CH307561A - Verfahren zur Herstellung einer Diammoniumverbindung. - Google Patents

Verfahren zur Herstellung einer Diammoniumverbindung.

Info

Publication number
CH307561A
CH307561A CH307561DA CH307561A CH 307561 A CH307561 A CH 307561A CH 307561D A CH307561D A CH 307561DA CH 307561 A CH307561 A CH 307561A
Authority
CH
Switzerland
Prior art keywords
preparation
diammonium compound
ethoxy
bis
diammonium
Prior art date
Application number
Other languages
English (en)
Inventor
Ag J R Geigy
Original Assignee
Ag J R Geigy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ag J R Geigy filed Critical Ag J R Geigy
Publication of CH307561A publication Critical patent/CH307561A/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
    • C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
    • C07D295/08—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms
    • C07D295/084—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
    • C07D295/088—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D211/00—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings
    • C07D211/04—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D211/06—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members
    • C07D211/08—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members with hydrocarbon or substituted hydrocarbon radicals directly attached to ring carbon atoms
    • C07D211/10—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members with hydrocarbon or substituted hydrocarbon radicals directly attached to ring carbon atoms with radicals containing only carbon and hydrogen atoms attached to ring carbon atoms
    • C07D211/14—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members with hydrocarbon or substituted hydrocarbon radicals directly attached to ring carbon atoms with radicals containing only carbon and hydrogen atoms attached to ring carbon atoms with hydrocarbon or substituted hydrocarbon radicals attached to the ring nitrogen atom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Hydrogenated Pyridines (AREA)

Description


      Verfahren        zur        Herstellung   <B>einer</B>     Diammoniumverbinau        g.       Gegenstand des vorliegenden Patentes ist  ein Verfahren zur Herstellung einer     Diammo-          niumverbindung.    Das Verfahren ist dadurch  gekennzeichnet, dass man auf 1     Mol        1,10-Bis-          (ss-4'-methyl-piperidino-äthoxy)-dekan    2     Mol          Benzylbromid    einwirken lässt.  



  Die erhaltene neue Verbindung, das     1,10-          Bis-    [     ss-        (benzyl    - 4'     -methyl    -     piperidinium)    -     äth-          oxy]-dekan-dibromid,        schmilzt    bei 150-151.  Sie soll als Arzneimittel und als Zwischen  produkt für Arzneimittel Verwendung finden.

           Beispiel:       4,24 Teile     1.,10-Bis-(ss-4'-methyl-piperidino)-          äthoxy-dekan    und 4,1 Teile     Benzylbromid     werden in 20 Teilen     Butanon    etwa 14 Stunden  unter     Rüekfluss    gekocht. Nach Kühlen wird    das abgeschiedene rohe     quartäre    Salz abge  trennt und aus     Butanon    unter Zugabe von  wenig     Isopropanol    oder Methanol umkristal  lisiert. Hierauf trocknet man bei 50-60  im  Hochvakuum.

   Das     1,10-Bis-[ss-(benzyl-4'-me-          thyl-piperidinium)        -äthoxy]        -dekan-dibromid     schmilzt bei 150-151 .

Claims (1)

  1. PATENTANSPRUCH: Verfahren zur Herstellung einer Diammo- niumverbindung, dadurch gekennzeichnet, dass man auf 1 Mol 1,10-Bis-(ss-4'-inethyl-piperi- dino-äthoxy)-dekan 2 lfol Benzylbromid ein wirken lässt. Die erhaltene neue Verbindung, das 1,10- Bis- [ss- (benzyl -4' -methyl -piperidinium) - äth- oxy]-dekan-dibromid, schmilzt bei 150-151 .
CH307561D 1952-04-21 1952-04-21 Verfahren zur Herstellung einer Diammoniumverbindung. CH307561A (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH305890T 1952-04-21
CH307561T 1952-04-21

Publications (1)

Publication Number Publication Date
CH307561A true CH307561A (de) 1955-05-31

Family

ID=25735026

Family Applications (1)

Application Number Title Priority Date Filing Date
CH307561D CH307561A (de) 1952-04-21 1952-04-21 Verfahren zur Herstellung einer Diammoniumverbindung.

Country Status (1)

Country Link
CH (1) CH307561A (de)

Similar Documents

Publication Publication Date Title
CH307561A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH307556A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH307562A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH307558A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH307554A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH307559A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH307557A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH307564A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH306915A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH307551A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH307560A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH306914A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH306913A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH307563A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH307555A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH306919A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH306922A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH306916A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH306912A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH306917A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH306920A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH306923A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH306911A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH307565A (de) Verfahren zur Herstellung einer Diammoniumverbindung.
CH306924A (de) Verfahren zur Herstellung einer Diammoniumverbindung.