CH136243A - Process for the preparation of an arylaminonaphthalene derivative. - Google Patents

Process for the preparation of an arylaminonaphthalene derivative.

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Publication number
CH136243A
CH136243A CH136243DA CH136243A CH 136243 A CH136243 A CH 136243A CH 136243D A CH136243D A CH 136243DA CH 136243 A CH136243 A CH 136243A
Authority
CH
Switzerland
Prior art keywords
preparation
derivative
arylaminonaphthalene
amino
diaminonaphthalene
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellsc Farbenindustrie
Original Assignee
Ig Farbenindustrie Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ig Farbenindustrie Ag filed Critical Ig Farbenindustrie Ag
Publication of CH136243A publication Critical patent/CH136243A/en

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  Verfahren zur Darstellung eines     Arylaminonaphtalinderivates.       Analog dem im Hauptpatent beschriebenen  Verfahren kann man     1.5-Di-(4'-oxyphenyl-          amino)-naphtalin    darstellen, wenn man 1.5  Diaminonaphtalin und     4-Amino-l-oxybenzol     mit     Bisulfitlauge    im     offenen    oder im Druck  gefäss durch Erhitzen kondensiert.  



  <I>Beispiel:</I>  <B>158</B> Teile     1.5-Diaminonaphtalin    werden  in einem verbleiten     Rührkessel    mit einer  Lösung von 400 Teilen     Alkalibisulfit    in 3000  Teilen Wasser und 260 Teilen     4-Amino-l-          ogybenzol    unter Druck und Rühren etwa  36 Stunden auf 115-120   C erhitzt. Die  Aufarbeitung erfolgt wie im Beispiel des  Zusatzpatentes Nr.     135646    beschrieben. Das  Endprodukt ist identisch mit dem dort er  haltenen.



  Process for the preparation of an arylaminonaphthalene derivative. 1.5-Di- (4'-oxyphenyl-amino) -naphthalene can be prepared analogously to the process described in the main patent if 1.5-diaminonaphthalene and 4-amino-1-oxybenzene are condensed with bisulfite lye in an open or in a pressure vessel by heating.



  <I> Example: </I> <B> 158 </B> parts of 1,5-diaminonaphthalene are in a leaded stirred tank with a solution of 400 parts of alkali bisulfite in 3000 parts of water and 260 parts of 4-amino-l-ogybenzene under pressure and Stirring heated to 115-120 ° C. for about 36 hours. Working up is carried out as described in the example of additional patent no. 135646. The end product is identical to the one received there.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Darstellung eines Aryl- aminonaphtalinderivates, dadurch gekenn zeichnet, dass man 1.5-Diaminonaphtalin und 4-Amino-l-oxybenzol in Gegenwart von Bi- sulfitlauge auf höhere Temperatur erwärmt. UNTERANSPRUCH: Verfahren nach Patentanspruch, dadurch gekennzeichnet, dass man die Umsetzung unter Druck im geschlossenen Gefäss vor nimmt. Claim: Process for the preparation of an aryl aminonaphthalene derivative, characterized in that 1,5-diaminonaphthalene and 4-amino-1-oxybenzene are heated to a higher temperature in the presence of bisulfite lye. SUBCLAIM: Method according to claim, characterized in that the reaction is carried out under pressure in a closed vessel.
CH136243D 1926-12-13 1927-12-03 Process for the preparation of an arylaminonaphthalene derivative. CH136243A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE136243X 1926-12-13
CH132030T 1927-12-03

Publications (1)

Publication Number Publication Date
CH136243A true CH136243A (en) 1929-10-31

Family

ID=25711770

Family Applications (1)

Application Number Title Priority Date Filing Date
CH136243D CH136243A (en) 1926-12-13 1927-12-03 Process for the preparation of an arylaminonaphthalene derivative.

Country Status (1)

Country Link
CH (1) CH136243A (en)

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