CN101126713A - Bipolar ultraviolet spectrum identification method - Google Patents

Bipolar ultraviolet spectrum identification method Download PDF

Info

Publication number
CN101126713A
CN101126713A CNA2007101639559A CN200710163955A CN101126713A CN 101126713 A CN101126713 A CN 101126713A CN A2007101639559 A CNA2007101639559 A CN A2007101639559A CN 200710163955 A CN200710163955 A CN 200710163955A CN 101126713 A CN101126713 A CN 101126713A
Authority
CN
China
Prior art keywords
identification method
ultraviolet spectrum
polarity
bipolar
spectrum identification
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CNA2007101639559A
Other languages
Chinese (zh)
Inventor
王承华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CNA2007101639559A priority Critical patent/CN101126713A/en
Publication of CN101126713A publication Critical patent/CN101126713A/en
Pending legal-status Critical Current

Links

Landscapes

  • Medicines Containing Plant Substances (AREA)

Abstract

The utility model relates to a double-polarity ultraviolet chromatogram identification method, which is characterized in that double-polarity (polarity and non-polarity) two solvent systems allows to describe ultraviolet absorption spectrum of Chinese traditional medicine based on previous operation, and make the identification of the Chinese traditional medicine according to the quantity, position, height and integral shape of chromatogram peak.

Description

Bipolar ultraviolet spectrum identification method
Technical field this method is applied to aspects such as the production, scientific research, check, quality control of Chinese medicine industry.
The background technology ultraviolet spectrum is differentiated the application of Chinese medicine, and is quite general.The ultraviolet spectrum of domestic research Chinese medicine, difference because of method, solvent, single solvent system, multisolvent system are arranged respectively, single order, second order, three order derivative ultraviolet spectrums, these achievements in research, shown that ultraviolet spectrum aspect TCD identification, has easy, quick, sensitive, characteristic of accurate, for popularization and application is laid a good foundation.
Summary of the invention is present, and this type of research makes same medicinal material multiple different ultraviolet spectrum occur because of the difference of method, solvent, is unfavorable for promoting the use of, and demands the Chinese medicine ultraviolet spectrum identification method of setting up a kind of simple and clear practicality, being convenient to popularize urgently.
The present invention is on the basis of previous work, adopt bipolar (polarity and nonpolar) two kinds of solvent systems, describe the ultra-violet absorption spectrum of Chinese medicine, according to collection of illustrative plates superiors's quantity, position, highly (absorbance log) and global shape carry out the evaluation of Chinese medicine, are " bipolar ultraviolet spectrum identification method " so name.Method: accurately take by weighing 2 parts in Chinese medicine sample, every part of 1.0g, add distilled water, each 10ml of sherwood oil (60~90 ℃) respectively in tool plug test tube, close plug, sonic oscillation 30min, filter, (1.0~100mg/ml) as need testing solution, presses test condition: slit 1nm, sweep limit 200~400nm for filtrate or dilution, sweep velocity 100nm/min measures ultraviolet spectrum, according to the quantity at collection of illustrative plates peak, position, highly (absorbance log) and global shape carry out the evaluation of Chinese medicine.

Claims (1)

1. the present invention relates to a kind of Chinese traditional medicine identification method, especially ultraviolet spectrum identification method.It is characterized in that only selecting polarity and nonpolar two kinds of solvent systems, carry out UV scanning respectively, absorption peak quantity, position, height and global shape according to two spectral lines carry out the evaluation of Chinese medicine.
CNA2007101639559A 2007-10-12 2007-10-12 Bipolar ultraviolet spectrum identification method Pending CN101126713A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNA2007101639559A CN101126713A (en) 2007-10-12 2007-10-12 Bipolar ultraviolet spectrum identification method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNA2007101639559A CN101126713A (en) 2007-10-12 2007-10-12 Bipolar ultraviolet spectrum identification method

Publications (1)

Publication Number Publication Date
CN101126713A true CN101126713A (en) 2008-02-20

Family

ID=39094792

Family Applications (1)

Application Number Title Priority Date Filing Date
CNA2007101639559A Pending CN101126713A (en) 2007-10-12 2007-10-12 Bipolar ultraviolet spectrum identification method

Country Status (1)

Country Link
CN (1) CN101126713A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106679812A (en) * 2017-01-17 2017-05-17 云南中医学院 Color quantitative detection method for traditional Chinese medicine injection

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106679812A (en) * 2017-01-17 2017-05-17 云南中医学院 Color quantitative detection method for traditional Chinese medicine injection

Similar Documents

Publication Publication Date Title
CN102876323A (en) Cadmium ion fluorescence probe, preparation method and application
CN102998411B (en) A kind of detection method of ageratum dripping pill
CN104181215A (en) Preparation of electro-polymerization molecularly imprinted polymer hollow channel paper device and application of paper device in instant pesticide residue detection
CN102297902A (en) Method for detecting nivalenol and deoxynivalenol (DON) toxins in traditional Chinese medicine
CN104003935A (en) 4-aroyl-1,8-naphthalimide compound and preparation method and use thereof
CN101638402A (en) Online quality monitoring method for salvianolic acid B production
CN101126713A (en) Bipolar ultraviolet spectrum identification method
CN108459009A (en) A method of measuring phosphate radical with Surface enhanced Raman spectroscopy
CN103387830A (en) Chromium-ion ratio type fluorescence probe as well as preparation method and application thereof
CN102068627B (en) Quality control method for Chinese medicine preparation Xinnaojing tabelets
CN105223260A (en) Trace is electrochemical sensor detecting butyl p-hydroxybenzoate and preparation method thereof fast
CN102879499A (en) Method for detecting antioxidant constituents in nitraria fruit juice by using 1,1-diphenyl-2-picrylhydrazyl (DPPH)-high performance liquid chromatography (HPLC) method
CN101530463B (en) Quality detection method of Chinese herb gentian
CN101220036B (en) Extraction of active ingredient such as betulinic acid from common camptotheca fruit with clean method
Kamel et al. Solid Contact Biosensor Based On Man-Tailored Polymers For Acetylcholine Detection: Application To Acetylcholinesterase Assay
CN102565235B (en) Method for detecting phthalic ester in white emulsion for cigarette use
CN103509069A (en) Preparation method of crude product of tea saponin and preparation method of tea saponin B1
CN105486785A (en) Method for detecting enantiomer impurity in apremilast
CN110082451A (en) A kind of SFC detection method of the chloro- 1- of 2- (the fluoro- chroman -2- of 6-) ethyl alcohol chirality alcohol intermediate preparation process
CN104655602B (en) A kind of hydrophobic ionic liquid [MBPy] Tf2The fluorescence detection method of N
CN105486761A (en) Method for determining scutelloside content in traditional Chinese medicine granules
CN1996007A (en) Identification and determination method for pear juice doped in apple juice or discoloured apple juice
CN102507830A (en) High performance liquid chromatograph method for measuring content of Quzhazhigan in Rheum lhasaense
CN103837619B (en) Fingerprint detection method for traditional Chinese medicinal Ganyanlin injection and raw medicinal material thereof
CN209416990U (en) A kind of composite chromatography column and a kind of two-dimensional liquid chromatography system

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C02 Deemed withdrawal of patent application after publication (patent law 2001)
WD01 Invention patent application deemed withdrawn after publication

Open date: 20080220