CA2305513A1 - Transparent substrate bearing an anti-stain, hydrophobic coating, and process for making it - Google Patents

Transparent substrate bearing an anti-stain, hydrophobic coating, and process for making it Download PDF

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Publication number
CA2305513A1
CA2305513A1 CA002305513A CA2305513A CA2305513A1 CA 2305513 A1 CA2305513 A1 CA 2305513A1 CA 002305513 A CA002305513 A CA 002305513A CA 2305513 A CA2305513 A CA 2305513A CA 2305513 A1 CA2305513 A1 CA 2305513A1
Authority
CA
Canada
Prior art keywords
transparent substrate
stain
organosilane
treatment solution
coating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA002305513A
Other languages
French (fr)
Other versions
CA2305513C (en
Inventor
Yongan Yan
Din-Guo Chen
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yazaki Corp
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2305513A1 publication Critical patent/CA2305513A1/en
Application granted granted Critical
Publication of CA2305513C publication Critical patent/CA2305513C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
    • G02B1/10—Optical coatings produced by application to, or surface treatment of, optical elements
    • G02B1/18—Coatings for keeping optical surfaces clean, e.g. hydrophobic or photo-catalytic films
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/28—Surface treatment of glass, not in the form of fibres or filaments, by coating with organic material
    • C03C17/30—Surface treatment of glass, not in the form of fibres or filaments, by coating with organic material with silicon-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
    • G02B1/10—Optical coatings produced by application to, or surface treatment of, optical elements

Landscapes

  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Optics & Photonics (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Wood Science & Technology (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Paints Or Removers (AREA)
  • Surface Treatment Of Glass (AREA)
  • Laminated Bodies (AREA)
  • Surface Treatment Of Optical Elements (AREA)

Abstract

A process is described for applying a thin-film, hydrophobic, oil-repellant, stain-resistant, optical coating to a transparent substrate. The coating is applied using a treatment solution that incorporates an organosilane in a solvent of water, alcohol, and ethylene glycol or glycerol, and an acid catalyst, with the organosilane having a preferred concentration in the range of 0.05 to 50 mmole per liter. The treatment solution preferably is prepared in a two-step procedure, in which the organosilane is first reacted in concentrated form and then diluted. After the treatment solution has been applied to the transparent substrate, e. g., by dip coating, the coated substrate is dried, preferably by flash-drying at room temperature and then heating it to a prescribed elevated temperature, in a prescribed humidity.
CA002305513A 1997-10-15 1998-10-14 Transparent substrate bearing an anti-stain, hydrophobic coating, and process for making it Expired - Fee Related CA2305513C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US6234997P 1997-10-15 1997-10-15
US60/063,349 1997-10-28
PCT/US1998/021797 WO1999019084A1 (en) 1997-10-15 1998-10-14 Transparent substrate bearing an anti-stain, hydrophobic coating, and process for making it

Publications (2)

Publication Number Publication Date
CA2305513A1 true CA2305513A1 (en) 1999-04-22
CA2305513C CA2305513C (en) 2005-01-04

Family

ID=22041892

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002305513A Expired - Fee Related CA2305513C (en) 1997-10-15 1998-10-14 Transparent substrate bearing an anti-stain, hydrophobic coating, and process for making it

Country Status (5)

Country Link
EP (1) EP1044073A4 (en)
JP (1) JP3579655B2 (en)
AU (1) AU737281B2 (en)
CA (1) CA2305513C (en)
WO (1) WO1999019084A1 (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19941753A1 (en) * 1999-09-02 2001-05-10 Nanogate Gmbh Processes and substances
DE10135684A1 (en) * 2001-07-21 2003-02-06 Nano X Gmbh Material used for making abrasion-resistant, hydrophobic and/or oleophobic coatings comprises an alkoxysilane and/or hydrolyzate with an alkyl and/or polyfluoroalkyl and/or perfluoroalkyl group
FR2858627B1 (en) * 2003-08-06 2006-01-21 Laurent Victor Charles Jacob COMPOSITION FOR CREATING A POLYMER LAYER ON A SUPPORT COMPRISING A MINERAL GLASS FACE FORMING A COMPLEX MATERIAL WITH THE SUPPORT. PROCESS FOR PRODUCING SUCH MATERIALS
DE102005060401A1 (en) * 2005-12-15 2007-06-21 Degussa Gmbh Storage-stable coating composition for abrasion-resistant and weather-resistant equipment of smooth inorganic surfaces with "easy-to-clean" properties
EP2886205A1 (en) 2013-12-19 2015-06-24 Institute of Solid State Physics, University of Latvia Method for antireflective coating protection with organosilanes

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0166363B1 (en) * 1984-06-26 1991-08-07 Asahi Glass Company Ltd. Low reflectance transparent material having antisoiling properties
EP0195493B1 (en) * 1985-03-22 1993-03-24 Toray Industries, Inc. Transparent article and process for preparation thereof
US4636440A (en) * 1985-10-28 1987-01-13 Manville Corporation Novel process for coating substrates with glass-like films and coated substrates
US4778721A (en) * 1986-07-09 1988-10-18 Battelle Memorial Institute Method of forming abrasion-resistant plasma coatings and resulting articles
JP2874391B2 (en) * 1991-06-05 1999-03-24 日産自動車株式会社 Manufacturing method of water-repellent glass
KR100214288B1 (en) * 1993-04-16 1999-08-02 성재갑 Compositions for antifogging coating and molding articles using the same
US5443914A (en) * 1993-12-17 1995-08-22 Nordam Chemically induced crazing resistant acrylic
US5846649A (en) * 1994-03-03 1998-12-08 Monsanto Company Highly durable and abrasion-resistant dielectric coatings for lenses
US6337133B1 (en) * 1996-08-19 2002-01-08 Central Glass Company, Limited Water-repellent glass pane and method for producing same

Also Published As

Publication number Publication date
EP1044073A4 (en) 2005-04-13
AU1090199A (en) 1999-05-03
AU737281B2 (en) 2001-08-16
WO1999019084A1 (en) 1999-04-22
JP2003521360A (en) 2003-07-15
CA2305513C (en) 2005-01-04
EP1044073A1 (en) 2000-10-18
JP3579655B2 (en) 2004-10-20

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