CN101011742A - Controlled method of preparing metal nano particle - Google Patents
Controlled method of preparing metal nano particle Download PDFInfo
- Publication number
- CN101011742A CN101011742A CN 200710026834 CN200710026834A CN101011742A CN 101011742 A CN101011742 A CN 101011742A CN 200710026834 CN200710026834 CN 200710026834 CN 200710026834 A CN200710026834 A CN 200710026834A CN 101011742 A CN101011742 A CN 101011742A
- Authority
- CN
- China
- Prior art keywords
- inert gas
- metal
- nano particle
- film
- metal nanoparticles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000000034 method Methods 0.000 title claims abstract description 17
- 239000002082 metal nanoparticle Substances 0.000 title claims description 20
- 239000002184 metal Substances 0.000 claims abstract description 15
- 229910052751 metal Inorganic materials 0.000 claims abstract description 15
- 239000011261 inert gas Substances 0.000 claims abstract description 14
- 238000010438 heat treatment Methods 0.000 claims abstract description 11
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 10
- 239000001257 hydrogen Substances 0.000 claims abstract description 10
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000011248 coating agent Substances 0.000 claims abstract description 5
- 238000000576 coating method Methods 0.000 claims abstract description 5
- 238000002360 preparation method Methods 0.000 claims description 12
- 239000000758 substrate Substances 0.000 claims description 11
- 239000000463 material Substances 0.000 claims description 10
- 239000007789 gas Substances 0.000 claims description 7
- 230000008021 deposition Effects 0.000 claims description 4
- 150000002431 hydrogen Chemical class 0.000 claims description 3
- 238000003723 Smelting Methods 0.000 abstract 1
- 239000007888 film coating Substances 0.000 abstract 1
- 238000009501 film coating Methods 0.000 abstract 1
- 239000010409 thin film Substances 0.000 abstract 1
- 239000002105 nanoparticle Substances 0.000 description 22
- 229910001254 electrum Inorganic materials 0.000 description 20
- XXOYNJXVWVNOOJ-UHFFFAOYSA-N fenuron Chemical compound CN(C)C(=O)NC1=CC=CC=C1 XXOYNJXVWVNOOJ-UHFFFAOYSA-N 0.000 description 20
- 239000010931 gold Substances 0.000 description 11
- 238000009826 distribution Methods 0.000 description 9
- 229910052737 gold Inorganic materials 0.000 description 8
- 239000002245 particle Substances 0.000 description 7
- 229910052709 silver Inorganic materials 0.000 description 7
- 239000006185 dispersion Substances 0.000 description 5
- 229910052802 copper Inorganic materials 0.000 description 4
- 239000010949 copper Substances 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 4
- 238000004544 sputter deposition Methods 0.000 description 4
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- 238000005530 etching Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000004332 silver Substances 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 238000000151 deposition Methods 0.000 description 2
- 238000010894 electron beam technology Methods 0.000 description 2
- 238000002524 electron diffraction data Methods 0.000 description 2
- PQTCMBYFWMFIGM-UHFFFAOYSA-N gold silver Chemical compound [Ag].[Au] PQTCMBYFWMFIGM-UHFFFAOYSA-N 0.000 description 2
- 238000002173 high-resolution transmission electron microscopy Methods 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 238000013021 overheating Methods 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000003708 ampul Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005566 electron beam evaporation Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 239000013528 metallic particle Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910021421 monocrystalline silicon Inorganic materials 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
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Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200710026834A CN100586614C (en) | 2007-02-08 | 2007-02-08 | Controlled method of preparing metal nano particle |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200710026834A CN100586614C (en) | 2007-02-08 | 2007-02-08 | Controlled method of preparing metal nano particle |
Publications (2)
Publication Number | Publication Date |
---|---|
CN101011742A true CN101011742A (en) | 2007-08-08 |
CN100586614C CN100586614C (en) | 2010-02-03 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN200710026834A Expired - Fee Related CN100586614C (en) | 2007-02-08 | 2007-02-08 | Controlled method of preparing metal nano particle |
Country Status (1)
Country | Link |
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CN (1) | CN100586614C (en) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102310038A (en) * | 2011-09-29 | 2012-01-11 | 华东交通大学 | Method for improving surface hydrophobicity of metal film |
CN102381676A (en) * | 2011-10-27 | 2012-03-21 | 无锡英普林纳米科技有限公司 | Quartz micro needle surface nano metal chain and preparation method thereof |
CN102806354A (en) * | 2012-07-31 | 2012-12-05 | 东南大学 | Method for preparing gold nanoparticles by annealing of gold film |
CN103691962A (en) * | 2013-12-20 | 2014-04-02 | 中山大学 | Preparation method of size-controllable metal nano particles |
CN107132210A (en) * | 2017-05-03 | 2017-09-05 | 北京理工大学 | A kind of substrate manufacture method of the surface-enhanced Raman based on dynamic control |
CN108807631A (en) * | 2018-05-03 | 2018-11-13 | 五邑大学 | A kind of LED epitaxial wafer and preparation method thereof of double mirror surface structures |
CN115464149A (en) * | 2022-10-18 | 2022-12-13 | 厦门大学 | Preparation method of metal nanoparticles |
-
2007
- 2007-02-08 CN CN200710026834A patent/CN100586614C/en not_active Expired - Fee Related
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102310038A (en) * | 2011-09-29 | 2012-01-11 | 华东交通大学 | Method for improving surface hydrophobicity of metal film |
CN102381676A (en) * | 2011-10-27 | 2012-03-21 | 无锡英普林纳米科技有限公司 | Quartz micro needle surface nano metal chain and preparation method thereof |
CN102381676B (en) * | 2011-10-27 | 2014-10-08 | 无锡英普林纳米科技有限公司 | Quartz micro needle surface nano metal chain and preparation method thereof |
CN102806354A (en) * | 2012-07-31 | 2012-12-05 | 东南大学 | Method for preparing gold nanoparticles by annealing of gold film |
CN103691962A (en) * | 2013-12-20 | 2014-04-02 | 中山大学 | Preparation method of size-controllable metal nano particles |
CN103691962B (en) * | 2013-12-20 | 2016-06-01 | 中山大学 | The preparation method of the metal nanoparticle that a kind of size is controlled |
CN107132210A (en) * | 2017-05-03 | 2017-09-05 | 北京理工大学 | A kind of substrate manufacture method of the surface-enhanced Raman based on dynamic control |
CN107132210B (en) * | 2017-05-03 | 2019-09-17 | 北京理工大学 | A kind of substrate manufacturing method of the surface-enhanced Raman based on dynamic control |
CN108807631A (en) * | 2018-05-03 | 2018-11-13 | 五邑大学 | A kind of LED epitaxial wafer and preparation method thereof of double mirror surface structures |
CN115464149A (en) * | 2022-10-18 | 2022-12-13 | 厦门大学 | Preparation method of metal nanoparticles |
Also Published As
Publication number | Publication date |
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CN100586614C (en) | 2010-02-03 |
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SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C53 | Correction of patent for invention or patent application | ||
CB03 | Change of inventor or designer information |
Inventor after: Xu Ningsheng Inventor after: Yao Rihui Inventor after: She Juncong Inventor after: Deng Shaozhi Inventor after: Chen Jun Inventor before: Xu Ningsheng Inventor before: Yao Rihui Inventor before: She Juncong Inventor before: Deng Shaozhi Inventor before: Chen Jun |
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CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20100203 Termination date: 20170208 |
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CF01 | Termination of patent right due to non-payment of annual fee |