CA2665966A1 - Lubricating coating composition suitable for tubular threaded joints - Google Patents

Lubricating coating composition suitable for tubular threaded joints Download PDF

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Publication number
CA2665966A1
CA2665966A1 CA002665966A CA2665966A CA2665966A1 CA 2665966 A1 CA2665966 A1 CA 2665966A1 CA 002665966 A CA002665966 A CA 002665966A CA 2665966 A CA2665966 A CA 2665966A CA 2665966 A1 CA2665966 A1 CA 2665966A1
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CA
Canada
Prior art keywords
basic
set forth
coating composition
lubricating coating
salt
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA002665966A
Other languages
French (fr)
Other versions
CA2665966C (en
Inventor
Ryuichi Imai
Kunio Goto
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Vallourec Oil and Gas France SAS
Nippon Steel Corp
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2665966A1 publication Critical patent/CA2665966A1/en
Application granted granted Critical
Publication of CA2665966C publication Critical patent/CA2665966C/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04Mixtures of base-materials and additives
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16LPIPES; JOINTS OR FITTINGS FOR PIPES; SUPPORTS FOR PIPES, CABLES OR PROTECTIVE TUBING; MEANS FOR THERMAL INSULATION IN GENERAL
    • F16L15/00Screw-threaded joints; Forms of screw-threads for such joints
    • F16L15/04Screw-threaded joints; Forms of screw-threads for such joints with additional sealings
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/022Ethene
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/14Synthetic waxes, e.g. polythene waxes
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/16Paraffin waxes; Petrolatum, e.g. slack wax
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/17Fisher Tropsch reaction products
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/18Natural waxes, e.g. ceresin, ozocerite, bees wax, carnauba; Degras
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02Hydroxy compounds
    • C10M2207/023Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/0235Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings used as base material
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02Hydroxy compounds
    • C10M2207/023Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/028Overbased salts thereof
    • C10M2207/0285Overbased salts thereof used as base material
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10Carboxylix acids; Neutral salts thereof
    • C10M2207/12Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/1253Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids used as base material
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10Carboxylix acids; Neutral salts thereof
    • C10M2207/12Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/126Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/26Overbased carboxylic acid salts
    • C10M2207/262Overbased carboxylic acid salts derived from hydroxy substituted aromatic acids, e.g. salicylates
    • C10M2207/2623Overbased carboxylic acid salts derived from hydroxy substituted aromatic acids, e.g. salicylates used as base material
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/046Overbasedsulfonic acid salts
    • C10M2219/0463Overbasedsulfonic acid salts used as base material
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/64Environmental friendly compositions
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00Form in which the lubricant is applied to the material being lubricated
    • C10N2050/015Dispersions of solid lubricants
    • C10N2050/02Dispersions of solid lubricants dissolved or suspended in a carrier which subsequently evaporates to leave a lubricant coating
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00Form in which the lubricant is applied to the material being lubricated
    • C10N2050/10Semi-solids; greasy
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2080/00Special pretreatment of the material to be lubricated, e.g. phosphatising or chromatising of a metal
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B17/00Drilling rods or pipes; Flexible drill strings; Kellies; Drill collars; Sucker rods; Cables; Casings; Tubings
    • E21B17/02Couplings; joints
    • E21B17/04Couplings; joints between rod or the like and bit or between rod and rod or the like
    • E21B17/042Threaded

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Lubricants (AREA)
  • Non-Disconnectible Joints And Screw-Threaded Joints (AREA)

Abstract

A tubular threaded joint for connecting tubing or casing used to excavate oil wells have a lubricating coating formed from a lubricating coating composition comprising one or more basic lubricants selected from a basic sulfonate salt, a basic salicylate salt, a basic phenate salt, and a basic carboxylate salt and having biodegradability value (BOD) of at least 20% when measured after 28 days in seawater. The joint can be used without application of a compound grease containing heavy metals even in a country or region having severe environmental regulations.

Claims (10)

1. A lubricating coating composition comprising at least one basic lubricant selected from a basic sulfonate salt, a basic salicylate salt, a basic phenate salt, and a basic carboxylate salt, the composition having a biodegradability value (BOD) of at least 20% when measured after 28 days in seawater.
2. A lubricating coating composition as set forth in claim 1 which further comprises at least one additional lubricant selected from those having a higher biodegradability than that of the basic lubricant.
3. A lubricating coating composition as set forth in claim 2 wherein the additional lubricant is selected from a fatty acid metal salt and a wax.
4. A lubricating coating composition as set forth in claim 3 wherein the additional lubricant comprises at least one fatty acid metal salt and at least one wax.
5. A lubricating coating composition as set forth in claim 4 which contains 0 - 30 mass% of a volatile organic dissolving medium, the remainder comprising, when its total amount is taken as 100 parts by mass, 55 - 75 parts by mass of the basic lubricant, 20 - 25 parts by mass of the fatty acid metal salt, and 10 -20 parts by mass of the wax.
6. A lubricating coating composition as set forth in any one of claims 3 to wherein the fatty acid metal salt is selected from alkaline earth metal salts of stearic acid or oleic acid.
7. A tubular threaded joint constituted by a pin and a box each having a threaded portion and an unthreaded metal-to-metal contact portion as engaging portions, characterized in that the surfaces of the engaging portions of at least one of the pin and the box have a coating formed from a lubricating coating composition as set forth in any one of claims 1 to 5 and having a thickness of at least 10 micrometers.
8. A tubular threaded joint as set forth in claim 7 wherein the coating has a thickness of from 10 to 200 micrometers.
9. A tubular threaded joint as set forth in claim 7 or 8 wherein the surfaces have a surface roughness of 5 - 40 micrometers Rmax.
10. A tubular threaded joint as set forth in claim 9 wherein the surface roughness is formed by treating the surfaces by a method selected from sand or grit blasting, acid etching, phosphating, electroplating with iron or copper, and blast plating with zinc or a zinc alloy,
CA2665966A 2006-10-13 2007-10-12 Lubricating coating composition suitable for tubular threaded joints Expired - Fee Related CA2665966C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2006280478A JP5145684B2 (en) 2006-10-13 2006-10-13 Lubricating film forming composition suitable for threaded joints for steel pipes
JP2006-280478 2006-10-13
PCT/JP2007/070393 WO2008044799A1 (en) 2006-10-13 2007-10-12 Lubricating coating composition suitable for tubular threaded joints

Publications (2)

Publication Number Publication Date
CA2665966A1 true CA2665966A1 (en) 2008-04-17
CA2665966C CA2665966C (en) 2012-01-03

Family

ID=39282983

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2665966A Expired - Fee Related CA2665966C (en) 2006-10-13 2007-10-12 Lubricating coating composition suitable for tubular threaded joints

Country Status (11)

Country Link
US (1) US20090264326A1 (en)
EP (1) EP2079822A4 (en)
JP (1) JP5145684B2 (en)
CN (1) CN101535458B (en)
AR (1) AR063281A1 (en)
BR (1) BRPI0717398A2 (en)
CA (1) CA2665966C (en)
MX (1) MX336519B (en)
NO (1) NO20091381L (en)
RU (1) RU2418041C2 (en)
WO (1) WO2008044799A1 (en)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR076167A1 (en) * 2009-03-30 2011-05-26 Sumitomo Metal Ind APPLIANCE AND METHOD FOR THE APPLICATION OF A LUBRICANT TO A THREADED PORTION OF A STEEL PIPE
FR2966191B1 (en) 2010-10-15 2013-11-01 Vallourec Mannesmann Oil & Gas TUBULAR THREADED COMPONENT AND RESULTING SEAL
DE202011104255U1 (en) 2011-08-11 2011-11-15 Voswinkel Entwicklungs- Und Verwaltungs-Gmbh & Co. Kg Screw coupling for releasably connecting high pressure hydraulic lines
MX2016002519A (en) 2013-09-02 2016-06-16 Nippon Steel & Sumitomo Metal Corp Composition for forming lubricating coating film, and threaded joint for steel pipe.
US9643206B2 (en) * 2013-09-20 2017-05-09 Nabors Industries, Inc. Lubricant application to threaded pipe connections
JP5979795B2 (en) * 2014-10-28 2016-08-31 ヤマハ発動機株式会社 Connecting rod, internal combustion engine and motor vehicle
RU2606388C1 (en) * 2015-07-20 2017-01-10 Общество с ограниченной ответственностью Научно-исследовательское производственное предприятие"ВАЛЬМА" Thread lubricant
EP3480504A4 (en) * 2016-06-30 2020-01-01 Nippon Steel Corporation Screw joint for pipe and manufacturing method for screw joint for pipe
CN109863341A (en) * 2016-10-18 2019-06-07 新日铁住金株式会社 The manufacturing method of pipe screw joint and pipe screw joint
US11732211B2 (en) 2021-11-30 2023-08-22 Rtx Scientific, Incorporated Pipe sealing compound/adjunct lubricant

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2813375B1 (en) 2000-08-31 2003-06-20 Vallourec Mannesmann Oil & Gas THREADED ELEMENT FOR TUBULAR THREAD-RESISTANT THREADED JOINT
JP4092871B2 (en) * 2000-12-04 2008-05-28 住友金属工業株式会社 Composition for forming a lubricating coating suitable for lubricating treatment of threaded joints
JP2003073681A (en) * 2001-09-03 2003-03-12 Hitachi Ltd Working medium composition for refrigerator and refrigerator using the composition
US6919301B2 (en) * 2001-10-16 2005-07-19 Nsk Ltd. Grease composition and rolling apparatus
JP2003301190A (en) * 2002-02-06 2003-10-21 Nsk Ltd Grease composition and rotary apparatus
JP4218423B2 (en) * 2002-05-31 2009-02-04 住友金属工業株式会社 Threaded joints for steel pipes
ES2334658T3 (en) * 2002-05-31 2010-03-15 Sumitomo Metal Industries, Ltd. THREAD UNION FOR STEEL CONDUCT.
JP4305631B2 (en) * 2003-04-11 2009-07-29 株式会社ジャパンエナジー Biodegradable lubricant
JP4599874B2 (en) * 2004-04-06 2010-12-15 住友金属工業株式会社 Threaded joint for oil well pipe and method for manufacturing the same
EP1864048B1 (en) 2005-03-29 2013-07-17 Nippon Steel & Sumitomo Metal Corporation Threaded joint for steel pipes

Also Published As

Publication number Publication date
EP2079822A4 (en) 2014-08-20
JP2008095019A (en) 2008-04-24
BRPI0717398A2 (en) 2013-10-15
RU2418041C2 (en) 2011-05-10
EP2079822A1 (en) 2009-07-22
CN101535458A (en) 2009-09-16
CN101535458B (en) 2013-06-05
JP5145684B2 (en) 2013-02-20
WO2008044799A1 (en) 2008-04-17
US20090264326A1 (en) 2009-10-22
NO20091381L (en) 2009-07-09
MX336519B (en) 2016-01-21
MX2009003864A (en) 2009-07-02
RU2009117854A (en) 2010-11-20
CA2665966C (en) 2012-01-03
AR063281A1 (en) 2009-01-21

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