CA2860031C - Recuperation d'elements organiques et nutritifs a partir de residus de digesteur anaerobie - Google Patents
Recuperation d'elements organiques et nutritifs a partir de residus de digesteur anaerobie Download PDFInfo
- Publication number
- CA2860031C CA2860031C CA2860031A CA2860031A CA2860031C CA 2860031 C CA2860031 C CA 2860031C CA 2860031 A CA2860031 A CA 2860031A CA 2860031 A CA2860031 A CA 2860031A CA 2860031 C CA2860031 C CA 2860031C
- Authority
- CA
- Canada
- Prior art keywords
- liquid
- stages
- ammonia
- digestate
- air
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000011084 recovery Methods 0.000 title description 30
- 235000015097 nutrients Nutrition 0.000 title description 25
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 303
- 239000007788 liquid Substances 0.000 claims abstract description 166
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 135
- 238000000034 method Methods 0.000 claims abstract description 98
- 239000007787 solid Substances 0.000 claims abstract description 95
- 230000008569 process Effects 0.000 claims abstract description 84
- 239000010802 sludge Substances 0.000 claims abstract description 48
- 239000003570 air Substances 0.000 claims description 75
- 239000007789 gas Substances 0.000 claims description 35
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 31
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 24
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 22
- 235000011130 ammonium sulphate Nutrition 0.000 claims description 22
- 238000001035 drying Methods 0.000 claims description 22
- 230000029087 digestion Effects 0.000 claims description 21
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 18
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 14
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 13
- 239000010815 organic waste Substances 0.000 claims description 13
- 239000001569 carbon dioxide Substances 0.000 claims description 11
- 239000000908 ammonium hydroxide Substances 0.000 claims description 10
- 239000000126 substance Substances 0.000 claims description 7
- 230000005484 gravity Effects 0.000 claims description 4
- 238000010408 sweeping Methods 0.000 claims description 3
- 239000012080 ambient air Substances 0.000 claims description 2
- 230000005855 radiation Effects 0.000 claims description 2
- 238000007664 blowing Methods 0.000 claims 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 86
- 239000008188 pellet Substances 0.000 abstract description 48
- 229910052757 nitrogen Inorganic materials 0.000 abstract description 45
- 239000003337 fertilizer Substances 0.000 abstract description 33
- 150000003863 ammonium salts Chemical class 0.000 abstract description 27
- 239000000243 solution Substances 0.000 abstract description 22
- 239000012266 salt solution Substances 0.000 abstract description 21
- 239000000835 fiber Substances 0.000 abstract description 13
- 230000002378 acidificating effect Effects 0.000 abstract description 6
- 235000021049 nutrient content Nutrition 0.000 abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 55
- 235000012970 cakes Nutrition 0.000 description 42
- 239000000047 product Substances 0.000 description 26
- 239000002699 waste material Substances 0.000 description 25
- 210000003608 fece Anatomy 0.000 description 20
- 239000010871 livestock manure Substances 0.000 description 20
- 239000002253 acid Substances 0.000 description 19
- 239000000706 filtrate Substances 0.000 description 16
- 241000196324 Embryophyta Species 0.000 description 15
- 239000008187 granular material Substances 0.000 description 15
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 14
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 13
- 238000005276 aerator Methods 0.000 description 11
- 229910052700 potassium Inorganic materials 0.000 description 10
- 239000002918 waste heat Substances 0.000 description 10
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 9
- 235000011114 ammonium hydroxide Nutrition 0.000 description 9
- 239000002361 compost Substances 0.000 description 9
- 230000001965 increasing effect Effects 0.000 description 9
- 239000011591 potassium Substances 0.000 description 9
- 238000010790 dilution Methods 0.000 description 8
- 239000012895 dilution Substances 0.000 description 8
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 8
- 238000003860 storage Methods 0.000 description 8
- 238000001704 evaporation Methods 0.000 description 7
- 230000008020 evaporation Effects 0.000 description 7
- 238000000926 separation method Methods 0.000 description 7
- 239000002002 slurry Substances 0.000 description 7
- 239000000758 substrate Substances 0.000 description 6
- 238000004065 wastewater treatment Methods 0.000 description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 5
- 241001465754 Metazoa Species 0.000 description 5
- 229910052799 carbon Inorganic materials 0.000 description 5
- 239000003518 caustics Substances 0.000 description 5
- 239000000701 coagulant Substances 0.000 description 5
- 239000000446 fuel Substances 0.000 description 5
- 125000001477 organic nitrogen group Chemical group 0.000 description 5
- 125000005461 organic phosphorous group Chemical group 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- 230000000717 retained effect Effects 0.000 description 5
- 150000003839 salts Chemical class 0.000 description 5
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
- 239000003929 acidic solution Substances 0.000 description 4
- 239000001099 ammonium carbonate Substances 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 229910052698 phosphorus Inorganic materials 0.000 description 4
- 229920000642 polymer Polymers 0.000 description 4
- 241001148471 unidentified anaerobic bacterium Species 0.000 description 4
- 229910000013 Ammonium bicarbonate Inorganic materials 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 3
- 239000002028 Biomass Substances 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- -1 ammonia ions Chemical class 0.000 description 3
- 235000012538 ammonium bicarbonate Nutrition 0.000 description 3
- 230000033228 biological regulation Effects 0.000 description 3
- 238000002485 combustion reaction Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 239000000428 dust Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 230000014759 maintenance of location Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000010841 municipal wastewater Substances 0.000 description 3
- 229910000069 nitrogen hydride Inorganic materials 0.000 description 3
- 244000052769 pathogen Species 0.000 description 3
- 238000005453 pelletization Methods 0.000 description 3
- 239000002689 soil Substances 0.000 description 3
- 241000287828 Gallus gallus Species 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- 238000005273 aeration Methods 0.000 description 2
- 230000001580 bacterial effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000003139 buffering effect Effects 0.000 description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 description 2
- 235000010216 calcium carbonate Nutrition 0.000 description 2
- 238000004364 calculation method Methods 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000009264 composting Methods 0.000 description 2
- 230000001143 conditioned effect Effects 0.000 description 2
- 230000003750 conditioning effect Effects 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 238000006073 displacement reaction Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000013067 intermediate product Substances 0.000 description 2
- 239000012528 membrane Substances 0.000 description 2
- 235000019645 odor Nutrition 0.000 description 2
- 150000002894 organic compounds Chemical class 0.000 description 2
- 239000005416 organic matter Substances 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- 244000144977 poultry Species 0.000 description 2
- 230000003134 recirculating effect Effects 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- 230000000153 supplemental effect Effects 0.000 description 2
- 231100000331 toxic Toxicity 0.000 description 2
- 230000002588 toxic effect Effects 0.000 description 2
- QGZKDVFQNNGYKY-OUBTZVSYSA-N Ammonia-15N Chemical compound [15NH3] QGZKDVFQNNGYKY-OUBTZVSYSA-N 0.000 description 1
- USFZMSVCRYTOJT-UHFFFAOYSA-N Ammonium acetate Chemical compound N.CC(O)=O USFZMSVCRYTOJT-UHFFFAOYSA-N 0.000 description 1
- 239000005695 Ammonium acetate Substances 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 1
- 229920000388 Polyphosphate Polymers 0.000 description 1
- 241000282849 Ruminantia Species 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000002154 agricultural waste Substances 0.000 description 1
- 229940037003 alum Drugs 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 229940043376 ammonium acetate Drugs 0.000 description 1
- 235000019257 ammonium acetate Nutrition 0.000 description 1
- 235000012501 ammonium carbonate Nutrition 0.000 description 1
- 230000003190 augmentative effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000002551 biofuel Substances 0.000 description 1
- 230000033558 biomineral tissue development Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000000567 combustion gas Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000001599 direct drying Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 235000021463 dry cake Nutrition 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000002657 fibrous material Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000007701 flash-distillation Methods 0.000 description 1
- 239000008394 flocculating agent Substances 0.000 description 1
- 238000005188 flotation Methods 0.000 description 1
- 230000009969 flowable effect Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000010794 food waste Substances 0.000 description 1
- 230000002538 fungal effect Effects 0.000 description 1
- 210000001035 gastrointestinal tract Anatomy 0.000 description 1
- 239000005431 greenhouse gas Substances 0.000 description 1
- 230000020169 heat generation Effects 0.000 description 1
- 239000008236 heating water Substances 0.000 description 1
- 238000003898 horticulture Methods 0.000 description 1
- 230000001976 improved effect Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000009267 in-vessel composting Methods 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 229910003480 inorganic solid Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 description 1
- 230000000696 methanogenic effect Effects 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- 239000003895 organic fertilizer Substances 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000020477 pH reduction Effects 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000002846 particulate organic matter Substances 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 239000001205 polyphosphate Substances 0.000 description 1
- 235000011176 polyphosphates Nutrition 0.000 description 1
- 238000010248 power generation Methods 0.000 description 1
- 238000007781 pre-processing Methods 0.000 description 1
- 239000010909 process residue Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- YWYZEGXAUVWDED-UHFFFAOYSA-N triammonium citrate Chemical compound [NH4+].[NH4+].[NH4+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O YWYZEGXAUVWDED-UHFFFAOYSA-N 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
- 239000012855 volatile organic compound Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
- 238000009269 windrow composting Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W10/00—Technologies for wastewater treatment
- Y02W10/10—Biological treatment of water, waste water, or sewage
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
Landscapes
- Fertilizers (AREA)
- Treatment Of Sludge (AREA)
Abstract
L'invention concerne le traitement de la boue d'un digesteur anaérobie pour récupérer une ou plusieurs fibres, ou solides ou liquides ayant une teneur élevée en éléments nutritifs. Les solides ou les liquides peuvent être utilisés en tant qu'engrais. Les fibres peuvent être utilisées dans un milieu de culture de plantes. Les solides sont séparés des liquides dans la boue et séchés. Les solides peuvent être séchés pour produire des paillettes ou des pastilles. L'ammoniac dans les liquides est récupéré et utilisé pour produire une solution concentrée de sel d'ammonium acide. Cette solution peut être mélangée avec les solides pour produire un solide enrichi en azote. Les fibres et solides ou liquides peuvent aussi être utilisés en combinaison pour produire un milieu de culture de plantes amélioré. Un dispositif et un procédé pour éliminer l'ammoniac d'un liquide peuvent être utilisés dans le système ou séparément.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA2860031A CA2860031C (fr) | 2011-12-21 | 2012-12-18 | Recuperation d'elements organiques et nutritifs a partir de residus de digesteur anaerobie |
Applications Claiming Priority (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161578703P | 2011-12-21 | 2011-12-21 | |
| US61/578,703 | 2011-12-21 | ||
| CAPCT/CA2012/000144 | 2012-02-17 | ||
| PCT/CA2012/000144 WO2012109737A1 (fr) | 2011-02-17 | 2012-02-17 | Récupération de matières organiques et de nutriments des résidus d'un digesteur anaérobie |
| US201261707467P | 2012-09-28 | 2012-09-28 | |
| US61/707,467 | 2012-09-28 | ||
| CA2860031A CA2860031C (fr) | 2011-12-21 | 2012-12-18 | Recuperation d'elements organiques et nutritifs a partir de residus de digesteur anaerobie |
| PCT/CA2012/050907 WO2013091094A1 (fr) | 2011-12-21 | 2012-12-18 | Récupération d'éléments organiques et nutritifs à partir de résidus de digesteur anaérobie |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2860031A1 CA2860031A1 (fr) | 2013-06-27 |
| CA2860031C true CA2860031C (fr) | 2021-11-16 |
Family
ID=51422245
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2860031A Active CA2860031C (fr) | 2011-12-21 | 2012-12-18 | Recuperation d'elements organiques et nutritifs a partir de residus de digesteur anaerobie |
Country Status (1)
| Country | Link |
|---|---|
| CA (1) | CA2860031C (fr) |
-
2012
- 2012-12-18 CA CA2860031A patent/CA2860031C/fr active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CA2860031A1 (fr) | 2013-06-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request |
Effective date: 20171218 |