CN101260042A - Method for preparing cinnamyl acetate - Google Patents
Method for preparing cinnamyl acetate Download PDFInfo
- Publication number
- CN101260042A CN101260042A CNA2008100473584A CN200810047358A CN101260042A CN 101260042 A CN101260042 A CN 101260042A CN A2008100473584 A CNA2008100473584 A CN A2008100473584A CN 200810047358 A CN200810047358 A CN 200810047358A CN 101260042 A CN101260042 A CN 101260042A
- Authority
- CN
- China
- Prior art keywords
- cinnamyl acetate
- styryl carbinol
- cinnamyl
- temperature
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- SDOFMBGMRVAJNF-KVTDHHQDSA-N (2r,3r,4r,5r)-6-aminohexane-1,2,3,4,5-pentol Chemical compound NC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO SDOFMBGMRVAJNF-KVTDHHQDSA-N 0.000 title claims abstract description 37
- WJSDHUCWMSHDCR-VMPITWQZSA-N cinnamyl acetate Natural products CC(=O)OC\C=C\C1=CC=CC=C1 WJSDHUCWMSHDCR-VMPITWQZSA-N 0.000 title claims abstract description 37
- 238000000034 method Methods 0.000 title abstract description 8
- 238000006243 chemical reaction Methods 0.000 claims abstract description 12
- 238000002360 preparation method Methods 0.000 claims abstract description 8
- 238000005406 washing Methods 0.000 claims abstract description 7
- OOCCDEMITAIZTP-QPJJXVBHSA-N (E)-cinnamyl alcohol Chemical compound OC\C=C\C1=CC=CC=C1 OOCCDEMITAIZTP-QPJJXVBHSA-N 0.000 claims description 27
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 14
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 claims description 10
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 7
- 238000009413 insulation Methods 0.000 claims description 7
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 8
- 239000003054 catalyst Substances 0.000 abstract description 2
- 150000001298 alcohols Chemical class 0.000 abstract 3
- 150000004075 acetic anhydrides Chemical class 0.000 abstract 2
- 238000003912 environmental pollution Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 238000006386 neutralization reaction Methods 0.000 abstract 1
- 238000004321 preservation Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- 239000000047 product Substances 0.000 description 14
- 239000012043 crude product Substances 0.000 description 6
- 239000002994 raw material Substances 0.000 description 3
- IWTYTFSSTWXZFU-UHFFFAOYSA-N 3-chloroprop-1-enylbenzene Chemical compound ClCC=CC1=CC=CC=C1 IWTYTFSSTWXZFU-UHFFFAOYSA-N 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 2
- OOCCDEMITAIZTP-UHFFFAOYSA-N allylic benzylic alcohol Natural products OCC=CC1=CC=CC=C1 OOCCDEMITAIZTP-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 235000007173 Abies balsamea Nutrition 0.000 description 1
- 244000099147 Ananas comosus Species 0.000 description 1
- 235000007119 Ananas comosus Nutrition 0.000 description 1
- 239000004857 Balsam Substances 0.000 description 1
- 241000167854 Bourreria succulenta Species 0.000 description 1
- 244000037364 Cinnamomum aromaticum Species 0.000 description 1
- 235000014489 Cinnamomum aromaticum Nutrition 0.000 description 1
- 244000068485 Convallaria majalis Species 0.000 description 1
- 235000009046 Convallaria majalis Nutrition 0.000 description 1
- 244000018716 Impatiens biflora Species 0.000 description 1
- 235000010254 Jasminum officinale Nutrition 0.000 description 1
- 240000005385 Jasminum sambac Species 0.000 description 1
- 240000007472 Leucaena leucocephala Species 0.000 description 1
- 235000010643 Leucaena leucocephala Nutrition 0.000 description 1
- 235000011430 Malus pumila Nutrition 0.000 description 1
- 244000070406 Malus silvestris Species 0.000 description 1
- 235000015103 Malus silvestris Nutrition 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 229920006330 Styrox Polymers 0.000 description 1
- 244000223014 Syzygium aromaticum Species 0.000 description 1
- 235000016639 Syzygium aromaticum Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 235000019693 cherries Nutrition 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 235000020995 raw meat Nutrition 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200810047358A CN100595185C (en) | 2008-04-17 | 2008-04-17 | Method for preparing cinnamyl acetate |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200810047358A CN100595185C (en) | 2008-04-17 | 2008-04-17 | Method for preparing cinnamyl acetate |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101260042A true CN101260042A (en) | 2008-09-10 |
CN100595185C CN100595185C (en) | 2010-03-24 |
Family
ID=39960778
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN200810047358A Expired - Fee Related CN100595185C (en) | 2008-04-17 | 2008-04-17 | Method for preparing cinnamyl acetate |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN100595185C (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101591243B (en) * | 2009-05-11 | 2012-06-20 | 江苏省原子医学研究所 | Method for preparing acetic acid phenolic ester by catalyzing bisphosphonates |
CN105104922A (en) * | 2015-07-23 | 2015-12-02 | 江西省添美食品有限公司 | Additive used for quick-frozen pastries |
-
2008
- 2008-04-17 CN CN200810047358A patent/CN100595185C/en not_active Expired - Fee Related
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101591243B (en) * | 2009-05-11 | 2012-06-20 | 江苏省原子医学研究所 | Method for preparing acetic acid phenolic ester by catalyzing bisphosphonates |
CN105104922A (en) * | 2015-07-23 | 2015-12-02 | 江西省添美食品有限公司 | Additive used for quick-frozen pastries |
CN105104922B (en) * | 2015-07-23 | 2018-09-07 | 帅兵 | A kind of additive for quick-frozen pastry |
Also Published As
Publication number | Publication date |
---|---|
CN100595185C (en) | 2010-03-24 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: HUBEI YUANCHENG PHARMACEUTICAL CO., LTD. Free format text: FORMER OWNER: WUHAN HEZHONG BIO-CHEMICAL MANUFATURE CO., LTD. Effective date: 20111107 |
|
C41 | Transfer of patent application or patent right or utility model | ||
COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 430064 WUHAN, HUBEI PROVINCE TO: 432100 XIAOGAN, HUBEI PROVINCE |
|
TR01 | Transfer of patent right |
Effective date of registration: 20111107 Address after: 432100, Hubei province Xiaogan City Industrial Park Road Patentee after: Hubei Yuancheng Pharmaceutical Co., Ltd. Address before: 430064, No. 201, 1000 street, Wuchang District, Hubei, Wuhan (No. 496, Zhongshan Road) Patentee before: Wuhan Hezhong Bio-chemical Manufature Co., Ltd. |
|
C56 | Change in the name or address of the patentee |
Owner name: HUBEI YUANCHENG SAICHUANG TECHNOLOGY CO., LTD. Free format text: FORMER NAME: HUBEI YUANCHENG PHARMACEUTICAL CO., LTD. |
|
CP01 | Change in the name or title of a patent holder | ||
CP01 | Change in the name or title of a patent holder |
Address after: 432100, Hubei province Xiaogan City Industrial Park Road Patentee after: HUBEI YUANCHENG PHARMACEUTICAL CO., LTD. Address before: 432100, Hubei province Xiaogan City Industrial Park Road Patentee before: Hubei Yuancheng Pharmaceutical Co., Ltd. |
|
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20100324 Termination date: 20160417 |
|
CF01 | Termination of patent right due to non-payment of annual fee |