cost and assures the high quality requirements of the products.
Description
The present invention be relevant a kind of be the method that raw material is produced cocoa butter equivalent with the Chinese tallow tree seed, its goods can be used as edible special oil, are to produce chocolate raw material.
Chinese tallow tree is the distinctive woody oleiferous plants plant of China, and the fruit-Chinese tallow tree seed of its knot is a kind of seed that had not only contained Chinese tallow tree fat but also contained Chinese catalpa oil.The structure of seed is divided into mesocarp part and seed shell, seed benevolence part.Mesocarp accounts for about 32%, and its major ingredient is a Chinese tallow tree fat, and this is a kind of edibility grease.The contained grease major ingredient of seed benevolence part is a Chinese catalpa oil, and this is a kind of to the deleterious semi-drying oil of human body.
In China, the ripe ， And of technology that utilizes Chinese tallow tree fat to produce cocoa butter equivalent enters industrial production.Introduced a kind of method of utilizing Chinese tallow tree fat to produce cocoa butter equivalent among China patent application prospectus CN85100006, it is to add organic solvent in oleum sapii, heating is all dissolved oleum sapii, through once or the secondary crystallisation by cooling, filter to divide and carry, the LMP fraction leach-s/tive through remove solvent ， And through depickling, decolouring, deodorization handle cocoa butter equivalent.This method is raw material with the oleum sapii, promptly earlier the Chinese tallow tree seed is produced oleum sapii, produces cocoa butter equivalent with oleum sapii again, and its operational path is longer.And and as adopt outsourcing raw material Chinese tallow tree fat because the quality of Chinese tallow tree fat is difficult to guarantee that this will influence the quality of its product cocoa butter equivalent.
The object of the present invention is to provide a kind of is the method that raw material is produced cocoa butter equivalent with the Chinese tallow tree seed directly, to guarantee the quality of product.Another object of the present invention is to simplify processing method, improve yield, reduce production costs.Other purpose of the present invention will embody in detailed narration.
Main points of the present invention are, the Chinese tallow tree seed is packed in the leaching equipment, add organic solvent, the add-on of organic solvent is 1～2 times of raw material weight, the control leaching temperature is 5～25 ℃, leaches 0.5～4 hour, and filtering separation is fallen solid matters such as seed slag, remove organic solvent, through dephosphorization fat, depickling, the deodorization of routine handle cocoa butter equivalent.
Chinese tallow tree seed of the present invention is not for containing the Chinese tallow tree seed of foreign material through screening.In order to improve yield, shorten leaching time, also can adopt mechanical barking method such as peeling machine or other method earlier the Chinese tallow tree seed to be carried out peeling, the mesocarp that will contain Chinese tallow tree fat is then packed into and is leached in the leaching equipment.
The organic solvent that the present invention adopts must be the solvent that allows use in the food service industry, therefore can adopt sherwood oil or acetone or soybean solvent oil (industrial naptha).
Leaching temperature in the processing parameter of the present invention and leaching time are according to factor such as the quality that adopts raw material and definite.Cross low and leaching time when too short when leaching temperature, the fusing point of goods and yield will reduce a lot; When the too high and leaching time of leaching temperature is long, the fusing point of goods will raise, and quality product is with defective.According to experiment, when directly adopting the leaching of Chinese tallow tree seed, its optimum soaking extracting temperature is 10-15 ℃, and leaching time is 1-2 hour; When utilizing the mechanical barking method to adopt the mesocarp leaching, its leaching temperature is generally 5-20 ℃, and leaching time is 0.5-2 hour; Optimum soaking extracting temperature is 5-12 ℃, and leaching time is 1-1.5 hour.
Filtration procedure of the present invention is the simple filtration process of a routine, and its effect is to separate solid matters such as removing the seed slag.Solid matters such as the seed slag that removes by filter contain materials such as high-melting-point Chinese tallow tree fat, can utilize it to be processed into other products.
Of the present inventionly remove the method that the organic solvent process generally can adopt heating evaporation, the recyclable recycling of organic solvent.
Dephosphorization fat of the present invention, depickling, deodorising process adopt method commonly used in the oils industry.Dephosphorization fat adopts the aquation method, and the alkali refining method is adopted in depickling, and deodorization is adopted and feed steam distilled method under high temperature, condition of high vacuum degree.
When adopting the darker raw material of some color and luster, also need increase decolouring and handling, can adopt the atlapulgite of technology maturation to wait and decolour.
The present invention is a raw material with the Chinese tallow tree seed, utilize and be separated with the method that one deck is difficult for the structure of the hard seed shell that soaked into by organic solvent or adopts mechanical barking between Chinese tallow tree seed mesocarp and the seed benevolence, leach the technology of certain hour at a certain temperature with organic solvent, one step directly proposed the LMP part-cocoa butter equivalent of the contained Chinese tallow tree oil of mesocarp, its production technique is fairly simple, greatly reduce production cost, guaranteed the quality of product, reached the present invention's purpose.
Detailed process of the present invention can be described in detail by following embodiment.
Embodiment 1
Taking by weighing Chinese tallow tree seed 1000 grams, put into a container, add 1200 milliliters of soybean solvent oils, is under 20 ℃ in temperature, leaches 1.5 hours, removes by filter solid matters such as seed slag, and heating evaporation removes the soybean solvent oil and gets raw product in the immigration vaporizer; Raw product is put into beaker, fed steam 0.5 hour, standing separation is fallen phosphatide; Goods behind the dephosphorization fat are heated to 40 ℃, and Kuai speed Jiao Ban And adds 10% caustic soda soln (add-on can be determined according to greasy acid value), after caustic soda soln adds, stirs at a slow speed 20 minutes again, is warming up to 60 ℃, and the insulation standing separation is fallen soap stock, and is extremely neutral with hot water wash; Grease after the depickling is put into glass reactor, a reactor and a vacuum pump join, make it produce the vacuum tightness of 750 mmhg, feed steam to reactor after being heated to 80 ℃, adopt the sand-bath method to continue to be heated to 200-220 ℃, kept 4-6 hour, and naturally cooled to below 80 ℃, take out goods and be cocoa butter equivalent.
Embodiment 2
Method is with embodiment 1, and its leaching temperature is 15 ℃, and leaching time is 1.5 hours.
Embodiment 3
Method is with embodiment 1, and its leaching temperature is 10 ℃, and leaching time is 1.5 hours.
Embodiment 4
Method is with embodiment 1, and its leaching temperature is 10 ℃, and leaching time is 1 hour.
Embodiment 5
Method is with embodiment 1, and its leaching temperature is 5 ℃, and leaching time is 1 hour.
Embodiment 6
Utilizing peeling machine that the Chinese tallow tree seed is carried out peeling And separates mesocarp with seed benevolence, take by weighing mesocarp 1000 grams, putting into a container, add 1500 milliliters of soybean solvent oils, is under 10 ℃ in temperature, leached 1 hour, remove by filter solid matters such as slag crust, move in the vaporizer heating evaporation and remove the soybean solvent oil and get raw product, through dephosphorization fat, depickling, deodorization handle cocoa butter equivalent (dephosphorization fat, depickling, technological process of deodorization are with embodiment 1).
Embodiment 7
Method is with embodiment 6, and its leaching temperature is 15 ℃, and leaching time is 0.5 hour.
The experimental result data of each embodiment such as following table:
Leaching temperature leaching time recovery rate goods fusing point
Embodiment
(℃) (hour) (%) (℃)
1 20 1.5 8.7 36
2 15 1.5 8.6 35
3 10 1.5 8.1 34
4 10 1 7.0 31
5 5 1 4.9 30
6 10 1 28.9 34
7 15 0.5 31.5 36
The cocoa butter equivalent goods that the present invention makes are very close with external like product physico-chemical property, concrete parameter such as following table:
Claims (5)
1, be the method that raw material is produced cocoa butter equivalent with the Chinese tallow tree seed, feature of the present invention is, the Chinese tallow tree seed is packed in the leaching equipment, add organic solvent, the add-on of organic solvent is 1-2 a times of raw material weight, and the control leaching temperature is 5-25 ℃, leached 0.5-4 hour, filtering separation is fallen solid matters such as seed slag, removes organic solvent, through dephosphorization fat, depickling, deodorization handle cocoa butter equivalent.
2, in accordance with the method for claim 1, it is characterized in that the organic solvent that adopts is sherwood oil or acetone or soybean solvent oil (industrial naptha).
3, according to claim 1 or 2 described methods, it is characterized in that leaching temperature is 10-15 ℃, leaching time is 1-2 hour.
4, according to claim 1 or 2 described methods, it is characterized in that adopting mechanical barking method such as peeling machine earlier the Chinese tallow tree seed to be carried out peeling, then mesocarp being packed into, to leach ， And control leaching temperature in the leaching equipment be 5-20 ℃, and leaching time is 0.5-2 hour.
5, in accordance with the method for claim 4, it is characterized in that leaching temperature is 5-12 ℃, leaching time is 1-1.5 hour.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 87105207 CN1012822B (en) | 1987-07-28 | 1987-07-28 | Extraction of near-cocoa oil from seed of chinese tallowtree |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 87105207 CN1012822B (en) | 1987-07-28 | 1987-07-28 | Extraction of near-cocoa oil from seed of chinese tallowtree |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1030935A CN1030935A (en) | 1989-02-08 |
| CN1012822B true CN1012822B (en) | 1991-06-12 |
Family
ID=4815239
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 87105207 Expired CN1012822B (en) | 1987-07-28 | 1987-07-28 | Extraction of near-cocoa oil from seed of chinese tallowtree |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1012822B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100437321C (en) * | 2004-07-27 | 2008-11-26 | 能源变换设备有限公司 | Binary beam steering device |
-
1987
- 1987-07-28 CN CN 87105207 patent/CN1012822B/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100437321C (en) * | 2004-07-27 | 2008-11-26 | 能源变换设备有限公司 | Binary beam steering device |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1030935A (en) | 1989-02-08 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CA1155113A (en) | Process for recovery of polyol fatty acid polyesters | |
| EP2449071B1 (en) | Process for manufacturing palm oil fractions containing virtually no 3-monochloropropanediol fatty acid esters | |
| IE59171B1 (en) | A refined fish oil product and the production process for same | |
| Leibovitz et al. | Our experiences in processing maize (corn) germ oil | |
| WO2019027315A2 (en) | Process for producing a refined palm fruit oil having a reduced 3-mcpd content | |
| CN110396453A (en) | A kind of production technology of linseed oil | |
| CN1057115C (en) | Abstracting and processing method of "Huangshu" sunflower seed oil | |
| CN1012822B (en) | Extraction of near-cocoa oil from seed of chinese tallowtree | |
| WO1994009098A1 (en) | Triglyceride fractionation | |
| Jawad et al. | Quality characteristics of physically refined soyabean oil: effects of pre‐treatment and processing time and temperature | |
| EP0170242B1 (en) | In-line dewaxing of edible vegetable oils | |
| US5210242A (en) | Process for soap splitting using a high temperature treatment | |
| Trisakti et al. | Comparison of mass balance and oil quality in plant refinery I and IV | |
| Chayen et al. | The application of impulse rendering to the animal‐fat industry | |
| US3345389A (en) | Separation of fatty materials | |
| CN1272335C (en) | Method of producing powder phosphatide using of peanut, soyabeun, repeseed phosphatide from milky | |
| CN86104413A (en) | With the Chinese tallow tree seed is the method that raw material is produced cocoa butter equivalent | |
| US4160774A (en) | Process of degumming fatty glycerides using sodium acetate and acetic acid buffer | |
| JPS63174940A (en) | Separation of lignin and phenol from pnenol solution | |
| Ahmad et al. | The effect of processing operations on the total sulphur content in rapeseed oil | |
| CN1140754A (en) | Method for extracting fat from gromwell seeds | |
| CN107629867A (en) | The improvement aqua method of seed oil is extracted from oilseeds | |
| CN115557989A (en) | Method for extracting phospholipid containing high unsaturated fatty acids EPA and DHA in squid oil | |
| SU137506A1 (en) | The method of obtaining phytol | |
| Sharma et al. | Processing of prepressed solvent extracted oil from indian soybean‐refining loss studies |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C13 | Decision | ||
| GR02 | Examined patent application | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CI01 | Correction of invention patent gazette |
Correction item: Business affairs Correct: delete False: Termination of patent right Number: 23 Page: 113 Volume: 9 |
|
| ERR | Gazette correction |
Free format text: CORRECT: AFFAIRS; FROM: CESSATION OF PATENT RIGHT TO: DELETION |
|
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |