CN101220234A - Anticorrosion paint and method for producing the same - Google Patents
Anticorrosion paint and method for producing the same Download PDFInfo
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- CN101220234A CN101220234A CNA2008100568349A CN200810056834A CN101220234A CN 101220234 A CN101220234 A CN 101220234A CN A2008100568349 A CNA2008100568349 A CN A2008100568349A CN 200810056834 A CN200810056834 A CN 200810056834A CN 101220234 A CN101220234 A CN 101220234A
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Abstract
The invention relates to a coating and a preparation method, in particular to an anti-corrosion coating and the preparation method thereof. The invention belongs to the technical field of coating. The anti-corrosion coating of the invention consists of component A and component B; wherein, the components of A by weight percentage are as follows: epoxy modified acrylic resin accounting for 40 to 60 percent, dissolvent accounting for 2 to 6 percent, nomalbutylacetat accounting for 6 to 10 percent, rutile type titanium dioxide accounting for 35 to 40 percent, functional accessory ingredient accounting for 0.4 to 0.8 percent; the component B contains modified urethane resin; the weight ratio of component A to component B is (2 to 6): 1. The coating has the advantages of good acid resistant, alkali resistant and salt corrosion resistant properties, strong adhesive force, good flexibility, strong penetrability, high weather resistance, innoxious property, high drying speed, convenient construction and being capable of coating rubiginous base steel layer.
Description
(1) technical field
The present invention relates to a kind of coating and preparation method thereof, especially a kind of protective system and preparation method thereof.The technical field that belongs to coating.
(2) background technology
Protective system is a very fast industry of development in recent years, but, though a lot of protective systems can reach certain preservative activity, but under the wearing and tearing of irradiation of sunlight or external force, be difficult to reach lastingly the rot-resistant purpose, in addition, because coating industry, the problem of environmental protection also is an important factors.
(3) summary of the invention
[problem that will solve]
Purpose of the present invention provides a kind of protective system and preparation method thereof.
[technical scheme]
The inventor has optimized the component and the ratio thereof of protective system through for many years development, has adjusted the preparation method simultaneously, successfully manufactures experimently out acid-and base-resisting, brine corrosion performance, strong adhesion, and snappiness is good, and perviousness is strong, good weatherability, and nontoxic, fast drying.
Through secular test, the contriver has obtained the component and the ratio thereof of protective system of the present invention, and is specific as follows:
A kind of protective system of the present invention, it is made up of A, B two portions, wherein:
Composition and the weight ratio of A comprise:
Epoxy modified acrylic resin 40-60
Solvent 2-6
N-butyl acetate 6-10
Rutile titanium white powder 35-40
Functional aid 0.4-0.8;
The composition of B is as follows:
Modified polyurethane resin;
The part by weight of A component and B component is (2-6): 1.
Above-mentioned protective system, wherein, the preferred composition and the weight ratio of described A component comprise:
Epoxy modified acrylic resin 50
Solvent 4
N-butyl acetate 8
Rutile titanium white powder 37.4
Functional aid 0.6.
Preferred 4: 1 of the part by weight of above-mentioned A component and B component.
Also include following component and weight part ratio thereof in the above-mentioned A component: chlorinated polyether resin 3-8, acrylic resin 3-8, inorganic silicic acid resin 3-8, nano titanium oxide 1-5, nano-aluminium oxide 2-5, nano zircite 1-4, adding three kinds of above-mentioned resins is an invention of the present invention, passed through the arduous test of contriver, be surprised to find, after having added above-mentioned three kinds of resins, in conjunction with epoxy modified acrylic resin, again through the allotment part by weight, make the antiseptic property of product of the present invention increase substantially, passed through strict test after, the result who obtains is very good.Another invention of the present invention is exactly to add above-mentioned nano material, though also often use above-mentioned nano material in this area as the wear resistance and the ability and ultraviolet resistance that strengthen coating, but through experiment many times, add wherein a kind of or too much kind separately and can not obtain gratifying effect, at last, discovery adds above-mentioned component according to above-mentioned ratio, has best enhancing antiultraviolet corrosive effect and best attrition resistant effect, especially film forming better effects if.
Above-mentioned solvent is selected from: a kind of in N-BUTYL ACETATE, aromatic solvent, dimethylbenzene, toluene, pimelinketone, the propyl carbinol, preferably butylacetate.Above-mentioned functional aid: one or more in defoamer, flow agent, dispersion agent, anti-flood and anti-float agent, adhesion promoter, the sag prevention auxiliary agent, addition are conventional amount used, preferably add the poly-methyl alkyl siloxane of convention amount.These all are the ordinary skill in the art, add getting final product with the ratio of routine.
Go up as follows as the production stage of product:
1). batching, proportionally with various resins, functional aid (or preferably adding again: nano titanium oxide, nano-aluminium oxide, nano zircite), under rotating speed 650-750 rev/min, carry out pre-dispersedly, 20-40 minute is evenly;
2). proportionally titanium dioxide is dropped in the above-mentioned stoste, again with rotating speed 1200-1400 rev/min high speed dispersion 25-45 minute;
3). with machine sand milling on finely dispersed material 2-3 time, each 20-50 minute;
4). routine inspection;
5). filter, strainer or the 160 order metallic sieves of qualified after testing coating with 50-100 μ m are filtered, separately packing;
6). pack the product of the present invention that arrives that promptly gets separately after proportionally taking by weighing the B component.
Above-mentioned steps 3) processing parameter of described sand milling is: rotating speed is 1800-2200 rev/min during operation, and sand milling barrel temperature 50-60 degree wherein, adopts cooling water temperature.
Above-mentioned steps 3) in, in the sand grinding process, needs that the discharging filtering net is carried out discontinuity and scrub,, preferably once cleaned every 5-8 minute in order to avoid mesh stops up.
Above-mentioned steps 4) in, the standard of check is: viscosity is 〉=50s; Fineness is≤60 μ m.
[beneficial effect]
Protective system of the present invention has the following advantages:
This coating has excellent acid, alkali, brine corrosion performance, strong adhesion, and snappiness is good, and perviousness is strong, good weatherability, and nontoxic, fast drying, easy construction, and advantage such as can on the base steel layer of rust also, brush.Its key technical indexes meets national coating technology quality standard Q/320582TQ01-1999 set quota, and product uses and shows that its performance is in international most advanced level.Product wholesomeness of the present invention meets GB/T17219-1998 " producing the water hygiene administration Regulations for Supervision " standard code requirement.
(4) description of drawings
Fig. 1: preparation technology's schema of protective system of the present invention.
(5) embodiment
Following examples are used to explain method of the present invention, but are not used for limiting the scope of the invention.
Embodiment 1
1). batching, proportionally with epoxy modified acrylic resin, chlorinated polyether resin, acrylic resin, the inorganic silicic acid resin, functional aid carries out pre-dispersedly under 750 rev/mins of rotating speeds, and 40 minutes are evenly;
2). proportionally titanium dioxide is dropped in the above-mentioned stoste, again with 1200 rev/mins of high speed dispersion of rotating speed 45 minutes;
3). with machine sand milling on the finely dispersed material 3 times, each 20 minutes; The processing parameter of sand milling is: rotating speed is 2200 rev/mins during operation, and sand milling barrel temperature 60 degree wherein, adopt cooling water temperature.In the sand grinding process, need that the discharging filtering net is carried out discontinuity and scrub,, preferably once cleaned every 8 minutes in order to avoid mesh stops up.
4). routine inspection; The standard of check is: viscosity is 〉=50s; Fineness is≤60 μ m.
5). filter, the strainer of qualified after testing coating with 50 μ m filtered, separately packing;
6). pack the product of the present invention that arrives that promptly gets separately after proportionally taking by weighing the B component.
Composition and the weight ratio of A comprise:
Epoxy modified acrylic resin 60
Chlorinated polyether resin 8
Acrylic resin 3
Inorganic silicic acid resin 8
Chlorinated polyether resin 8
Acrylic resin 3
Inorganic silicic acid resin 8
Solvent 6
N-butyl acetate 10
Rutile titanium white powder 40
Functional aid 0.8;
The composition of B is as follows:
Modified polyurethane resin;
The part by weight of A component and B component is 4: 1.
Embodiment 2
1). batching, proportionally with epoxy modified acrylic resin, chlorinated polyether resin, acrylic resin, inorganic silicic acid resin, functional aid carry out pre-dispersedly under 650 rev/mins of rotating speeds, and 20-40 minute is evenly;
2). proportionally titanium dioxide is dropped in the above-mentioned stoste, again with 1200 rev/mins of high speed dispersion of rotating speed 45 minutes;
3). with machine sand milling on the finely dispersed material 2 times, each 50 minutes; The processing parameter of sand milling is: rotating speed is 1800 rev/mins during operation, and sand milling barrel temperature 50 degree wherein, adopt cooling water temperature.In the sand grinding process, need that the discharging filtering net is carried out discontinuity and scrub,, preferably once cleaned every 8 minutes in order to avoid mesh stops up.
4). routine inspection; The standard of check is: viscosity is 〉=50s; Fineness is≤60 μ m.
5). filter, the strainer of qualified after testing coating with 100 μ m filtered, separately packing;
6). pack the product of the present invention that arrives that promptly gets separately after proportionally taking by weighing the B component.
Composition and the weight ratio of A comprise:
Epoxy modified acrylic resin 60
Chlorinated polyether resin 8
Acrylic resin 3
Inorganic silicic acid resin 8
Solvent 6
N-butyl acetate 10
Rutile titanium white powder 40
Functional aid 0.8;
The composition of B is as follows:
Modified polyurethane resin;
The part by weight of A component and B component is 6: 1.
Embodiment 3
1). batching, proportionally with epoxy modified acrylic resin, chlorinated polyether resin, acrylic resin, the inorganic silicic acid resin, functional aid, inorganic silicic acid resin, nano titanium oxide, nano-aluminium oxide, nano zircite carries out pre-dispersedly under 750 rev/mins of rotating speeds, and 20 minutes are evenly;
2). proportionally titanium dioxide is dropped in the above-mentioned stoste, again with 1400 rev/mins of high speed dispersion of rotating speed 25 minutes;
3). with machine sand milling on the finely dispersed material 3 times, each 320-50 minute; The processing parameter of sand milling is: rotating speed is 1800 rev/mins during operation, and sand milling barrel temperature 50 degree wherein, adopt cooling water temperature.In the sand grinding process, need that the discharging filtering net is carried out discontinuity and scrub,, preferably once cleaned every 8 minutes in order to avoid mesh stops up.
4). routine inspection; The standard of check is: viscosity is 〉=50s; Fineness is≤60 μ m.
5). filter, the strainer of qualified after testing coating with 80 μ m filtered, separately packing;
6). pack the product of the present invention that arrives that promptly gets separately after proportionally taking by weighing the B component.
Composition and the weight ratio of A comprise:
Epoxy modified acrylic resin 40
Chlorinated polyether resin 8
Acrylic resin 3
Inorganic silicic acid resin 8
Solvent 2
N-butyl acetate 6
Rutile titanium white powder 35
Functional aid 0.4
Inorganic silicic acid resin 3
Nano titanium oxide 1
Nano-aluminium oxide 2
Nano zircite 1;
The composition of B is as follows:
Modified polyurethane resin;
The part by weight of A component and B component is 4: 1.
Embodiment 4
1). batching, proportionally with epoxy modified acrylic resin, chlorinated polyether resin, acrylic resin, the inorganic silicic acid resin, functional aid, inorganic silicic acid resin, nano titanium oxide, nano-aluminium oxide, nano zircite carries out pre-dispersedly under 650 rev/mins of rotating speeds, and 20 minutes are evenly;
2). proportionally titanium dioxide is dropped in the above-mentioned stoste, again with 1200 rev/mins of high speed dispersion of rotating speed 35 minutes;
3). with machine sand milling on the finely dispersed material 2 times, each 40 minutes; The processing parameter of sand milling is:
Rotating speed is 1800 rev/mins during operation, and sand milling barrel temperature 50 degree wherein, adopt cooling water temperature.In the sand grinding process, need that the discharging filtering net is carried out discontinuity and scrub,, preferably once cleaned every 6 minutes in order to avoid mesh stops up.
4). routine inspection; The standard of check is: viscosity is 〉=50s; Fineness is≤60 μ m.
5). filter, qualified after testing coating is filtered with 160 order metallic sieves, separately packing;
6). pack the product of the present invention that arrives that promptly gets separately after proportionally taking by weighing the B component.
Composition and the weight ratio of A comprise:
Epoxy modified acrylic resin 60
Chlorinated polyether resin 8
Acrylic resin 3
Inorganic silicic acid resin 8
Solvent 6
N-butyl acetate 10
Rutile titanium white powder 40
Functional aid 0.8;
Inorganic silicic acid resin 8
Nano titanium oxide 5
Nano-aluminium oxide 5
Nano zircite 4;
The composition of B is as follows:
Modified polyurethane resin;
The part by weight of A component and B component is 2: 1.
Embodiment 5
1). batching, proportionally with epoxy modified acrylic resin, chlorinated polyether resin, acrylic resin, the inorganic silicic acid resin, functional aid, inorganic silicic acid resin, nano titanium oxide, nano-aluminium oxide, nano zircite carries out pre-dispersedly under 690 rev/mins of rotating speeds, and 35 minutes are evenly;
2). proportionally titanium dioxide is dropped in the above-mentioned stoste, again with 1300 rev/mins of high speed dispersion 25-45 of rotating speed minutes;
3). with machine sand milling on the finely dispersed material 2 times, each 50 minutes; The processing parameter of sand milling is: rotating speed is 2000 rev/mins during operation, and sand milling barrel temperature 60 degree wherein, adopt cooling water temperature.In the sand grinding process, need that the discharging filtering net is carried out discontinuity and scrub,, preferably once cleaned every 8 minutes in order to avoid mesh stops up.
4). routine inspection; The standard of check is: viscosity is 〉=50s; Fineness is≤60 μ m.
5). filter, the strainer of qualified after testing coating with 50 μ m filtered, separately packing;
6). pack the product of the present invention that arrives that promptly gets separately after proportionally taking by weighing the B component.
Composition and the weight ratio of A comprise:
Epoxy modified acrylic resin 60
Chlorinated polyether resin 8
Acrylic resin 3
Inorganic silicic acid resin 8
Solvent 2
N-butyl acetate 10
Rutile titanium white powder 35
Functional aid 0.8;
The composition of B is as follows:
Modified polyurethane resin;
The part by weight of A component and B component is 6: 1.
Embodiment 6
Method is with embodiment 1;
Composition and the weight ratio of A comprise:
Epoxy modified acrylic resin 50
Chlorinated polyether resin 8
Acrylic resin 3
Inorganic silicic acid resin 8
Solvent 4
N-butyl acetate 8
Rutile titanium white powder 37.4
Functional aid 0.6;
The composition of B is as follows:
Modified polyurethane resin;
The part by weight of A component and B component is 4: 1.
Embodiment 7
Method is with embodiment 5;
Composition and the weight ratio of A comprise:
Epoxy modified acrylic resin 50
Chlorinated polyether resin 8
Acrylic resin 8
Inorganic silicic acid resin 8
Solvent 4
N-butyl acetate 8
Rutile titanium white powder 37.4
Poly-methyl alkyl siloxane 0.6
Inorganic silicic acid resin 5
Nano titanium oxide 3
Nano-aluminium oxide 3
Nano zircite 3;
The composition of B is as follows:
Modified polyurethane resin;
The part by weight of A component and B component is 4: 1.
Embodiment 8
Method is with embodiment 5;
Composition and the weight ratio of A comprise:
Epoxy modified acrylic resin 50
Chlorinated polyether resin 3
Acrylic resin 3
Inorganic silicic acid resin 3
Solvent 4
N-butyl acetate 8
Rutile titanium white powder 37.4
Poly-methyl alkyl siloxane 0.6
Inorganic silicic acid resin 5
Nano titanium oxide 3
Nano-aluminium oxide 3
Nano zircite 3;
The composition of B is as follows:
Modified polyurethane resin;
The part by weight of A component and B component is 4: 1.
Embodiment 9
Method is with embodiment 5;
Composition and the weight ratio of A comprise:
Epoxy modified acrylic resin 50
Chlorinated polyether resin 8
Acrylic resin 3
Inorganic silicic acid resin 8
Solvent 4
N-butyl acetate 8
Rutile titanium white powder 37.4
Poly-methyl alkyl siloxane 0.6
Inorganic silicic acid resin 5
Nano titanium oxide 3
Nano-aluminium oxide 3
Nano zircite 3;
The composition of B is as follows:
Modified polyurethane resin;
The part by weight of A component and B component is 4: 1.
The protective system technical indicator that obtains with above-mentioned preferred embodiment is as follows:
Project | Unit | Index | |
Color and luster | The A component | Yellowish or white, grey liquid | |
The B component | Pale yellow transparent liquid | ||
Appearance of film | Smooth smooth | ||
Time of drying | Hour | Surface drying: 1; Do solid work: 24 | |
Viscosity (being coated with 4 glasss) (colored paint) | Second | 50-70 |
Solids content | % | 60 |
Hide sub-power | g/m 2 | 95 |
Shock strength | kg·cm | 80 |
Sticking power (colored paint) | Level | 1 |
Temper(ing) (2000 hours) | Level | 1 |
Snappiness | Mm | 1 |
Water-intake rate (24 hours) is not more than | % | 0.2 |
Wear resistance (1000 change load-carrying 750kg) | g | 0.05 |
Corrosion resistance nature
Medium | Concentration | Soak time | Anti-corrosion degree |
Salt solution | 3% | 2 years | Excellent |
Sulfuric acid | 10% 30% 50% | 500 hours 500 hours 30 days | Excellent excellent |
Hydrochloric acid | 10% 30% | 30 days 500 hours | Excellent |
Phosphoric acid | 10% 30% | 500 hours 500 hours | Excellent |
Sodium hydroxide | 10% 30% | 500 hours 30 days | Excellent |
Ammoniacal liquor | 27% | 30 days | Excellent |
Gasoline | 7 days | Excellent | |
Salt fog | 1032 hours | Excellent | |
Warm | 10 days | Excellent | |
Ultraviolet ray | 2 years | Excellent |
Claims (10)
1. protective system, it is characterized in that: it is made up of A, B two portions, wherein:
Composition and the weight ratio of A comprise:
Epoxy modified acrylic resin 40-60
Solvent 2-6
N-butyl acetate 6-10
Rutile titanium white powder 35-40
Functional aid 0.4-0.8;
The composition of B is as follows:
Modified polyurethane resin;
The part by weight of A component and B component is (2-6): 1.
2. protective system as claimed in claim 1 is characterized in that:
Composition and the weight ratio of described A comprise:
Epoxy modified acrylic resin 50
Solvent 4
N-butyl acetate 8
Rutile titanium white powder 37.4
Functional aid 0.6.
3. protective system as claimed in claim 1 or 2, it is characterized in that: also include following component and weight part ratio thereof in the described A component: chlorinated polyether resin 3-8, acrylic resin 3-8, inorganic silicic acid resin 3-8, nano titanium oxide 1-5, nano-aluminium oxide 2-5, nano zircite 1-4 (have to strengthen and put ultraviolet ray corrosion and attrition resistant especially effect).
4. protective system as claimed in claim 1 is characterized in that: preferred 4: 1 of the part by weight of A component and B component.
5. protective system as claimed in claim 1 or 2 is characterized in that: described solvent is selected from: a kind of in N-BUTYL ACETATE, aromatic solvent, dimethylbenzene, toluene, pimelinketone, the propyl carbinol, preferably butylacetate.
6. protective system as claimed in claim 1 or 2, it is characterized in that: described functional aid: one or more in defoamer, flow agent, dispersion agent, anti-flood and anti-float agent, adhesion promoter, the sag prevention auxiliary agent, addition is a conventional amount used, preferably adds the poly-methyl alkyl siloxane of convention amount.
7. as the preparation method of product as described among the claim 1-6 any, it is characterized in that: the production stage of product is as follows: 1). batching, proportionally various resins, functional aid (or preferably add: nano titanium oxide again, nano-aluminium oxide, nano zircite), carry out pre-dispersedly under rotating speed 650-750 rev/min, 20-40 minute evenly; 2). proportionally titanium dioxide is dropped in the above-mentioned stoste, again with rotating speed 1200-1400 rev/min high speed dispersion 25-45 minute; 3). with machine sand milling on finely dispersed material 2-3 time, each 20-50 minute; 4). routine inspection; 5). filter, strainer or the 160 order metallic sieves of qualified after testing coating with 50-100 μ m are filtered, separately packing; 6). pack the product of the present invention that arrives that promptly gets separately after proportionally taking by weighing the B component.
8. as the preparation method of product as described in the claim 7, it is characterized in that: the processing parameter of the described sand milling of step 3) is: rotating speed is 1800-2200 rev/min during operation, and sand milling barrel temperature 50-60 degree wherein, adopts cooling water temperature.
9. as the preparation method of product as described in claim 7 or 8, it is characterized in that: in the step 3), in the sand grinding process, need to carry out discontinuity and scrubs,, preferably once cleaned every 5-8 minute in order to avoid mesh stops up to the discharging filtering net.
10. as the preparation method of product as described in the claim 7, it is characterized in that: in the step 4), the standard of check is: viscosity is 〉=50s; Fineness is≤60 μ m.
Priority Applications (1)
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CNA2008100568349A CN101220234A (en) | 2008-01-25 | 2008-01-25 | Anticorrosion paint and method for producing the same |
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CNA2008100568349A CN101220234A (en) | 2008-01-25 | 2008-01-25 | Anticorrosion paint and method for producing the same |
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CN105778672B (en) * | 2014-12-19 | 2018-02-23 | 天津科瑞达涂料化工有限公司 | A kind of ultrafast dry resist blocking and that cast tube anticorrosive paint |
CN104877533A (en) * | 2015-06-05 | 2015-09-02 | 广西大学 | Paint composition for amphibious ship and dock |
CN105820683A (en) * | 2016-05-24 | 2016-08-03 | 杭州萧山临江化工制品有限公司 | Anti-corrosion coating for marine steel structure |
CN105860779A (en) * | 2016-06-24 | 2016-08-17 | 张秋莲 | Anti-corrosion environmentally friendly paint for electric vehicle and preparation method of anti-corrosion environmentally friendly paint |
CN106634291A (en) * | 2016-10-09 | 2017-05-10 | 深圳市烯世传奇科技有限公司 | Functional anticorrosion coating for steel surfaces and a preparing method thereof |
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