CA2213446A1 - Apparatus and its use for oxychlorination - Google Patents

Apparatus and its use for oxychlorination

Info

Publication number
CA2213446A1
CA2213446A1 CA002213446A CA2213446A CA2213446A1 CA 2213446 A1 CA2213446 A1 CA 2213446A1 CA 002213446 A CA002213446 A CA 002213446A CA 2213446 A CA2213446 A CA 2213446A CA 2213446 A1 CA2213446 A1 CA 2213446A1
Authority
CA
Canada
Prior art keywords
delimitation
gas
gas stream
gas inlet
catalyst
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA002213446A
Other languages
French (fr)
Other versions
CA2213446C (en
Inventor
Reinhard Krumbock
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Vinnolit Monomer GmbH and Co KG
Original Assignee
Hoechst Aktiengesellschaft
Reinhard Krumbock
Vinnolit Monomer Gmbh & Co. Kg
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst Aktiengesellschaft, Reinhard Krumbock, Vinnolit Monomer Gmbh & Co. Kg filed Critical Hoechst Aktiengesellschaft
Publication of CA2213446A1 publication Critical patent/CA2213446A1/en
Application granted granted Critical
Publication of CA2213446C publication Critical patent/CA2213446C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1818—Feeding of the fluidising gas
    • B01J8/1827—Feeding of the fluidising gas the fluidising gas being a reactant
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1818—Feeding of the fluidising gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1836—Heating and cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/15—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination
    • C07C17/152—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination of hydrocarbons
    • C07C17/156—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination of hydrocarbons of unsaturated hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/00141—Coils

Abstract

The preparation of 1,2-dichloroethane from ethylene, hydrogen chloride and oxygen or an oxygen-containing gas (oxychlorination) advantageously proceeds in a reactor having a lower delimitation for a catalyst fluid bed, a first gas inlet (distributor tubes) being arranged above the delimitation and within the catalyst fluid bed, which gas inlet contains nozzles distributed over the entire cross section of the reactor, these nozzles opening into tubes which conduct the exiting gas stream essentially in the opposite direction to the gas stream which fluidizes the catalyst, this gas stream being fed through a second gas inlet beneath the delimitation.
CA002213446A 1995-02-20 1995-05-17 Apparatus and its use for oxychlorination Expired - Fee Related CA2213446C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19505664.7 1995-02-20
DE19505664A DE19505664C2 (en) 1995-02-20 1995-02-20 Device and its use for oxychlorination
PCT/EP1995/001874 WO1996026003A1 (en) 1995-02-20 1995-05-17 Device and use thereof for oxi-chlorination

Publications (2)

Publication Number Publication Date
CA2213446A1 true CA2213446A1 (en) 1996-08-29
CA2213446C CA2213446C (en) 2002-01-29

Family

ID=7754432

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002213446A Expired - Fee Related CA2213446C (en) 1995-02-20 1995-05-17 Apparatus and its use for oxychlorination

Country Status (21)

Country Link
EP (1) EP0810902B1 (en)
JP (1) JPH11500062A (en)
KR (1) KR100368512B1 (en)
CN (1) CN1089026C (en)
AU (1) AU702305B2 (en)
BG (1) BG62436B1 (en)
BR (1) BR9510383A (en)
CA (1) CA2213446C (en)
CZ (1) CZ289342B6 (en)
DE (2) DE19505664C2 (en)
ES (1) ES2126296T3 (en)
HU (1) HU221883B1 (en)
IN (1) IN188066B (en)
NO (1) NO973714D0 (en)
PL (1) PL180784B1 (en)
RO (1) RO118119B1 (en)
RU (1) RU2157726C2 (en)
SK (1) SK282850B6 (en)
UA (1) UA42056C2 (en)
WO (1) WO1996026003A1 (en)
ZA (1) ZA961278B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3039687A4 (en) * 2013-08-29 2017-02-08 Honeywell International Inc. Fluidized bed reactors including conical gas distributors and related methods of fluorination

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19753165B4 (en) 1997-12-01 2006-10-19 Vinnolit Monomer Gmbh & Co. Kg Process for the preparation of 1,2-dichloroethane by oxychlorination
DE19849709C2 (en) * 1998-10-28 2000-09-14 Krupp Uhde Gmbh Process and fluidized bed reactor for oxychlorination of ethylene, oxygen and HCl
DE19903335A1 (en) * 1999-01-28 2000-08-17 Vinnolit Monomer Gmbh & Co Kg Process for the preparation of 1,2-dichloroethane from oxychlorination
DE19911078A1 (en) * 1999-03-12 2000-09-21 Krupp Uhde Gmbh Process for the production of VCM
US6991767B1 (en) * 2000-09-18 2006-01-31 Procedyne Corp. Fluidized bed gas distributor system for elevated temperature operation
DE10258180A1 (en) * 2002-12-12 2004-06-24 Basf Ag Preparation of chlorine involves oxidation of hydrogen chloride and gas stream comprising molecular oxygen in presence of fixed-bed catalyst is carried out in reactor having annular and disk-shaped deflection plates between catalyst tubes
CA2522674A1 (en) 2003-05-09 2004-11-25 The Standard Oil Company Fluidized bed reactor with gas cooler
US7488601B2 (en) 2003-06-20 2009-02-10 Roche Diagnostic Operations, Inc. System and method for determining an abused sensor during analyte measurement
MY140160A (en) 2004-01-28 2009-11-30 Shell Int Research Heat exchanger for carrying out an exothermic reaction
CN1929908B (en) * 2004-03-08 2010-11-03 国际壳牌研究有限公司 Gas distributor for a reactor
AU2006334754B2 (en) * 2005-12-23 2011-06-16 Posco Distributor bottom
CN100435928C (en) * 2006-09-20 2008-11-26 浙江大学 Air distributor
DE102006049546A1 (en) * 2006-10-20 2008-04-30 Vinnolit Gmbh & Co.Kg Profitcenter Vintec Apparatus for oxychlorinating alkenes to produce chlorinated alkanes comprises a fluidized bed reactor with vertical arrays of gas inlets and coolers
DE102008048526A1 (en) * 2008-09-23 2010-04-01 Uhde Gmbh Process for the use of the heat of reaction in the production process of 1,2-dichloroethane from ethylene in a fluidized bed reactor
US8092755B2 (en) 2009-04-06 2012-01-10 Lummus Technology Inc. Devices for injection of gaseous streams into a bed of fluidized solids
CN104941524B (en) * 2014-03-31 2020-11-03 英尼奥斯欧洲股份公司 Feed distributor design for ammoxidation reactor
CN105727846B (en) * 2016-01-29 2019-02-05 清华大学 Flow-guiding type spouted bed and flow-guiding type spouted fluidized bed
JP6373523B1 (en) * 2017-06-19 2018-08-15 旭化成株式会社 Method for producing compound
JP2023503117A (en) * 2019-11-20 2023-01-26 中国石油化工股▲ふん▼有限公司 Gas distribution plate, fluidization device and reaction method
KR20230076022A (en) * 2021-11-23 2023-05-31 주식회사 엘지화학 Bubble column reactor

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1265770A (en) * 1969-07-01 1972-03-08
US4436507A (en) * 1981-07-16 1984-03-13 Foster Wheeler Energy Corporation Fluidized bed reactor utilizing zonal fluidization and anti-mounding air distributors
US4801731A (en) * 1987-12-14 1989-01-31 E. I. Du Pont De Nemours And Company Preparation of acrylonitrile
DE69007965T2 (en) * 1989-10-04 1994-11-03 Asahi Chemical Ind APPARATUS FOR THE PRODUCTION OF ALPHA-BETA-UNSATURATED NITRILES.
DE9116161U1 (en) * 1991-12-07 1992-03-26 Hoechst Ag, 6230 Frankfurt, De
DE4305001A1 (en) * 1993-02-18 1994-08-25 Hoechst Ag Oxychlorination device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3039687A4 (en) * 2013-08-29 2017-02-08 Honeywell International Inc. Fluidized bed reactors including conical gas distributors and related methods of fluorination

Also Published As

Publication number Publication date
DE19505664A1 (en) 1996-08-29
HUT77918A (en) 1998-10-28
UA42056C2 (en) 2001-10-15
CZ289342B6 (en) 2002-01-16
PL180784B1 (en) 2001-04-30
NO973714L (en) 1997-08-12
RU2157726C2 (en) 2000-10-20
PL321830A1 (en) 1997-12-22
IN188066B (en) 2002-08-17
ES2126296T3 (en) 1999-03-16
JPH11500062A (en) 1999-01-06
SK113497A3 (en) 1998-01-14
KR100368512B1 (en) 2003-03-26
CN1175219A (en) 1998-03-04
MX9706276A (en) 1997-11-29
DE59504023D1 (en) 1998-11-26
KR19980702341A (en) 1998-07-15
EP0810902B1 (en) 1998-10-21
SK282850B6 (en) 2002-12-03
CA2213446C (en) 2002-01-29
BG101745A (en) 1998-05-29
BR9510383A (en) 1998-06-02
ZA961278B (en) 1996-08-27
CZ265797A3 (en) 1998-02-18
EP0810902A1 (en) 1997-12-10
AU2881095A (en) 1996-09-11
DE19505664C2 (en) 1996-12-12
BG62436B1 (en) 1999-11-30
CN1089026C (en) 2002-08-14
NO973714D0 (en) 1997-08-12
AU702305B2 (en) 1999-02-18
WO1996026003A1 (en) 1996-08-29
RO118119B1 (en) 2003-02-28
HU221883B1 (en) 2003-02-28

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