CN101148316B - Method and device for producing quartz glass cotton - Google Patents

Method and device for producing quartz glass cotton Download PDF

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CN101148316B
CN101148316B CN2007100531458A CN200710053145A CN101148316B CN 101148316 B CN101148316 B CN 101148316B CN 2007100531458 A CN2007100531458 A CN 2007100531458A CN 200710053145 A CN200710053145 A CN 200710053145A CN 101148316 B CN101148316 B CN 101148316B
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quartz glass
burner
glass cotton
condensers
motor
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CN101148316A (en
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欧阳葆华
刘礼智
丰凯云
鲁昌硕
吴学民
付林
杨德斌
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HUBEI FEILIHUA QUARTZ GLASS CO Ltd
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HUBEI FEILIHUA QUARTZ GLASS CO Ltd
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Abstract

The present invention relates to quartz glass wool producing process and apparatus, and belongs to the field of quartz glass fiber producing technology. The quartz glass wool producing process is one two-stage smelting process including the first drawing quartz glass rod in inner mixing burners at flame temperature of 1800-2200 deg.c into quartz glass filament and the subsequent smelting the quartz glass filament in jetting burners at flame temperature of 2000-2200 deg.c to form quartz glass wool. The apparatus consists of one precise stepless speed changing rod feeder, one inner mixing burner set, one roller drawing unit, supporting rods, one locating board, one jetting burner set, one wool collector, one frame and two motors. The present invention has homogeneous fineness of the produced quartz glass wool and high production efficiency, and is suitable for producing quartz glass wool of different sizes.

Description

A kind of manufacturing method and apparatus of quartz glass cotton
Technical field:
The present invention relates to a kind of manufacture method of quartz glass cotton and be used for the device of this manufacture method, belong to the manufacturing technology field of quartz glass fibre.
Background technology:
At present, the production of simple glass cotton has two kinds of methods, centrifuging and flame spraying, centrifuging are that raw material is melted in crucible or tank furnace, and the glass metal that fusing is good flows out through the bushing of material road end, enter sedimentator, under supercentrifuge drives, throw away the glass thread by the sidewall of sedimentator, the glass thread is under the effect of combustion chamber high temperature high-speed flame, become cellucotton by further drawing-off, by condensers it is gathered into cotton again.Flame ejection method also is that raw material is melted in crucible, and the glass metal that fusing is good flows out through bushing and forms one silk, and this is delivered in the flame of combustion chamber ejection under the traction of glue rod, forms cotton fibre, by condensers it is gathered into cotton again.But can not produce quartz glass cotton with the method for producing the simple glass cotton, its reason is that the melt temperature of silica glass need be controlled at 1800~2200 ℃, melt temperature than simple glass fiber exceeds more than 500 ℃, therefore, produce quartz glass cotton with two kinds of methods of above-mentioned production simple glass cotton and have difficulty greatly.Existing method of producing quartz glass cotton is to adopt the rod method production that blows floating, be about to quartz pushrod and quartz pushrod blown out quartz glass cotton after with 1 800~2200 ℃ high temperature and high speed flame fusing, but the quartz glass cotton filament diameter thickness that this method is produced is inhomogeneous, influence result of use, and production efficiency is extremely low.
Summary of the invention:
The objective of the invention is to: a kind of method that burner and one group of spraying burner carry out two-stage melt production quartz glass cotton of mixing in adopting a group is provided, the silica wool filament diameter thickness that the production method of the existing silica wool of solution is produced is inhomogeneous, production efficiency is low, the problem of inconvenient operation; And the supporting isolated plant of production method for this reason.
The present invention realizes above-mentioned purpose by the following technical solutions:
The manufacture method of this quartz glass cotton realizes that as follows it comprises following five different steps:
The first step: with diameter is that pack into the Precision Stepless speed change of manufacturing installation of quartz glass cotton of the 2-10 root quartz glass bar of 1-4mm is sent in the excellent device, can not deflection or dress strand when packing into.
Second step: the oxygen pressure of oxygen supply device of air is adjusted to more than or equal to 0.25MPa, gaseous-pressure for gas combustion apparatus is adjusted to more than or equal to 0.2Mpa, mix the gas ignition device of burner at first opening, open oxygen again after lighting combustion gas, and the temperature of flame is transferred to 1800-2200 ℃; Open the gas ignition device of spraying burner then, open oxygen after lighting again, the temperature of flame is transferred to 2000-2200 ℃, and the combustion jet gas velocity of spraying burner is transferred to 400m/s-500m/s.
The 3rd step: open motor power, send the linear velocity of excellent device to transfer to 15mm/min-50mm/min the Precision Stepless speed change, making quartz pushrod is 2.4 seconds-8 seconds through the fusion time of interior mixed burner flame; Linear velocity with the pair roller fiber feeder transfers to 1700mm/min-2600mm/min again.
The 4th step: the quartz glass bar that will be melted at the burner port of interior mixed burner draws with the quartz glass bar point and draws wire
Figure DEST_PATH_GSB00000060913300011
0.15mm-
Figure DEST_PATH_GSB00000060913300012
0.25mm after, send in the pair roller fiber feeder.
The 5th step: the silk that the pair roller fiber feeder is pulled out is by behind the artificial introducing pressure pin, accurately is incorporated into the burner port of spraying burner through location boundling plate, is melted the back and sprayed by the high temperature and high speed air-flow of spraying burner and form quartz glass cotton, and send in the condensers.
The 6th step: take out the quartz glass cotton of sending in the condensers and detect qualified continuation production; If defective, finely tune the linear velocity that the Precision Stepless speed change that quartz glass bar is housed is sent excellent device again according to detected result again, till the linear velocity standard that reached for the 3rd step.
The 7th step: when containing the combustion jet air-flow process condensers of quartz glass cotton, condensers is collected in quartz glass cotton together, and every 20-30min that crosses is again with the quartz glass cotton collecting packing on the condensers.
The device that is used for the manufacture method of above-mentioned quartz glass cotton send excellent device by the Precision Stepless speed change, motor a, motor b, the interior burner that mixes, the pair roller fiber feeder, pressure pin, location boundling plate, spraying burner, condensers and frame constitute, it is characterized in that: the Precision Stepless speed change is housed above the frame left end send excellent device, motor a is housed below, mix burner in being equipped with above the frame right-hand member, the pair roller fiber feeder, pressure pin, location boundling plate and spraying burner, location boundling plate and the top of spraying burner are equipped with a condensers by pole, motor b are housed below the frame right-hand member.
Mix on burner and the spraying burner in described and be connected with gas line and oxygen hose respectively.
The present invention's beneficial effect compared with prior art is, mixed burner and one group of spraying burner two-stage fused method were carried out the production of quartz glass cotton in the present invention adopted one group, make quartz glass bar elder generation after the temperature of 1800-2200 ℃ flame is drawn into silk, temperature through 2000-2200 ℃ flame is melt into quartz glass cotton again, it is inhomogeneous to have solved the silica wool filament diameter thickness that the method for existing production quartz glass cotton produces, production efficiency is extremely low, and the problem of inconvenient operation.
Description of drawings:
Fig. 1 is the front view of the manufacturing installation of quartz glass cotton;
Fig. 2 is the vertical view of the manufacturing installation of quartz glass cotton;
Fig. 3 is the partial enlarged drawing of overlooking of the manufacturing installation of quartz glass cotton.
Among the figure: 1, the Precision Stepless speed change is sent excellent device, and 2, interior mixed burner, 3, the pair roller fiber feeder, 4, pressure pin, 5, location boundling plate, 6, spraying burner, 7, condensers, 8, frame, 9, motor a, 10, motor b.
Embodiment:
The device that is used for the manufacture method of quartz glass cotton of the present invention send excellent device 1, interior mixed burner 2, pair roller fiber feeder 3, pressure pin 4, location boundling plate 5, spraying burner 6, condensers 7, frame 8, motor a9 and motor b10 to constitute (referring to accompanying drawing 1-3) by the Precision Stepless speed change.The Precision Stepless speed change is housed above frame 8 left ends send excellent device 1, motor a9 is housed below, mix burner 2, pair roller fiber feeder 3, pressure pin 4, location boundling plate 5 and spraying burner 6 in being equipped with above frame 8 right-hand members, location boundling plate 5 and the top of spraying burner 6 are equipped with a condensers 7 by pole, motor b10 are housed below frame 8 right-hand members.Interior mixing on burner 2 and the spraying burner 6 is connected with gas line and oxygen hose respectively.
The manufacture method that adopts said apparatus to produce quartz glass cotton to the present invention is lifted two specific embodiments below:
Embodiment one:
The employing diameter is that the quartz glass bar of Ф 2.0mm is produced the quartz glass cotton about 51 μ m, and hydrogen is adopted in combustion gas.
The first step: 10 quartz glass bars that with diameter are Ф 2.0mm send in the excellent device 1 by the mode of the accompanying drawing 2 Precision Stepless speed change of packing into, can not deflection or dress strand when packing into.
Second step: the oxygen pressure of oxygen supply device of air is adjusted to greater than 0.25MPa, and the hydrogen pressure of hydrogen supply device of air is adjusted to greater than 0.2Mpa.Mix the hydrogen portfire of burner 2 in opening again, open oxygen again after hydrogen is lighted, the temperature with oxyhydrogen flame transfers to 2000 ℃ again.And then open the hydrogen portfire of spraying burner 6, and after being lighted, hydrogen opens oxygen again, and the temperature with oxyhydrogen flame transfers to 2200 ℃ again, and the combustion jet gas velocity of spraying burner 6 is transferred to 460m/s.
The 3rd step: open the power supply of motor a9 and motor b10, send the linear velocity of excellent device 1 to transfer to 35mm/min the Precision Stepless speed change, making quartz pushrod is 3.4 seconds through the time of the flame of interior mixed burner 2; Linear velocity with pair roller fiber feeder 3 transfers to 2230mm/min again.After adjustment finishes, send will pack into 10 quartz glass bars in it of excellent device 1 to mix the burner port of burner 2 in being sent to by the Precision Stepless speed change that drives by motor a9, quartz glass bar is 3.4 seconds through the fusion time of the burner port of interior mixed burner 2, and quartz glass bar is melted.
The 4th step: quartz glass bar is after the burner port of interior mixed burner 2 is melted, send in the pair roller fiber feeder 3 that drives by motor b10 that linear velocity is 2230mm/min by the silica glass silk that manually draws into 0.22mm again with the quartz glass bar point, and the left side wire drawing of formation pair roller fiber feeder 3, its right automatic feeding.
The 5th step: behind the silica glass silk process pressure pin of manually pair roller fiber feeder 3 being sent 4, put into location boundling plate 5, accurately be incorporated into the burner port of spraying burner 6 through location boundling plate 5, make its under 2200 ℃ oxyhydrogen flame of burner port with the fusion of silica glass silk, spray with the high temperature and high speed air-flow of 460m/s by spraying burner 6 again and form quartz glass cotton (as shown in Figure 3), and send in the condensers 7.
The 6th step: take out the quartz glass cotton of sending in the condensers and detect qualified continuation production; If defective, finely tune the linear velocity that the Precision Stepless speed change that quartz glass bar is housed is sent excellent device 1 again according to detected result, till the linear velocity standard that reached for the 3rd step.
The 7th step: the high temperature and high speed air-flow that contains quartz glass cotton is during through condensers 7, and condensers 7 is collected in quartz glass cotton together, every cross 20min again by artificial with the quartz glass cotton collecting packing on the condensers 7.
Embodiment two:
The employing diameter is that the quartz glass bar of Φ 3.0mm is produced the quartz glass cotton about 9 μ m, and hydrogen is adopted in combustion gas.
The first step: 10 quartz glass bars that with diameter are Φ 3.0mm send in the excellent device 1 by the mode of the accompanying drawing 2 Precision Stepless speed change of packing into, can not deflection or dress strand when packing into.
Second step: the oxygen pressure of oxygen supply device of air is adjusted to greater than 0.25MPa, and the hydrogen pressure of hydrogen supply device of air is adjusted to greater than 0.2Mpa.Mix the hydrogen portfire of burner 2 in opening again, open oxygen again after hydrogen is lighted, the temperature with oxyhydrogen flame transfers to 2100 ℃ again.And then open the hydrogen portfire of spraying burner 6, and after being lighted, hydrogen opens oxygen again, and the temperature with oxyhydrogen flame transfers to 2200 ℃ again, and the combustion jet gas velocity of spraying burner 6 is transferred to 430m/s.
The 3rd step: open the power supply of motor a9 and motor b10, send the linear velocity of excellent device 1 to transfer to 20mm/min the Precision Stepless speed change, making quartz pushrod is 6 seconds through the time of the flame of interior mixed burner 2; Linear velocity with pair roller fiber feeder 3 transfers to 2410mm/min again.After adjustment finishes, send will pack into 10 quartz glass bars in it of excellent device 1 to mix the burner port of burner 2 in being sent to by the Precision Stepless speed change that drives by motor a9, quartz glass bar is 6 seconds through the fusion time of the burner port of interior mixed burner 2, and quartz glass bar is melted.
The 4th step: quartz glass bar is after the burner port of interior mixed burner 2 is melted, send in the pair roller fiber feeder 3 that drives by motor b10 that linear velocity is 2418mm/min by the silica glass silk that manually draws into 0.24mm again with the quartz glass bar point, and the left side wire drawing of formation pair roller fiber feeder 3, its right automatic feeding.
The 5th step: behind the silica glass silk process pressure pin of manually pair roller fiber feeder 3 being sent 4, put into location boundling plate 5, accurately be incorporated into the burner port of spraying burner 6 through location boundling plate 5, make its under 2200 ℃ oxyhydrogen flame of burner port with the fusion of silica glass silk, spray with the high temperature and high speed air-flow of 430m/s by spraying burner 6 again and form quartz glass cotton (as shown in Figure 3), and send in the condensers 7.
The 6th step: take out the quartz glass cotton of sending in the condensers and detect qualified continuation production; If defective, finely tune the linear velocity that the Precision Stepless speed change that quartz glass bar is housed is sent excellent device 1 again according to detected result, till the linear velocity standard that reached for the 3rd step.
The 7th step: the high temperature and high speed air-flow that contains quartz glass cotton is during through condensers 7, and condensers 7 is collected in quartz glass cotton together, every cross 30min again by artificial with the quartz glass cotton collecting packing on the condensers 7.

Claims (3)

1. the manufacture method of a quartz glass cotton, it is characterized in that: it is made of following steps:
The first step: with diameter is that pack into the Precision Stepless speed change of manufacturing installation of quartz glass cotton of the 2-10 root quartz glass bar of 1-4mm is sent in the excellent device (1), can not deflection or dress strand when packing into;
Second step: the oxygen pressure of oxygen supply device of air is adjusted to more than or equal to 0.25MPa, adjusted to more than or equal to 0.2Mpa for the gaseous-pressure of gas combustion apparatus; Mix burner at first opening
(2) gas ignition device is opened oxygen again after lighting combustion gas, and the temperature of flame is transferred to 1800-2200 ℃; Open the gas ignition device of spraying burner (6) then, open oxygen after lighting again, the temperature of flame is transferred to 2000-2200 ℃, and the combustion jet gas velocity of spraying burner (6) is transferred to 400m/s-500m/s;
The 3rd step: the power supply of opening motor a (9) and motor b (10), make it drive the Precision Stepless speed change respectively and send excellent device (1) and pair roller fiber feeder (3), send the linear velocity of excellent device (1) to transfer to 15mm/min-50mm/min the Precision Stepless speed change, making quartz glass bar is 2.4 seconds-8 seconds through the fusion time of interior mixed burner (2) flame; Linear velocity with pair roller fiber feeder (3) transfers to 1700mm/min-2600mm/min again;
The 4th step: the quartz glass bar that will be melted at the burner port of interior mixed burner (2) is pulled by another root quartz glass bar point of artificial usefulness
Figure FSB00000060913200011
Behind the silk, send in the pair roller fiber feeder (3);
The 5th the step: with pair roller fiber feeder (3) pull out the silk by behind the artificial introducing pressure pin (4), accurately be incorporated into the burner port of spraying burner (6) through location boundling plate (5), high temperature and high speed air-flow injection by spraying burner (6) after being melted forms quartz glass cotton, and sends in the condensers (7);
The 6th step: take out the quartz glass cotton of sending in the condensers and detect qualified continuation production; If defective, finely tune the linear velocity that the Precision Stepless speed change that quartz glass bar is housed is sent excellent device (1) again according to detected result again, till the linear velocity standard that reached for the 3rd step;
The 7th step: when containing the combustion jet air-flow process condensers (7) of quartz glass cotton, condensers (7) is collected in quartz glass cotton together, and every 20-30min that crosses is again with the quartz glass cotton collecting packing on the condensers (7).
2. device that is used for the manufacture method of the described quartz glass cotton of claim 1, it send excellent device (1), motor a (9), motor b (10), interior mixed burner (2), pair roller fiber feeder (3), pressure pin (4), location boundling plate (5), spraying burner (6), condensers (7) and frame (8) to constitute by the Precision Stepless speed change, it is characterized in that: above frame (8) left end Precision Stepless speed change is housed and send excellent device (1), motor a (9) is housed below, and motor a (9) is connected with accurate electrodeless variable-speed feed appliance (1); Mix burner (2), pair roller fiber feeder (3), pressure pin (4), location boundling plate (5) and spraying burner (6) in being equipped with above frame (8) right-hand member, location boundling plate (5) and the top of spraying burner (6) are equipped with a condensers (7) by pole, motor b (10) are housed below frame (8) right-hand member; Motor b (10) is connected with pair roller fiber feeder (3).
3. the device of the manufacture method of quartz glass cotton according to claim 2 is characterized in that: mix on burner (2) and the spraying burner (6) being connected with gas line and oxygen hose respectively in described.
CN2007100531458A 2007-09-04 2007-09-04 Method and device for producing quartz glass cotton Active CN101148316B (en)

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CN105130183B (en) * 2015-08-17 2017-07-11 武汉鑫友泰光电科技有限公司 A kind of high temperature resistant superthin quartz cellucotton and preparation method thereof
CN107175088A (en) * 2017-07-26 2017-09-19 湖北菲利华石英玻璃股份有限公司 A kind of preparation method of the quartzy blanket of photocatalyst catalysis
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CN112759251B (en) * 2021-03-04 2023-11-03 河南神玖天航新材料股份有限公司 Horizontal quartz cotton processing equipment
CN112897871B (en) * 2021-03-04 2023-06-30 河南神玖天航新材料股份有限公司 Horizontal quartz cotton production facility
CN113185115B (en) * 2021-05-18 2023-07-18 湖北菲利华石英玻璃股份有限公司 Method and device for drawing quartz glass fiber by using quartz glass thick rod
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Citations (1)

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Publication number Priority date Publication date Assignee Title
CN1120027A (en) * 1995-02-20 1996-04-10 中国东北电力集团科技开发公司 Production technology menthod of superfine glass wool

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1120027A (en) * 1995-02-20 1996-04-10 中国东北电力集团科技开发公司 Production technology menthod of superfine glass wool

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Denomination of invention: A manufacturing method and device for quartz glass wool

Effective date of registration: 20230925

Granted publication date: 20100811

Pledgee: China Everbright Bank Co.,Ltd. Jingzhou Branch

Pledgor: HUBEI FEILIHUA QUARTZ GLASS Co.,Ltd.

Registration number: Y2023980058350