CN100545624C - Smelting method for preparing borate glass base hole reservoir model - Google Patents
Smelting method for preparing borate glass base hole reservoir model Download PDFInfo
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- CN100545624C CN100545624C CNB2007100528737A CN200710052873A CN100545624C CN 100545624 C CN100545624 C CN 100545624C CN B2007100528737 A CNB2007100528737 A CN B2007100528737A CN 200710052873 A CN200710052873 A CN 200710052873A CN 100545624 C CN100545624 C CN 100545624C
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- galenite
- borate glass
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- velocity
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Abstract
The invention provides smelting method for preparing borate glass base hole reservoir model.This preparation method is that matrix, the natural galenite that hangs down velocity of wave are hole simulation snotter with the borate glass of high velocity of wave, galenite is processed into micron-sized particle, first melting borate glass in the high temperature muffle furnace is mixed in micron order galenite particle in the borate glass matrix when the glass ware forming and makes.The borate glass base hole reservoir model of the present invention's preparation, matrix ultrasonic velocity height, hole simulation snotter velocity of wave is low, matrix and hole velocity of wave coupling are better, moulded dimension is less, and realistic geological condition helps improving exploration success ratios such as reservoir, hydrocarbon-bearing pool.
Description
Technical field
The present invention relates to be used for geological research, especially simulate the preparation method of the cranny and cave reservoir physical model of oil gas reservoir matter condition.
Background technology
Hole be in the important space that oil gas preserves, migrates, the especially carbonate reservoir a large amount of holes of growing, solution cavity etc. more oil gas preserve the space condition that provides important.The research bore hole system is to the response of seismic event feature, analyze the relation between hole distribution and growth intensity and the seismic event characteristic attribute parameter, and then the feature of utilizing seismic event understands, is familiar with the distribution and the development degree of bore hole system in the subsurface reservoir, become more and more important research project of geophysicist.The ultrasound wave experiment of physical model by observation and the analysis to artificial physical model, can provide experimental basis as geophysical important research means for the underground opening systematic research.
Ultrasound wave research physical model principle is the rock under the simulation geologic condition and the hole of the inside, model-based n-body simulation n rocky condition normally, and the hole in hole wherein or the doping granule simulation rock.At present generally adopt the low macromolecular material of velocity of wave as matrix both at home and abroad, and select unmatched metal of velocity of wave or air, and physical size is bigger as the hole snotter.According to similarity criterion, the size of model is more little, and the actual geology size of embodiment is big more.Therefore the physical model that exists at present can not accurately reflect the actual conditions of geology, causes the data out of true, and error is bigger.The present invention is that matrix, galenite are the physical model of hole simulation snotter with the borate glass, and the velocity of wave coupling of matrix and snotter is better, and moulded dimension is less, realistic geological condition.
Do not see with the borate glass at present to be that matrix, galenite are patent and the bibliographical information that hole simulation snotter prepares the cranny and cave reservoir physical model.
Summary of the invention
The purpose of this invention is to provide a kind of preparation method of being convenient to explore the cranny and cave reservoir physical model of reservoir and hydrocarbon-bearing pool, i.e. smelting method for preparing borate glass base hole reservoir model.
Technical scheme of the present invention is:
The preparation method of borate glass base hole reservoir model is characterized in that smelting process, and this method is that matrix, the natural galenite that hangs down velocity of wave are hole simulation snotter with the borate glass of high velocity of wave, and galenite is processed into micron-sized particle.First melting borate glass in the high temperature muffle furnace is mixed in micron order galenite particle in the borate glass matrix when the glass ware forming again, makes borate glass base hole reservoir model.
The preparation method of borate glass base hole reservoir model of the present invention, undertaken by following step:
1. galenite ore reduction, grinding, screening are obtained a series of micron order galenite particles, select the galenite particle of 15 μ m, 30 μ m, 50 μ m, 100 μ m, 150 μ m for use;
2. the crucible that is heated to 1100 ℃ is in advance put in borate glass batch (seeing Table 1) gradation; continuation was warming up to 1200 ℃ of constant temperature 2 hours in muffle furnace; being cooled to 950 ℃ comes out of the stove; cast molding; used grinding tool is at 400 ℃ of constant temperature; to guarantee that glass does not burst, in cast molding, desired particle size galenite particle is mixed in the glass melt.Galenite particle addition is relevant with grain size, is respectively 15 μ m, 10; 30 μ m, 30; 50 μ m, 50; 100 μ m, 70; 150 μ m, 100;
3. after treating that glass ware forming solidifies, the glass-based model that will contain the definite shape of galenite particle places annealing furnace, by 0.5 ℃ of/minute clock rate annealing, takes out to room temperature;
4. the gained sample is carried out sharp processing, the polishing get final product.
The proportioning of table 1 borate glass batch
Relatively
Three oxygen
Actual
Divide
Change two
The raw material name
Molal quantity is theoretical with the pure actual quality of using of raw material
Son
Boron
Claim
(mol) amount (g) tolerance (g) percentage
Amount
Quality
Ratio
Percentage
Ratio
B
2O
3 70 3.062 214.331 98％ 218.705 0.410 1.000
Na
2B
4O
7?202 1.079 217.880 97％ 224.619 0.421 1.027
Na
2CO
3 106 0.574 60.854 99.80％ 60.976 0.114 0.278
KNO
3 101 0.195 19.678 99.70％ 19.737 0.037 0.090
Mg(OH)
2?58 0.139 8.072 98.00％ 8.237 0.015 0.037
NaF 42 0.035 1.461 99.40％ 1.470 0.003 0.007
Technical characterstic of the present invention
1. the borate glass with melting is a matrix, is that hole simulation snotter prepares the cranny and cave reservoir physical model with the galenite particle.
2. matrix ultrasonic velocity height, hole simulation snotter velocity of wave is low, and matrix is better with hole velocity of wave coupling, realistic geological condition.
Embodiment
The galenite ore is ground, sieves a series of micron order galenite particles of acquisition through crusher in crushing, mortar, and the galenite particle of choosing 15 μ m, 30 μ m, 50 μ m, 100 μ m, 150 μ m is standby;
Embodiment 1
The preparation of borate glass base hole reservoir model
The crucible that is heated to 1100 ℃ is in advance put in the gradation of borate glass batch, continuation was warming up to 1200 ℃ of constant temperature 2 hours in muffle furnace, being cooled to 950 ℃ comes out of the stove, cast molding, used grinding tool is at 400 ℃ of constant temperature, to guarantee that glass does not burst, in cast molding, be that the galenite particle of 15 μ m is mixed in the glass melt with 10 granularities; After treating that glass ware forming solidifies, the glass-based model that will contain the galenite particle places annealing furnace, by 0.5 ℃ of/minute clock rate annealing, takes out to room temperature; The gained sample is carried out sharp processing, polishing, promptly make borate glass base hole reservoir model.
Embodiment 2
The preparation of borate glass base hole reservoir model
The crucible that is heated to 1100 ℃ is in advance put in the gradation of borate glass batch, continuation was warming up to 1200 ℃ of constant temperature 2 hours in muffle furnace, being cooled to 950 ℃ comes out of the stove, cast molding, used grinding tool is at 400 ℃ of constant temperature, in cast molding, be that the galenite particle of 150 μ m is mixed in the glass melt with 100 granularities; After treating that glass ware forming solidifies, the glass-based model that will contain the galenite particle places annealing furnace, by 0.5 ℃ of/minute clock rate annealing, takes out to room temperature; The gained sample is carried out sharp processing, polishing, promptly make borate glass base hole reservoir model.
Embodiment 3,4,5
The preparation of borate glass base hole reservoir model
Its method of operating and process conditions are substantially the same manner as Example 1, and the galenite grain graininess that just is mixed in the glass melt is respectively 30 μ m, 30; 50 μ m, 50; 100 μ m, 70.
Claims (1)
1, the preparation method of borate glass base hole reservoir model is characterized in that, smelting process is undertaken by following step:
1), be a series of micron order galenite particles with galenite ore reduction, grinding, screening, select a kind of galenite particle among 15 μ m, 30 μ m, 50 μ m, 100 μ m or the 150 μ m for use;
2), the crucible that is heated to 1100 ℃ is in advance put in the gradation of borate glass batch, continuation was warming up to 1200 ℃ of constant temperature 2 hours in muffle furnace, being cooled to 950 ℃ comes out of the stove, cast molding, used grinding tool is at 400 ℃ of constant temperature, in cast molding, the galenite particle is mixed in the glass melt, galenite particle addition is relevant with grain size, is respectively 15 μ m, 10; 30 μ m, 30; 50 μ m, 50; 100 μ m, 70; 150 μ m, 100;
3), treat that glass ware forming solidifies after, the glass-based model that will contain the galenite particle places annealing furnace, by 0.5 ℃ of/minute clock rate annealing, takes out to room temperature;
4), step 3) gained sample is carried out sharp processing, the polishing get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100528737A CN100545624C (en) | 2007-07-31 | 2007-07-31 | Smelting method for preparing borate glass base hole reservoir model |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2007100528737A CN100545624C (en) | 2007-07-31 | 2007-07-31 | Smelting method for preparing borate glass base hole reservoir model |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101101246A CN101101246A (en) | 2008-01-09 |
| CN100545624C true CN100545624C (en) | 2009-09-30 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2007100528737A Expired - Fee Related CN100545624C (en) | 2007-07-31 | 2007-07-31 | Smelting method for preparing borate glass base hole reservoir model |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102053026B (en) * | 2009-10-30 | 2014-07-02 | 中国石油化工股份有限公司 | Material and method for manufacturing carbonate cave oil reservoir physical model |
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2007
- 2007-07-31 CN CNB2007100528737A patent/CN100545624C/en not_active Expired - Fee Related
Non-Patent Citations (2)
| Title |
|---|
| 石油产品和添加剂机械杂质测定法（重量法）. 中国石化销售公司华北分公司石油商品应用技术研究所.中华人民共和国国家标准 GB/T511-88. 1988 |
| 石油产品和添加剂机械杂质测定法(重量法). 中国石化销售公司华北分公司石油商品应用技术研究所.中华人民共和国国家标准 GB/T511-88. 1988 * |
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Granted publication date: 20090930 Termination date: 20110731 |