CA2122233A1 - Monitoring process consumption rates of additives - Google Patents
Monitoring process consumption rates of additivesInfo
- Publication number
- CA2122233A1 CA2122233A1 CA002122233A CA2122233A CA2122233A1 CA 2122233 A1 CA2122233 A1 CA 2122233A1 CA 002122233 A CA002122233 A CA 002122233A CA 2122233 A CA2122233 A CA 2122233A CA 2122233 A1 CA2122233 A1 CA 2122233A1
- Authority
- CA
- Canada
- Prior art keywords
- additive
- inert tracer
- concentration
- stream
- downstream
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 239000000654 additive Substances 0.000 title claims abstract description 205
- 238000012544 monitoring process Methods 0.000 title claims abstract description 85
- 238000000034 method Methods 0.000 claims abstract description 289
- 230000008569 process Effects 0.000 claims abstract description 246
- 230000000996 additive effect Effects 0.000 claims abstract description 189
- 239000000700 radioactive tracer Substances 0.000 claims abstract description 164
- 238000011143 downstream manufacturing Methods 0.000 claims abstract description 44
- 238000011144 upstream manufacturing Methods 0.000 claims abstract description 37
- 238000004519 manufacturing process Methods 0.000 claims abstract description 35
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 46
- 230000005284 excitation Effects 0.000 claims description 10
- 150000003839 salts Chemical class 0.000 claims description 10
- 241000894007 species Species 0.000 claims description 10
- PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical group C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 claims description 4
- KVBGVZZKJNLNJU-UHFFFAOYSA-N naphthalene-2-sulfonic acid Chemical group C1=CC=CC2=CC(S(=O)(=O)O)=CC=C21 KVBGVZZKJNLNJU-UHFFFAOYSA-N 0.000 claims description 4
- 150000003220 pyrenes Chemical class 0.000 claims description 4
- YZMHQCWXYHARLS-UHFFFAOYSA-N naphthalene-1,2-disulfonic acid Chemical compound C1=CC=CC2=C(S(O)(=O)=O)C(S(=O)(=O)O)=CC=C21 YZMHQCWXYHARLS-UHFFFAOYSA-N 0.000 claims description 3
- XTEGVFVZDVNBPF-UHFFFAOYSA-N naphthalene-1,5-disulfonic acid Chemical group C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1S(O)(=O)=O XTEGVFVZDVNBPF-UHFFFAOYSA-N 0.000 claims 4
- CZLSHVQVNDDHDQ-UHFFFAOYSA-N pyrene-1,3,6,8-tetrasulfonic acid Chemical group C1=C2C(S(=O)(=O)O)=CC(S(O)(=O)=O)=C(C=C3)C2=C2C3=C(S(O)(=O)=O)C=C(S(O)(=O)=O)C2=C1 CZLSHVQVNDDHDQ-UHFFFAOYSA-N 0.000 claims 2
- GPUMPJNVOBTUFM-UHFFFAOYSA-N naphthalene-1,2,3-trisulfonic acid Chemical compound C1=CC=C2C(S(O)(=O)=O)=C(S(O)(=O)=O)C(S(=O)(=O)O)=CC2=C1 GPUMPJNVOBTUFM-UHFFFAOYSA-N 0.000 claims 1
- NNQRIIHNSZKATJ-UHFFFAOYSA-N pyrene hydrate Chemical compound O.C1=CC=C2C=CC3=CC=CC4=CC=C1C2=C43 NNQRIIHNSZKATJ-UHFFFAOYSA-N 0.000 claims 1
- 238000005070 sampling Methods 0.000 description 40
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 36
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 36
- 239000007787 solid Substances 0.000 description 20
- 229910021529 ammonia Inorganic materials 0.000 description 18
- 241000196324 Embryophyta Species 0.000 description 14
- 150000001412 amines Chemical class 0.000 description 14
- 239000002994 raw material Substances 0.000 description 14
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 13
- 238000004458 analytical method Methods 0.000 description 13
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 13
- 239000000126 substance Substances 0.000 description 13
- 239000002699 waste material Substances 0.000 description 13
- 238000004065 wastewater treatment Methods 0.000 description 12
- 238000006731 degradation reaction Methods 0.000 description 11
- 230000004044 response Effects 0.000 description 11
- 229910019142 PO4 Inorganic materials 0.000 description 10
- 229940037003 alum Drugs 0.000 description 10
- 239000007788 liquid Substances 0.000 description 10
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 10
- 239000010452 phosphate Substances 0.000 description 10
- 238000000926 separation method Methods 0.000 description 10
- 239000000203 mixture Substances 0.000 description 9
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 8
- 238000012921 fluorescence analysis Methods 0.000 description 8
- 150000001875 compounds Chemical class 0.000 description 7
- 238000005259 measurement Methods 0.000 description 7
- 238000012545 processing Methods 0.000 description 7
- 239000002253 acid Substances 0.000 description 6
- 239000012530 fluid Substances 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- 239000002351 wastewater Substances 0.000 description 6
- 239000003643 water by type Substances 0.000 description 6
- 238000010790 dilution Methods 0.000 description 5
- 239000012895 dilution Substances 0.000 description 5
- 238000000151 deposition Methods 0.000 description 4
- 238000009472 formulation Methods 0.000 description 4
- 150000002500 ions Chemical class 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 230000015556 catabolic process Effects 0.000 description 3
- 239000013626 chemical specie Substances 0.000 description 3
- 239000012141 concentrate Substances 0.000 description 3
- 230000008021 deposition Effects 0.000 description 3
- 238000001506 fluorescence spectroscopy Methods 0.000 description 3
- 238000004128 high performance liquid chromatography Methods 0.000 description 3
- 238000007670 refining Methods 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- BHMLFPOTZYRDKA-IRXDYDNUSA-N (2s)-2-[(s)-(2-iodophenoxy)-phenylmethyl]morpholine Chemical compound IC1=CC=CC=C1O[C@@H](C=1C=CC=CC=1)[C@H]1OCCNC1 BHMLFPOTZYRDKA-IRXDYDNUSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 101100238304 Mus musculus Morc1 gene Proteins 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 230000002159 abnormal effect Effects 0.000 description 2
- 238000011088 calibration curve Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000005352 clarification Methods 0.000 description 2
- 238000010668 complexation reaction Methods 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 230000008878 coupling Effects 0.000 description 2
- 238000010168 coupling process Methods 0.000 description 2
- 238000005859 coupling reaction Methods 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- 230000005281 excited state Effects 0.000 description 2
- 239000007850 fluorescent dye Substances 0.000 description 2
- 238000002955 isolation Methods 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 241000208140 Acer Species 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- YFONKFDEZLYQDH-OPQQBVKSSA-N N-[(1R,2S)-2,6-dimethyindan-1-yl]-6-[(1R)-1-fluoroethyl]-1,3,5-triazine-2,4-diamine Chemical compound C[C@@H](F)C1=NC(N)=NC(N[C@H]2C3=CC(C)=CC=C3C[C@@H]2C)=N1 YFONKFDEZLYQDH-OPQQBVKSSA-N 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 241000430093 Proeces Species 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 150000004645 aluminates Chemical class 0.000 description 1
- AVKUERGKIZMTKX-NJBDSQKTSA-N ampicillin Chemical compound C1([C@@H](N)C(=O)N[C@H]2[C@H]3SC([C@@H](N3C2=O)C(O)=O)(C)C)=CC=CC=C1 AVKUERGKIZMTKX-NJBDSQKTSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000012993 chemical processing Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000701 coagulant Substances 0.000 description 1
- 230000001447 compensatory effect Effects 0.000 description 1
- 230000002844 continuous effect Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000012864 cross contamination Methods 0.000 description 1
- 230000002939 deleterious effect Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000013213 extrapolation Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000008394 flocculating agent Substances 0.000 description 1
- 238000005188 flotation Methods 0.000 description 1
- 125000001153 fluoro group Chemical group F* 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 239000003701 inert diluent Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 238000001616 ion spectroscopy Methods 0.000 description 1
- 239000002655 kraft paper Substances 0.000 description 1
- 238000000622 liquid--liquid extraction Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000005555 metalworking Methods 0.000 description 1
- MHIGBKBJSQVXNH-IWVLMIASSA-N methacycline Chemical compound C=C([C@H]1[C@@H]2O)C3=CC=CC(O)=C3C(=O)C1=C(O)[C@@]1(O)[C@@H]2[C@H](N(C)C)C(O)=C(C(N)=O)C1=O MHIGBKBJSQVXNH-IWVLMIASSA-N 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 150000002790 naphthalenes Chemical class 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000005456 ore beneficiation Methods 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000004537 pulping Methods 0.000 description 1
- 238000011002 quantification Methods 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000011946 reduction process Methods 0.000 description 1
- IOVGROKTTNBUGK-SJCJKPOMSA-N ritodrine Chemical compound N([C@@H](C)[C@H](O)C=1C=CC(O)=CC=1)CCC1=CC=C(O)C=C1 IOVGROKTTNBUGK-SJCJKPOMSA-N 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000002352 surface water Substances 0.000 description 1
- 239000002349 well water Substances 0.000 description 1
- 235000020681 well water Nutrition 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/18—Water
- G01N33/1826—Organic contamination in water
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A20/00—Water conservation; Efficient water supply; Efficient water use
- Y02A20/20—Controlling water pollution; Waste water treatment
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US5337493A | 1993-04-28 | 1993-04-28 | |
| US08/053,374 | 1993-04-28 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2122233A1 true CA2122233A1 (en) | 1994-10-29 |
Family
ID=21983783
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002122233A Abandoned CA2122233A1 (en) | 1993-04-28 | 1994-04-26 | Monitoring process consumption rates of additives |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP0624798A1 (OSRAM) |
| JP (1) | JP3260960B2 (OSRAM) |
| BR (1) | BR9401631A (OSRAM) |
| CA (1) | CA2122233A1 (OSRAM) |
| TW (1) | TW248590B (OSRAM) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016205944A1 (en) * | 2015-06-23 | 2016-12-29 | Trojan Technologies | Process and device for the treatment of a fluid containing a contaminant |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5413719A (en) * | 1994-01-18 | 1995-05-09 | Nalco Chemical Company | Fluorescent tracer in a water treatment process |
| US5411889A (en) * | 1994-02-14 | 1995-05-02 | Nalco Chemical Company | Regulating water treatment agent dosage based on operational system stresses |
| US6312644B1 (en) * | 1999-12-16 | 2001-11-06 | Nalco Chemical Company | Fluorescent monomers and polymers containing same for use in industrial water systems |
| JP4811703B2 (ja) * | 2005-05-18 | 2011-11-09 | 三浦工業株式会社 | 膜濾過システム |
| WO2007148981A1 (en) * | 2006-06-20 | 2007-12-27 | Institutt For Energiteknikk | The use of biphenyl, terphenyl, and fluorene sulphonic acid based tracers for monitoring streams of fluids |
| US7553673B2 (en) * | 2006-11-13 | 2009-06-30 | Rohmax Additives Gmbh | Quality control of a functional fluid |
| US20130233796A1 (en) * | 2012-03-06 | 2013-09-12 | Narasimha M. Rao | Treatment of industrial water systems |
| US9921155B2 (en) | 2014-11-25 | 2018-03-20 | Baker Hughes, A Ge Company, Llc | Methods of decreasing scale in aqueous systems |
| WO2019023699A1 (en) * | 2017-07-28 | 2019-01-31 | Chemtreat, Inc | METHODS FOR DETECTION OF AMINES FORMING A FILM IN WATER |
| CN113461087B (zh) * | 2021-08-17 | 2022-10-21 | 北京首创生态环保集团股份有限公司 | 一种节约型水厂药耗监测系统 |
| CN119756515B (zh) * | 2024-12-27 | 2025-10-24 | 西南石油大学 | 一种基于气浮分离的体积式流量计及工作方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4783314A (en) * | 1987-02-26 | 1988-11-08 | Nalco Chemical Company | Fluorescent tracers - chemical treatment monitors |
| EP0396732A4 (en) * | 1988-11-14 | 1992-10-07 | Robert M. Dowben | Fluorescent immunoassays and fluorescent compounds and tracers therefore |
| US5132432A (en) * | 1989-09-22 | 1992-07-21 | Molecular Probes, Inc. | Chemically reactive pyrenyloxy sulfonic acid dyes |
| US5128419A (en) * | 1990-08-20 | 1992-07-07 | Nalco Chemical Company | Synthesis of tagged polymers by post-polymerization (trans) amidation reaction |
| US5171450A (en) * | 1991-03-20 | 1992-12-15 | Nalco Chemical Company | Monitoring and dosage control of tagged polymers in cooling water systems |
| US5246860A (en) * | 1992-01-31 | 1993-09-21 | Union Oil Company Of California | Tracer chemicals for use in monitoring subterranean fluids |
-
1994
- 1994-04-25 EP EP94106404A patent/EP0624798A1/en not_active Withdrawn
- 1994-04-26 JP JP08830094A patent/JP3260960B2/ja not_active Expired - Fee Related
- 1994-04-26 CA CA002122233A patent/CA2122233A1/en not_active Abandoned
- 1994-04-27 BR BR9401631A patent/BR9401631A/pt not_active IP Right Cessation
- 1994-04-28 TW TW083103850A patent/TW248590B/zh active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016205944A1 (en) * | 2015-06-23 | 2016-12-29 | Trojan Technologies | Process and device for the treatment of a fluid containing a contaminant |
| US10807882B2 (en) | 2015-06-23 | 2020-10-20 | Trojan Technologies | Process and device for the treatment of a fluid containing a contaminant |
Also Published As
| Publication number | Publication date |
|---|---|
| TW248590B (OSRAM) | 1995-06-01 |
| JPH06343949A (ja) | 1994-12-20 |
| BR9401631A (pt) | 1994-11-01 |
| JP3260960B2 (ja) | 2002-02-25 |
| EP0624798A1 (en) | 1994-11-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FZDE | Dead |