CN101003916A - Jet type electrostatic spinning equipment capable of producing Nano fiber in bulk - Google Patents

Jet type electrostatic spinning equipment capable of producing Nano fiber in bulk Download PDF

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Publication number
CN101003916A
CN101003916A CN 200710036447 CN200710036447A CN101003916A CN 101003916 A CN101003916 A CN 101003916A CN 200710036447 CN200710036447 CN 200710036447 CN 200710036447 A CN200710036447 A CN 200710036447A CN 101003916 A CN101003916 A CN 101003916A
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China
Prior art keywords
storage tank
liquid storage
electrostatic spinning
shower nozzle
pole plate
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Granted
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CN 200710036447
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Chinese (zh)
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CN100503905C (en
Inventor
刘雍
何吉欢
俞建勇
徐岚
刘丽芳
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Donghua University
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Donghua University
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Priority to CNB2007100364474A priority Critical patent/CN100503905C/en
Publication of CN101003916A publication Critical patent/CN101003916A/en
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Publication of CN100503905C publication Critical patent/CN100503905C/en
Expired - Fee Related legal-status Critical Current
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  • Nonwoven Fabrics (AREA)

Abstract

The present invention discloses an air-jet type electrostatic spinning equipment for large lot production of nanofibre. Said equipment includes the following several portions: storage liquor tank, high-voltage electrostatic generator, spray head, air pump, receiving electrode plate, air-duct, receiving curtain, guiding roller, ground electrode withdrawal roller and winding roller. Besides, said invention also provides the connection mode of all the above-mentioned portions.

Description

A kind of jet type electrostatic spinning equipment that can be used for producing in enormous quantities nanofiber
Technical field
The present invention relates to a kind of spinning equipment, particularly relate to a kind of jet type electrostatic spinning equipment that can be used for producing in enormous quantities nanofiber.
Background technology
Mostly the device of present widely used electrostatic spinning nano fiber is single shower nozzle or many shower nozzles syringe-type device for spinning, as Chinese patent application ZL200420107832.5, ZL200420020596.3, ZL200320122276.4, ZL200410025622.6 etc., U.S. Pat 6616435, US6713011, US6753454, US6656394, world patent WO06043968, WO2005/073441, WO2005/073442, WO2006/018838, WO2006/007287, WO2005/026398, WO2005/123995, WO2004/016839, WO04074559, WO0209288A1, WO2005/099308, WO2006/049664, WO2005/090653A1, the multi-nozzle electrospinning apparatus structure schematic diagram that Fig. 1 arranges for matrix form.
No matter be single spray orifice or many spray orifices spinning process, because injection diameter is less, so have spinning efficiency and yield poorly down the easily stifled and cleaning difficulty of spinneret orifice, electric field serious interference between the adjacent spinning head can't satisfy the defectives such as requirement that production in enormous quantities and product are used.Even have indivedual patents such as WO 2005/090653A1 to adopt many spray orifices form of hydrojet that makes progress, but still have this shortcoming.
Summary of the invention
Technical problem to be solved by this invention provides a kind of jet type electrostatic spinning equipment that can be used for producing in enormous quantities nanofiber, to remedy the deficiencies in the prior art or defective, meets the demands of production and living.
In order to solve the problems of the technologies described above technical scheme that the present invention adopts be: a kind of jet type electrostatic spinning equipment that can be used for producing in enormous quantities nanofiber, comprise liquid storage tank 1, HV generator 2, shower nozzle 4, air pump 3 and reception pole plate 7, the upper end open of described liquid storage tank 1, the bottom surface of liquid storage tank 1 is provided with shower nozzle 4 vertically upward, shower nozzle 4 links to each other with air pump 3 by wireway 5, wireway 5 and air pump 3 connecting places are higher than the liquid level of liquid storage tank 1, liquid storage tank 1 links to each other with HV generator 2 by metal electrode, be provided with a conveyer directly over the liquid storage tank 1 and receive curtain 8, conveyer is formed by receiving pole plate 7 and deflector roll 9, receive curtain 8 and be close to reception pole plate 7 and deflector roll 9, provide tension force and part to transmit power by receiving pole plate 7 and deflector roll 9, receiving pole plate 7 links to each other with earth electrode 10 by deflector roll 9, receive curtain 8 one ends and connect unwinding roll shaft 11, the other end is connected with coiling roll shaft 12.
As optimized technical scheme: described shower nozzle 4 is a plurality of and presses matrix and arrange.
When the present invention works, at first inject solution or melt 6 in liquid storage tank 1, institute's liquid volume added should be lower than the upper port of liquid storage tank.Open air pump 3, air pressure is lower during beginning, earlier liquid in the wireway 5 is discharged, and slowly adds atmospheric pressure again, makes liquid level have rule vacuole, projection or fountain shape fluid column.Open HV generator 2 then, be adjusted to certain voltage.With polarized, electric charge will concentrate on protruding solution top to the liquid internal free charge under the high-pressure electrostatic effect, form taylor cone.One conveyer is arranged and receive curtain 8 apart from liquid storage tank 1 upper port certain distance, conveyer is formed by receiving pole plate 7 and deflector roll 9, receives pole plate 7 ground connection and forms negative pole, and form electric field between the liquid level.Under proper condition, because the effect of electrostatic force has the ejection of superfine liquid or melt jet from the taylor cone top, the directive negative plate is deposited on the reception curtain 8, forms a large amount of nanofibers, along with transmission device is with from the fibre-collecting zone.Receive curtain 8 and be wound on the unwinding roll shaft 11, the other end is connected on the coiling roll shaft 12, along with the carrying out of spinning, carries out unwinding and coiling with certain speed, thereby assurance fiber uniform fibers felt is with from spinning zone and is wound on the take up roll.
The invention has the beneficial effects as follows: can realize the needs of scale production of nanofiber, need not frequently to change spinneret orifice, and highly efficient in productivity, can satisfy the needs to nanofiber and Related product thereof such as production in enormous quantities and product application.
Description of drawings
The electrostatic spinning apparatus structural representation of many spray nozzle types of Fig. 1 prior art nanofiber
Fig. 2 structural representation of the present invention
The vertical structure schematic diagram of shower nozzle 4 among Fig. 3 the present invention
The transversary schematic diagram of shower nozzle 4 among Fig. 4 the present invention
Wherein, the 1-liquid storage tank, the 2-HV generator, the 3-air pump, the 4-shower nozzle, the 5-wireway, 6-solution or melt, 7-receives pole plate, and 8-receives curtain, 9-deflector roll, 10-earth electrode, 11-unwinding roll shaft, 12-coiling roll shaft
The specific embodiment
Below in conjunction with specific embodiment the present invention is further elaborated, with reference to accompanying drawing 1-4.
Embodiment 1
A kind of jet type electrostatic spinning equipment that can be used for producing in enormous quantities nanofiber, comprise liquid storage tank 1, HV generator 2, shower nozzle 4, air pump 3 and reception pole plate 7, the upper end open of described liquid storage tank 1, the bottom surface of liquid storage tank 1 is provided with by matrix arrangement shower nozzle 4 vertically upward, shower nozzle 4 links to each other with air pump 3 by wireway 5, conduit and air pump 3 connecting places are higher than the liquid level of liquid storage tank 1, liquid storage tank 1 links to each other with HV generator 2 by metal electrode, be provided with a conveyer directly over the liquid storage tank 1 and receive curtain 8, conveyer is formed by receiving pole plate 7 and deflector roll 9, receiving pole plate 7 links to each other with earth electrode 10 by deflector roll 9, receive curtain 8 one ends and connect unwinding roll shaft 11, the other end is connected with coiling roll shaft 12.

Claims (2)

1, a kind of jet type electrostatic spinning equipment that can be used for producing in enormous quantities nanofiber, comprise liquid storage tank (1), HV generator (2), shower nozzle (4), air pump (3) and reception pole plate (7), it is characterized in that: the upper end open of described liquid storage tank (1), the bottom surface of liquid storage tank (1) is provided with shower nozzle (4) vertically upward, shower nozzle (4) links to each other with air pump (3) by wireway (5), wireway (5) and air pump (3) connecting place are higher than the liquid level of liquid storage tank (1), liquid storage tank (1) links to each other with HV generator (2) by metal electrode, be provided with a conveyer directly over the liquid storage tank (1) and receive curtain (8), described conveyer is formed by receiving pole plate (7) and deflector roll (9), receive curtain (8) and be close to reception pole plate (7) and deflector roll (9), receiving pole plate (7) links to each other with earth electrode (10) by deflector roll (9), receive curtain (8) one ends and connect unwinding roll shaft (11), the other end is connected with coiling roll shaft (12).
2, electrostatic spinning apparatus according to claim 1 is characterized in that: described shower nozzle (4) is pressed matrix and is arranged.
CNB2007100364474A 2007-01-12 2007-01-12 Jet type electrostatic spinning equipment capable of producing Nano fiber Expired - Fee Related CN100503905C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNB2007100364474A CN100503905C (en) 2007-01-12 2007-01-12 Jet type electrostatic spinning equipment capable of producing Nano fiber

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNB2007100364474A CN100503905C (en) 2007-01-12 2007-01-12 Jet type electrostatic spinning equipment capable of producing Nano fiber

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Publication Number Publication Date
CN101003916A true CN101003916A (en) 2007-07-25
CN100503905C CN100503905C (en) 2009-06-24

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Cited By (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008095239A1 (en) * 2007-02-05 2008-08-14 Commonwealth Scientific And Industrial Research Organisation Nanofibre yarns
CN102015121A (en) * 2008-02-29 2011-04-13 斯托拉恩索公司 Method for producing particles electrostatically
CN101812733B (en) * 2009-02-20 2011-05-18 北京化工大学 Continuously-producing high-efficiency melt electrostatic spinning device
CN101586288B (en) * 2009-07-06 2011-08-31 江苏泰灵生物科技有限公司 Array multi-nozzle electrospinning device
CN102312297A (en) * 2011-08-22 2012-01-11 北京化工大学 Wire-brush-type differential fusant electrostatic spinning device and method
CN101871131B (en) * 2009-04-23 2012-05-02 廊坊高山电子科技有限公司 Nanoparticle/polymer material composite ultrafine fiber preparation device
CN102493000A (en) * 2011-11-30 2012-06-13 福建农林大学 Low-speed transmission belt type collector for electrostatic spinning equipment
CN102534822A (en) * 2012-02-18 2012-07-04 上海工程技术大学 Device and method for preparing polysulfonamide nanometer fiber nets by means of airflow-electrostatic combination
CN102703997A (en) * 2012-06-21 2012-10-03 中原工学院 Multi-nozzle closed type jet electrostatic spinning device for preparing nanofibers
CN102851752A (en) * 2012-10-15 2013-01-02 苏州大学 Device and method for preparing layered superfine fiber
CN102864505A (en) * 2012-10-25 2013-01-09 苏州大学 Nano- fiber preparation device and preparation method thereof
CN102137962B (en) * 2008-06-24 2013-05-22 斯泰伦博斯大学 Method and apparatus for the production of fine fibres
CN103147139A (en) * 2013-04-02 2013-06-12 厦门大学 Gas induced electrospinning device
CN103328697A (en) * 2010-12-06 2013-09-25 株式会社托普泰克 Field emission device and nanofiber manufacturing device
CN104532483A (en) * 2015-01-06 2015-04-22 江西先材纳米纤维科技有限公司 Needle-free electrostatic spinning polyimide nanofiber large-scale continuous manufacturing system
CN105274635A (en) * 2015-11-25 2016-01-27 苏州大学 Static bubble spinning device
CN105970313A (en) * 2016-07-25 2016-09-28 青岛中科凯尔科技有限公司 Electrostatic spinning device for preparing nano-fibers on large scale
CN106757420A (en) * 2017-01-20 2017-05-31 东华大学 A kind of spiral goove flute profile electrostatic spinning apparatus and its application method
CN107245776A (en) * 2017-07-19 2017-10-13 东华大学 One kind is applied to industrialization production nano fibre yarn line apparatus and its application method
CN107488879A (en) * 2017-08-10 2017-12-19 东华大学 A kind of high pressure resistant liquid-supplying system of electrostatic spinning
CN113862800A (en) * 2021-11-03 2021-12-31 常州诺金科技有限公司 Electrostatic spinning structure with multiple spray heads

Cited By (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008095239A1 (en) * 2007-02-05 2008-08-14 Commonwealth Scientific And Industrial Research Organisation Nanofibre yarns
US8286413B2 (en) 2007-02-05 2012-10-16 Commonwealth Scientific And Industrial Research Organisation Nanofibre yarns
CN102015121A (en) * 2008-02-29 2011-04-13 斯托拉恩索公司 Method for producing particles electrostatically
CN102137962B (en) * 2008-06-24 2013-05-22 斯泰伦博斯大学 Method and apparatus for the production of fine fibres
CN101812733B (en) * 2009-02-20 2011-05-18 北京化工大学 Continuously-producing high-efficiency melt electrostatic spinning device
CN101871131B (en) * 2009-04-23 2012-05-02 廊坊高山电子科技有限公司 Nanoparticle/polymer material composite ultrafine fiber preparation device
CN101586288B (en) * 2009-07-06 2011-08-31 江苏泰灵生物科技有限公司 Array multi-nozzle electrospinning device
CN103328697B (en) * 2010-12-06 2015-08-19 株式会社托普泰克 Field emission apparatus and nano-fiber manufacturing apparatus
CN103328697A (en) * 2010-12-06 2013-09-25 株式会社托普泰克 Field emission device and nanofiber manufacturing device
CN102312297A (en) * 2011-08-22 2012-01-11 北京化工大学 Wire-brush-type differential fusant electrostatic spinning device and method
CN102312297B (en) * 2011-08-22 2014-01-08 北京化工大学 Wire-brush-type differential fusant electrostatic spinning device and method
CN102493000A (en) * 2011-11-30 2012-06-13 福建农林大学 Low-speed transmission belt type collector for electrostatic spinning equipment
CN102493000B (en) * 2011-11-30 2014-03-26 福建农林大学 Low-speed transmission belt type collector for electrostatic spinning equipment
CN102534822A (en) * 2012-02-18 2012-07-04 上海工程技术大学 Device and method for preparing polysulfonamide nanometer fiber nets by means of airflow-electrostatic combination
CN102534822B (en) * 2012-02-18 2015-07-01 上海工程技术大学 Device and method for preparing polysulfonamide nanometer fiber nets by means of airflow-electrostatic combination
CN102703997A (en) * 2012-06-21 2012-10-03 中原工学院 Multi-nozzle closed type jet electrostatic spinning device for preparing nanofibers
CN102851752A (en) * 2012-10-15 2013-01-02 苏州大学 Device and method for preparing layered superfine fiber
CN102851752B (en) * 2012-10-15 2015-08-19 苏州大学 hierarchical structure superfine fibre preparation method and device
CN102864505A (en) * 2012-10-25 2013-01-09 苏州大学 Nano- fiber preparation device and preparation method thereof
CN103147139A (en) * 2013-04-02 2013-06-12 厦门大学 Gas induced electrospinning device
CN103147139B (en) * 2013-04-02 2015-12-23 厦门大学 A kind of gas induced electric spinning equipment
CN104532483A (en) * 2015-01-06 2015-04-22 江西先材纳米纤维科技有限公司 Needle-free electrostatic spinning polyimide nanofiber large-scale continuous manufacturing system
CN105274635A (en) * 2015-11-25 2016-01-27 苏州大学 Static bubble spinning device
CN105970313A (en) * 2016-07-25 2016-09-28 青岛中科凯尔科技有限公司 Electrostatic spinning device for preparing nano-fibers on large scale
CN106757420A (en) * 2017-01-20 2017-05-31 东华大学 A kind of spiral goove flute profile electrostatic spinning apparatus and its application method
CN106757420B (en) * 2017-01-20 2018-10-23 东华大学 A kind of spiral goove flute profile electrostatic spinning apparatus and its application method
CN107245776A (en) * 2017-07-19 2017-10-13 东华大学 One kind is applied to industrialization production nano fibre yarn line apparatus and its application method
CN107245776B (en) * 2017-07-19 2019-11-08 东华大学 One kind being suitable for industrialization production nano fibre yarn line apparatus and its application method
CN107488879A (en) * 2017-08-10 2017-12-19 东华大学 A kind of high pressure resistant liquid-supplying system of electrostatic spinning
CN113862800A (en) * 2021-11-03 2021-12-31 常州诺金科技有限公司 Electrostatic spinning structure with multiple spray heads

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