CN101168927A - Environment-friendly type reactive dye printing slurry and preparation method thereof - Google Patents
Environment-friendly type reactive dye printing slurry and preparation method thereof Download PDFInfo
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- CN101168927A CN101168927A CNA2007101334870A CN200710133487A CN101168927A CN 101168927 A CN101168927 A CN 101168927A CN A2007101334870 A CNA2007101334870 A CN A2007101334870A CN 200710133487 A CN200710133487 A CN 200710133487A CN 101168927 A CN101168927 A CN 101168927A
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Abstract
The invention discloses an environmental friendly active dye printing paste and a preparation method thereof. The invention is made of raw materials of etherified starch, Kx-356 synthetic resin, W-082 resin, RST resin, A-01 additive, sodium carbonate, sodium metanitrobenzne sulfonate, soft water, etc. Firstly the soft water, the sodium metanitrobenzne sulfonate and the sodium carbonate are poured into a container and stirred for 15 to 25 minutes under a speed of 800 to 1000 rotations per minute to be completely dissolved; then are heated to 70 to 90 DEG C and added with the etherified starch and stirred for 30 to 50 minutes under the speed of 800 to 1200 rotations per minute to be completely dissolved; and then are added with the W-082 resin and the A-01 additive and stirred for 25 to 35 minutes under the speed of 800 to 900 rotations per minute; and are finally added with the RST resin and continuously stirred for 25 to 35 minutes under the speed of 1500 to 1800 rotations per minute. The production cost can be greatly reduced by using the environmental friendly active dye printing paste. The invention is suitable for the screen printing and the roller printing in the textile printing industry.
Description
Technical field
The present invention relates to a kind of dye printing slurry and preparation method thereof.Specifically, be the printing paste and preparation method thereof of REACTIVE DYES.Be applicable to the wire mark or the roller printing of textile printing and dyeing industry.
Background technology
In the dye printing industry, it all is to add water with sodium alginate to mix that used printing with reactive dye is stuck with paste at present.Because sodium alginate is a natural material, it is apt to deteriorate in hot season to add the thickener that forms behind the water.Rotten for preventing it, all can in thickener, add formaldehyde usually, and formaldehyde is harmful substance, in use, not only pollutes the environment, and is unfavorable for health.In addition, in the food production industry, sodium alginate can be used as the additive of man-made jellyfish and other food.Sodium alginate can be used as the raw material of pharmacy behind over-churning.Because marine alga is a natural plants, even resource-constrained by artificial propagation, also is difficult to satisfy industrial needs.Therefore, its price comparison costliness, as printing paste, the growth cost is higher with it.
Summary of the invention
The problem to be solved in the present invention provides a kind of environment-friendly type reactive dye printing slurry.Use this environment-friendly type reactive dye printing slurry, not only do not pollute the environment, help health, and can reduce production costs.
Another problem that the present invention will solve provides a kind of method for preparing environment-friendly type reactive dye printing slurry.
For addressing the above problem, take following technical scheme:
Environment-friendly type reactive dye printing slurry characteristics of the present invention are the raw materials that contain following parts by weight:
15～25 parts of etherification starchs;
10～15 parts of Kx-356 synthetic resin;
0.5～1.0 part of W-082 resin;
15～20 parts of RST resins;
0.5～0.8 part of A-01 auxiliary agent;
10～15 parts in sodium carbonate;
3.0～6.0 parts of m-nitrobenzene sodium sulfonates;
45～65 parts of soft water;
Wherein: said etherification starch is the type etherification starch that Wuxi City tin dragon synthetic material Co., Ltd produces; Kx-356 synthetic resin is the product that rising sun chemical industry Co., Ltd of Wuxi City section produces; The W-082 resin is the product of the modest chemical industry of Shanghai City moral Co., Ltd; The RST resin is the product of Shanghai City Argonne chemistry trading company; The A-01 auxiliary agent is the product of Shanghai City Hua Jie Fine Chemical Co., Ltd; Sodium carbonate is the product of Wuxi City tin dragon synthetic material Co., Ltd; M-nitrobenzene sodium sulfonate is the product of rising sun chemical industry Co., Ltd of Wuxi City section.
The method for preparing environment-friendly type reactive dye printing slurry may further comprise the steps:
Earlier soft water, m-nitrobenzene sodium sulfonate and sodium carbonate are dropped in the container, under 800～1000 rev/mins rotating speed, stirred 15～25 minutes, they are dissolved fully;
Then, heat to 70～90 ℃; Afterwards, add etherification starch, under 800～1200 rev/mins rotating speed, stirred 30～50 minutes, make its dissolving;
Afterwards, add W-082 resin and A-01 auxiliary agent, under 800～900 rev/mins rotating speed, stirred 25～35 minutes;
At last, add the RST resin, under 1500～1800 rev/mins rotating speed, continue to stir 25～35 minutes, make environment-friendly type reactive dye printing slurry.
Take such scheme, have the following advantages:
Because environment-friendly type reactive dye printing slurry of the present invention is made by etherification starch, Kx-56 resin, W-082 resin, RST resin, A-01 auxiliary agent, sodium carbonate, m-nitrobenzene sodium sulfonate and soft water, etherification starch wherein is a modified starch, also modification of its molecular structure when synthetic is even make the dye printing of making starch in hot summer, also undergo no deterioration when temperature is higher.
Because environment-friendly type reactive dye printing slurry of the present invention undergoes no deterioration, and need not be added with harmful substances formaldehyde, in use, does not only pollute the environment, and has harmless.
In addition, because environment-friendly type reactive dye printing slurry of the present invention is except that soft water, raw materials used all is synthetic material, and the synthetic material price comparison is cheap.Compare as printing gum with adopting the natural plants sodium alginate, can reduce production costs greatly.
The specific embodiment
First embodiment:
Choose 15 parts etherification starch, 12 parts Kx-356 resin, 0.5 part W-082 resin, 20 parts RST resin, 0.6 part A-01 auxiliary agent, 10 parts sodium carbonate, 5.0 parts m-nitrobenzene sodium sulfonate and 48 parts soft water.
Earlier soft water, m-nitrobenzene sodium sulfonate and sodium carbonate are dropped in the container, use mixer, under 800 rev/mins rotating speed, stirred 15 minutes, they are dissolved fully.
Then, heat to 70 ℃.Afterwards, add etherification starch, under 800 rev/mins rotating speed, continue to stir 30 minutes, treat that etherification starch dissolves fully after, add the Kx-356 resin, under 800 rev/mins rotating speed, continue to stir 15 minutes.
Afterwards, add W-082 resin and A-01 auxiliary agent, under 800 rev/mins rotating speed, continue to stir 25 minutes.
At last, add the RST resin, under 1500 rev/mins rotating speed, continue to stir 25 minutes, make environment-friendly type reactive dye printing slurry.
Wherein:
Said etherification starch is the type etherification starch that Wuxi City tin dragon synthetic material Co., Ltd produces; Kx-356 synthetic resin is the product that rising sun chemical industry Co., Ltd of Wuxi City section produces; The W-082 resin is the product of the modest chemical industry of Shanghai City moral Co., Ltd; The RST resin is the product of Shanghai City Argonne chemistry trading company; The A-01 auxiliary agent is the product of Shanghai City Hua Jie Fine Chemical Co., Ltd; Sodium carbonate is the product of Wuxi City tin dragon synthetic material Co., Ltd; M-nitrobenzene sodium sulfonate is the product of rising sun chemical industry Co., Ltd of Wuxi City section.
Second embodiment:
Choose 20 parts etherification starch, 17 parts Kx-356 resin, 0.6 part W-082 resin, 15 parts RST resin, 0.7 part A-01 auxiliary agent, 16 parts sodium carbonate, 4.5 parts m-nitrobenzene sodium sulfonate and 55 parts soft water.
Earlier soft water, m-nitrobenzene sodium sulfonate and sodium carbonate are dropped in the container, use mixer, under 900 rev/mins rotating speed, stirred 18 minutes, they are dissolved fully.
Then, heat to 75 ℃.Afterwards, add etherification starch, under 1000 rev/mins rotating speed, continue to stir 40 minutes, treat that etherification starch dissolves fully after, add the Kx-356 resin, under 850 rev/mins rotating speed, continue to stir 20 minutes.
Afterwards, add W-082 resin and A-01 auxiliary agent, under 850 rev/mins rotating speed, continue to stir 30 minutes.
At last, add the RST resin, under 1650 rev/mins rotating speed, continue to stir 30 minutes, make environment-friendly type reactive dye printing slurry.
Wherein:
Said etherification starch is the type etherification starch that Wuxi City tin dragon synthetic material Co., Ltd produces; Kx-356 synthetic resin is the product that rising sun chemical industry Co., Ltd of Wuxi City section produces; The W-082 resin is the product of the modest chemical industry of Shanghai City moral Co., Ltd; The RST resin is the product of Shanghai City Argonne chemistry trading company; The A-01 auxiliary agent is the product of Shanghai City Hua Jie Fine Chemical Co., Ltd; Sodium carbonate is the product of Wuxi City tin dragon synthetic material Co., Ltd; M-nitrobenzene sodium sulfonate is the product of rising sun chemical industry Co., Ltd of Wuxi City section.
The 3rd embodiment:
Choose 25 parts etherification starch, 15 parts Kx-356 resin, 1.0 parts W-082 resin, 20 parts RST resin, 0.8 part A-01 auxiliary agent, 15 parts sodium carbonate, 6.0 parts m-nitrobenzene sodium sulfonate and 65 parts soft water.
Earlier soft water, m-nitrobenzene sodium sulfonate and sodium carbonate are dropped in the container, use mixer, under 1000 rev/mins rotating speed, stirred 20 minutes, they are dissolved fully.
Then, heat to 80 ℃.Afterwards, add etherification starch, under 1200 rev/mins rotating speed, continue to stir 50 minutes, treat that etherification starch dissolves fully after, add the Kx-356 resin, under 900 rev/mins rotating speed, continue to stir 25 minutes.
Afterwards, add W-082 resin and A-01 auxiliary agent, under 900 rev/mins rotating speed, continue to stir 35 minutes.
At last, add the RST resin, under 1800 rev/mins rotating speed, continue to stir 35 minutes, make environment-friendly type reactive dye printing slurry.
Wherein:
Said etherification starch is the type etherification starch that Wuxi City tin dragon synthetic material Co., Ltd produces; Kx-356 synthetic resin is the product that rising sun chemical industry Co., Ltd of Wuxi City section produces; The W-082 resin is the product of the modest chemical industry of Shanghai City moral Co., Ltd; The RST resin is the product of Shanghai City Argonne chemistry trading company; The A-01 auxiliary agent is the product of Shanghai City Hua Jie Fine Chemical Co., Ltd; Sodium carbonate is the product of Wuxi City tin dragon synthetic material Co., Ltd; M-nitrobenzene sodium sulfonate is the product of rising sun chemical industry Co., Ltd of Wuxi City section.
Claims (2)
1. environment-friendly type reactive dye printing slurry is characterized in that containing the raw material of following parts by weight:
15～25 parts of etherification starchs;
10～15 parts of Kx-356 synthetic resin;
0.5～1.0 part of W-082 resin;
15～20 parts of RST resins;
0.5～0.8 part of A-01 auxiliary agent;
10～15 parts in sodium carbonate;
3.0～6.0 parts of m-nitrobenzene sodium sulfonates;
45～65 parts of soft water;
Wherein: said etherification starch is the type etherification starch that Wuxi City tin dragon synthetic material Co., Ltd produces; Kx-356 synthetic resin is the product that rising sun chemical industry Co., Ltd of Wuxi City section produces; The W-082 resin is the product of the modest chemical industry of Shanghai City moral Co., Ltd; The RST resin is the product of Shanghai City Argonne chemistry trading company; The A-01 auxiliary agent is the product of Shanghai City Hua Jie Fine Chemical Co., Ltd; Sodium carbonate is the product of Wuxi City tin dragon synthetic material Co., Ltd; M-nitrobenzene sodium sulfonate is the product of rising sun chemical industry Co., Ltd of Wuxi City section.
2. according to the preparation method of the described environment-friendly type reactive dye printing slurry of claim 1, it is characterized in that may further comprise the steps:
Earlier soft water, m-nitrobenzene sodium sulfonate and sodium carbonate are dropped in the container, under 800～1000 rev/mins rotating speed, stirred 15～25 minutes, they are dissolved fully;
Then, heat to 70～90 ℃; Afterwards, add etherification starch, under 800～1200 rev/mins rotating speed, stirred 30～50 minutes, make its dissolving;
Afterwards, add W-082 resin and A-01 auxiliary agent, under 800～900 rev/mins rotating speed, stirred 25～35 minutes;
At last, add the RST resin, under 1500～1800 rev/mins rotating speed, continue to stir 25～35 minutes, make environment-friendly type reactive dye printing slurry.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200710133487A CN100588769C (en) | 2007-10-22 | 2007-10-22 | Environment-friendly type reactive dye printing slurry and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN200710133487A CN100588769C (en) | 2007-10-22 | 2007-10-22 | Environment-friendly type reactive dye printing slurry and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101168927A true CN101168927A (en) | 2008-04-30 |
| CN100588769C CN100588769C (en) | 2010-02-10 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN200710133487A Expired - Fee Related CN100588769C (en) | 2007-10-22 | 2007-10-22 | Environment-friendly type reactive dye printing slurry and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103741511A (en) * | 2013-12-04 | 2014-04-23 | 常熟市福亿印花炼染有限公司 | Reactive dye white discharge printing slurry and preparation method thereof |
-
2007
- 2007-10-22 CN CN200710133487A patent/CN100588769C/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103741511A (en) * | 2013-12-04 | 2014-04-23 | 常熟市福亿印花炼染有限公司 | Reactive dye white discharge printing slurry and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN100588769C (en) | 2010-02-10 |
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Granted publication date: 20100210 Termination date: 20101022 |