CA2957141C - Recuperation de l'helium de flux riches en azote - Google Patents

Recuperation de l'helium de flux riches en azote Download PDF

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Publication number
CA2957141C
CA2957141C CA2957141A CA2957141A CA2957141C CA 2957141 C CA2957141 C CA 2957141C CA 2957141 A CA2957141 A CA 2957141A CA 2957141 A CA2957141 A CA 2957141A CA 2957141 C CA2957141 C CA 2957141C
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Canada
Prior art keywords
nitrogen
enriched
gas
produce
pressure
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Expired - Fee Related
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CA2957141A
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CA2957141A1 (fr
Inventor
Vincent White
Paul Higginbotham
John Eugene Palamara
Alan Berger
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Air Products and Chemicals Inc
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Air Products and Chemicals Inc
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Publication of CA2957141A1 publication Critical patent/CA2957141A1/fr
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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/028Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of noble gases
    • F25J3/029Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of noble gases of helium
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
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    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0204Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the feed stream
    • F25J3/0209Natural gas or substitute natural gas
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    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0233Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of CnHm with 1 carbon atom or more
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    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
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    • F25J3/0228Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
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    • F25J2200/10Processes or apparatus using separation by rectification in a quadruple, or more, column or pressure system
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    • F25J2200/70Refluxing the column with a condensed part of the feed stream, i.e. fractionator top is stripped or self-rectified
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    • F25J2260/42Integration in an installation using nitrogen, e.g. as utility gas, for inerting or purging purposes in IGCC, POX, GTL, PSA, float glass forming, incineration processes, for heat recovery or for enhanced oil recovery
    • F25J2260/44Integration in an installation using nitrogen, e.g. as utility gas, for inerting or purging purposes in IGCC, POX, GTL, PSA, float glass forming, incineration processes, for heat recovery or for enhanced oil recovery using nitrogen for cooling purposes
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    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/34Details about subcooling of liquids

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  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Separation By Low-Temperature Treatments (AREA)

Abstract

La consommation dénergie globale dans un procédé de distillation cryogénique pour récupérer de lhélium à partir de gaz riches en azote comprenant de lhélium peut être réduite si lalimentation du système de colonne de distillation est au moins sensiblement condensée par échange de chaleur indirect contre un premier liquide de fond à une première pression, et un second liquide de fond à une seconde pression qui est différente de la première pression.
CA2957141A 2016-02-11 2017-02-06 Recuperation de l'helium de flux riches en azote Expired - Fee Related CA2957141C (fr)

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US15/041,305 US20170234611A1 (en) 2016-02-11 2016-02-11 Recovery Of Helium From Nitrogen-Rich Streams
US15/041,305 2016-02-11

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CN107875664B (zh) * 2017-12-21 2023-09-26 新疆工程学院 丙烯-丙烷热耦合精馏节能装置
WO2021028068A1 (fr) * 2019-08-13 2021-02-18 Linde Gmbh Procédé et installation pour traiter un mélange gazeux contenant de l'azote et du méthane
CN111981767B (zh) * 2020-08-20 2024-03-08 中国石油工程建设有限公司 一种天然气单塔深冷提氦装置和方法
CN114646187B (zh) * 2021-09-15 2023-08-29 中国石油天然气股份有限公司西南油气田分公司成都天然气化工总厂 一种适用于低含氦天然气的三塔低温提氦系统
CN114413570B (zh) * 2022-01-19 2023-01-31 四川空分设备(集团)有限责任公司 一种双塔落地式制氮装置

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US5017204A (en) * 1990-01-25 1991-05-21 Air Products And Chemicals, Inc. Dephlegmator process for the recovery of helium
US5041149A (en) * 1990-10-18 1991-08-20 Union Carbide Industrial Gases Technology Corporation Separation of nitrogen and methane with residue turboexpansion
US5167125A (en) * 1991-04-08 1992-12-01 Air Products And Chemicals, Inc. Recovery of dissolved light gases from a liquid stream
DE102005010054A1 (de) * 2005-03-04 2006-09-07 Linde Ag Verfahren zum gleichzeitigen Gewinnen einer Helium- und einer Stickstoff-Reinfraktion
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US9791210B2 (en) * 2012-08-02 2017-10-17 Air Products And Chemicals, Inc. Systems and methods for recovering helium from feed streams containing carbon dioxide

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EP3205964A2 (fr) 2017-08-16
EP3205964A3 (fr) 2017-12-13
AP2017009740A0 (en) 2017-02-28
US20190041128A1 (en) 2019-02-07
US20170234611A1 (en) 2017-08-17
CA2957141A1 (fr) 2017-08-11

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