CA2083198A1 - Areca food additives and its foods - Google Patents
Areca food additives and its foodsInfo
- Publication number
- CA2083198A1 CA2083198A1 CA002083198A CA2083198A CA2083198A1 CA 2083198 A1 CA2083198 A1 CA 2083198A1 CA 002083198 A CA002083198 A CA 002083198A CA 2083198 A CA2083198 A CA 2083198A CA 2083198 A1 CA2083198 A1 CA 2083198A1
- Authority
- CA
- Canada
- Prior art keywords
- areca
- food
- calcium
- group
- protein
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 241000202755 Areca Species 0.000 title claims abstract description 122
- 235000013373 food additive Nutrition 0.000 title claims abstract description 51
- 239000002778 food additive Substances 0.000 title claims abstract description 51
- 235000013305 food Nutrition 0.000 title claims abstract description 43
- 150000008442 polyphenolic compounds Chemical class 0.000 claims abstract description 24
- 150000001875 compounds Chemical class 0.000 claims abstract description 20
- 150000003839 salts Chemical class 0.000 claims abstract description 9
- 159000000007 calcium salts Chemical class 0.000 claims abstract description 6
- 125000000524 functional group Chemical group 0.000 claims abstract description 5
- 150000007524 organic acids Chemical class 0.000 claims abstract description 4
- 108090000623 proteins and genes Proteins 0.000 claims description 28
- 102000004169 proteins and genes Human genes 0.000 claims description 28
- 235000008180 Piper betle Nutrition 0.000 claims description 25
- 240000008154 Piper betle Species 0.000 claims description 25
- 239000000843 powder Substances 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 229940079593 drug Drugs 0.000 claims description 13
- 239000003814 drug Substances 0.000 claims description 13
- 235000013399 edible fruits Nutrition 0.000 claims description 13
- 244000081822 Uncaria gambir Species 0.000 claims description 10
- 235000010469 Glycine max Nutrition 0.000 claims description 9
- 244000068988 Glycine max Species 0.000 claims description 9
- -1 protein Chemical class 0.000 claims description 9
- 235000003599 food sweetener Nutrition 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 239000002304 perfume Substances 0.000 claims description 8
- 239000000049 pigment Substances 0.000 claims description 8
- 239000003765 sweetening agent Substances 0.000 claims description 8
- 239000003381 stabilizer Substances 0.000 claims description 7
- 235000008216 herbs Nutrition 0.000 claims description 6
- 241001465754 Metazoa Species 0.000 claims description 5
- 235000012907 honey Nutrition 0.000 claims description 5
- 235000013336 milk Nutrition 0.000 claims description 5
- 239000008267 milk Substances 0.000 claims description 5
- 210000004080 milk Anatomy 0.000 claims description 5
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- 244000223760 Cinnamomum zeylanicum Species 0.000 claims description 4
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- 150000001413 amino acids Chemical class 0.000 claims description 4
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- 235000015218 chewing gum Nutrition 0.000 claims description 4
- 229940112822 chewing gum Drugs 0.000 claims description 4
- 235000017803 cinnamon Nutrition 0.000 claims description 4
- 235000016213 coffee Nutrition 0.000 claims description 4
- 235000013353 coffee beverage Nutrition 0.000 claims description 4
- 235000009508 confectionery Nutrition 0.000 claims description 4
- 235000013601 eggs Nutrition 0.000 claims description 4
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- 239000003755 preservative agent Substances 0.000 claims description 4
- 239000001736 Calcium glycerylphosphate Substances 0.000 claims description 3
- 239000004287 Dehydroacetic acid Substances 0.000 claims description 3
- 235000006679 Mentha X verticillata Nutrition 0.000 claims description 3
- 235000002899 Mentha suaveolens Nutrition 0.000 claims description 3
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims description 3
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 3
- 244000061176 Nicotiana tabacum Species 0.000 claims description 3
- 244000088415 Raphanus sativus Species 0.000 claims description 3
- 235000006140 Raphanus sativus var sativus Nutrition 0.000 claims description 3
- 235000009470 Theobroma cacao Nutrition 0.000 claims description 3
- 244000299461 Theobroma cacao Species 0.000 claims description 3
- 235000010489 acacia gum Nutrition 0.000 claims description 3
- 239000001785 acacia senegal l. willd gum Substances 0.000 claims description 3
- 235000013361 beverage Nutrition 0.000 claims description 3
- 235000012970 cakes Nutrition 0.000 claims description 3
- UHHRFSOMMCWGSO-UHFFFAOYSA-L calcium glycerophosphate Chemical compound [Ca+2].OCC(CO)OP([O-])([O-])=O UHHRFSOMMCWGSO-UHFFFAOYSA-L 0.000 claims description 3
- 229940095618 calcium glycerophosphate Drugs 0.000 claims description 3
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- JEQRBTDTEKWZBW-UHFFFAOYSA-N dehydroacetic acid Chemical compound CC(=O)C1=C(O)OC(C)=CC1=O JEQRBTDTEKWZBW-UHFFFAOYSA-N 0.000 claims description 3
- PGRHXDWITVMQBC-UHFFFAOYSA-N dehydroacetic acid Natural products CC(=O)C1C(=O)OC(C)=CC1=O PGRHXDWITVMQBC-UHFFFAOYSA-N 0.000 claims description 3
- 239000000284 extract Substances 0.000 claims description 3
- 235000013311 vegetables Nutrition 0.000 claims description 3
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims description 2
- RWYRUDPAALLKPX-UHFFFAOYSA-N 2,2-difluoro-n-methylethanamine;hydrochloride Chemical compound Cl.CNCC(F)F RWYRUDPAALLKPX-UHFFFAOYSA-N 0.000 claims description 2
- 108010088751 Albumins Proteins 0.000 claims description 2
- 102000009027 Albumins Human genes 0.000 claims description 2
- CBOCVOKPQGJKKJ-UHFFFAOYSA-L Calcium formate Chemical compound [Ca+2].[O-]C=O.[O-]C=O CBOCVOKPQGJKKJ-UHFFFAOYSA-L 0.000 claims description 2
- 239000001749 Calcium fumarate Substances 0.000 claims description 2
- BCZXFFBUYPCTSJ-UHFFFAOYSA-L Calcium propionate Chemical compound [Ca+2].CCC([O-])=O.CCC([O-])=O BCZXFFBUYPCTSJ-UHFFFAOYSA-L 0.000 claims description 2
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 claims description 2
- SHZGCJCMOBCMKK-UHFFFAOYSA-N D-mannomethylose Natural products CC1OC(O)C(O)C(O)C1O SHZGCJCMOBCMKK-UHFFFAOYSA-N 0.000 claims description 2
- 108010022355 Fibroins Proteins 0.000 claims description 2
- 229930091371 Fructose Natural products 0.000 claims description 2
- 239000005715 Fructose Substances 0.000 claims description 2
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 2
- 108010010803 Gelatin Proteins 0.000 claims description 2
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 claims description 2
- 244000303040 Glycyrrhiza glabra Species 0.000 claims description 2
- 239000004378 Glycyrrhizin Substances 0.000 claims description 2
- 235000017443 Hedysarum boreale Nutrition 0.000 claims description 2
- 235000007858 Hedysarum occidentale Nutrition 0.000 claims description 2
- SHZGCJCMOBCMKK-JFNONXLTSA-N L-rhamnopyranose Chemical compound C[C@@H]1OC(O)[C@H](O)[C@H](O)[C@H]1O SHZGCJCMOBCMKK-JFNONXLTSA-N 0.000 claims description 2
- PNNNRSAQSRJVSB-UHFFFAOYSA-N L-rhamnose Natural products CC(O)C(O)C(O)C(O)C=O PNNNRSAQSRJVSB-UHFFFAOYSA-N 0.000 claims description 2
- 229920000161 Locust bean gum Polymers 0.000 claims description 2
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims description 2
- 239000004677 Nylon Substances 0.000 claims description 2
- 239000001888 Peptone Substances 0.000 claims description 2
- 108010080698 Peptones Proteins 0.000 claims description 2
- FNAQSUUGMSOBHW-UHFFFAOYSA-H calcium citrate Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O FNAQSUUGMSOBHW-UHFFFAOYSA-H 0.000 claims description 2
- 239000001354 calcium citrate Substances 0.000 claims description 2
- 235000013921 calcium diglutamate Nutrition 0.000 claims description 2
- 235000019255 calcium formate Nutrition 0.000 claims description 2
- 239000004281 calcium formate Substances 0.000 claims description 2
- 229940044172 calcium formate Drugs 0.000 claims description 2
- 235000019296 calcium fumarate Nutrition 0.000 claims description 2
- OLOZVPHKXALCRI-UHFFFAOYSA-L calcium malate Chemical compound [Ca+2].[O-]C(=O)C(O)CC([O-])=O OLOZVPHKXALCRI-UHFFFAOYSA-L 0.000 claims description 2
- 239000001362 calcium malate Substances 0.000 claims description 2
- 229940016114 calcium malate Drugs 0.000 claims description 2
- 235000011038 calcium malates Nutrition 0.000 claims description 2
- GUPPESBEIQALOS-UHFFFAOYSA-L calcium tartrate Chemical compound [Ca+2].[O-]C(=O)C(O)C(O)C([O-])=O GUPPESBEIQALOS-UHFFFAOYSA-L 0.000 claims description 2
- 235000011035 calcium tartrate Nutrition 0.000 claims description 2
- 239000001427 calcium tartrate Substances 0.000 claims description 2
- UMVAYAXXQSFULN-QHTZZOMLSA-L calcium;(2s)-2-aminopentanedioate;hydron Chemical compound [Ca+2].[O-]C(=O)[C@@H](N)CCC(O)=O.[O-]C(=O)[C@@H](N)CCC(O)=O UMVAYAXXQSFULN-QHTZZOMLSA-L 0.000 claims description 2
- HDRTWMBOUSPQON-ODZAUARKSA-L calcium;(z)-but-2-enedioate Chemical compound [Ca+2].[O-]C(=O)\C=C/C([O-])=O HDRTWMBOUSPQON-ODZAUARKSA-L 0.000 claims description 2
- PBUBJNYXWIDFMU-UHFFFAOYSA-L calcium;butanedioate Chemical compound [Ca+2].[O-]C(=O)CCC([O-])=O PBUBJNYXWIDFMU-UHFFFAOYSA-L 0.000 claims description 2
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 2
- 229930002875 chlorophyll Natural products 0.000 claims description 2
- 235000019804 chlorophyll Nutrition 0.000 claims description 2
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 claims description 2
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 claims description 2
- 239000008273 gelatin Substances 0.000 claims description 2
- 235000011852 gelatine desserts Nutrition 0.000 claims description 2
- LPLVUJXQOOQHMX-UHFFFAOYSA-N glycyrrhetinic acid glycoside Natural products C1CC(C2C(C3(CCC4(C)CCC(C)(CC4C3=CC2=O)C(O)=O)C)(C)CC2)(C)C2C(C)(C)C1OC1OC(C(O)=O)C(O)C(O)C1OC1OC(C(O)=O)C(O)C(O)C1O LPLVUJXQOOQHMX-UHFFFAOYSA-N 0.000 claims description 2
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- UYRUBYNTXSDKQT-UHFFFAOYSA-N glycyrrhizic acid Natural products CC1(C)C(CCC2(C)C1CCC3(C)C2C(=O)C=C4C5CC(C)(CCC5(C)CCC34C)C(=O)O)OC6OC(C(O)C(O)C6OC7OC(O)C(O)C(O)C7C(=O)O)C(=O)O UYRUBYNTXSDKQT-UHFFFAOYSA-N 0.000 claims description 2
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- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 claims description 2
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- JAWMENYCRQKKJY-UHFFFAOYSA-N [3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-ylmethyl)-1-oxa-2,8-diazaspiro[4.5]dec-2-en-8-yl]-[2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidin-5-yl]methanone Chemical compound N1N=NC=2CN(CCC=21)CC1=NOC2(C1)CCN(CC2)C(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F JAWMENYCRQKKJY-UHFFFAOYSA-N 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- WQZGKKKJIJFFOK-PHYPRBDBSA-N alpha-D-galactose Chemical compound OC[C@H]1O[C@H](O)[C@H](O)[C@@H](O)[C@H]1O WQZGKKKJIJFFOK-PHYPRBDBSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000000605 aspartame Substances 0.000 description 1
- IAOZJIPTCAWIRG-QWRGUYRKSA-N aspartame Chemical compound OC(=O)C[C@H](N)C(=O)N[C@H](C(=O)OC)CC1=CC=CC=C1 IAOZJIPTCAWIRG-QWRGUYRKSA-N 0.000 description 1
- 229960003438 aspartame Drugs 0.000 description 1
- 235000010357 aspartame Nutrition 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 235000014121 butter Nutrition 0.000 description 1
- 235000001465 calcium Nutrition 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 235000009120 camo Nutrition 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 239000005018 casein Substances 0.000 description 1
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 1
- 235000021240 caseins Nutrition 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 235000005607 chanvre indien Nutrition 0.000 description 1
- 229950001002 cianidanol Drugs 0.000 description 1
- 229940125904 compound 1 Drugs 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 201000004101 esophageal cancer Diseases 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 229930182830 galactose Natural products 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 229960003180 glutathione Drugs 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000011487 hemp Substances 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 235000015110 jellies Nutrition 0.000 description 1
- 239000008274 jelly Substances 0.000 description 1
- 239000008101 lactose Substances 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- AVCKMGVFKDWJML-UHFFFAOYSA-M lithium;2,6-ditert-butyl-4-methylphenolate Chemical compound [Li+].CC1=CC(C(C)(C)C)=C([O-])C(C(C)(C)C)=C1 AVCKMGVFKDWJML-UHFFFAOYSA-M 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 235000019713 millet Nutrition 0.000 description 1
- 235000013379 molasses Nutrition 0.000 description 1
- 235000013557 nattō Nutrition 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 235000020232 peanut Nutrition 0.000 description 1
- 229940048914 protamine Drugs 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 208000026451 salivation Diseases 0.000 description 1
- 235000014102 seafood Nutrition 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 235000010413 sodium alginate Nutrition 0.000 description 1
- 239000000661 sodium alginate Substances 0.000 description 1
- 229940005550 sodium alginate Drugs 0.000 description 1
- PDEFQWNXOUGDJR-UHFFFAOYSA-M sodium;2,2-dichloropropanoate Chemical compound [Na+].CC(Cl)(Cl)C([O-])=O PDEFQWNXOUGDJR-UHFFFAOYSA-M 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000009747 swallowing Effects 0.000 description 1
- 235000020234 walnut Nutrition 0.000 description 1
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Confectionery (AREA)
Abstract
ABSTRACT OF THE DISCLOSURE
This invention relates to areca food additives, especially, to additives for areca quids and foods containing areca component, and their preparation methods. High alkaline lime always exists in conventional areca food additive. Many problems consequently result such as oral cancer and the polluting of the environment by the spitting of a bright red liquid. A series of eatable neutral calcium salts of organic acid and compounds containing at least one of the following functional groups selected from the group consisting of -NH2, =NH, =N, -NH-, -CONH-, -HCO-, -CO-, -COOR-, -S-, and their salts were invented to replace lime. The taste of astringent and harms caused by the polyphenolic compounds of areca quid could be completely improved. The disease of quid chewer would be decreased and the problem of environmental pollution would be improved.
This invention relates to areca food additives, especially, to additives for areca quids and foods containing areca component, and their preparation methods. High alkaline lime always exists in conventional areca food additive. Many problems consequently result such as oral cancer and the polluting of the environment by the spitting of a bright red liquid. A series of eatable neutral calcium salts of organic acid and compounds containing at least one of the following functional groups selected from the group consisting of -NH2, =NH, =N, -NH-, -CONH-, -HCO-, -CO-, -COOR-, -S-, and their salts were invented to replace lime. The taste of astringent and harms caused by the polyphenolic compounds of areca quid could be completely improved. The disease of quid chewer would be decreased and the problem of environmental pollution would be improved.
Description
~3~
SPECIFICATION
Areca quid chewing is an almost universal indulgence in many regions of southeastern Asia, and in small and large islands adjacent to the coast, and in the Southwest Pacific area.
The preparation of the areca quid is fairly uniform in this part of the world, with variations existing only in the compositions of areca food additives. Lime is the most important component of areca food additive.
The other constituent may have been selected from the group consisting of gambir, tobacco, coffee, cocoa, Chinese herbs, and modifier such as sweetener, perfume, preserver, stabilizer, color pigment and fillers. The areca food additive is usually in the form of paste.
The preparation of traditional areca quid has been done in several ways.
1. Chewing is practiced by filrst inserting a piece of the areca seed pulp in the mouth. This is masticated for a few seconds, followed by with the betel leaf or betel fruit, with a generous helping of lime, being taken; a large wad then results, in which a long-continued indulgence of the tissues in the oral cavity becorne stained bright red. The mixture induces intense salivation. The areca seed is highly astringent. This unpleasant ef~ect, however, is neutralized by the lime in expectation.
SPECIFICATION
Areca quid chewing is an almost universal indulgence in many regions of southeastern Asia, and in small and large islands adjacent to the coast, and in the Southwest Pacific area.
The preparation of the areca quid is fairly uniform in this part of the world, with variations existing only in the compositions of areca food additives. Lime is the most important component of areca food additive.
The other constituent may have been selected from the group consisting of gambir, tobacco, coffee, cocoa, Chinese herbs, and modifier such as sweetener, perfume, preserver, stabilizer, color pigment and fillers. The areca food additive is usually in the form of paste.
The preparation of traditional areca quid has been done in several ways.
1. Chewing is practiced by filrst inserting a piece of the areca seed pulp in the mouth. This is masticated for a few seconds, followed by with the betel leaf or betel fruit, with a generous helping of lime, being taken; a large wad then results, in which a long-continued indulgence of the tissues in the oral cavity becorne stained bright red. The mixture induces intense salivation. The areca seed is highly astringent. This unpleasant ef~ect, however, is neutralized by the lime in expectation.
2~,~3~8 2. Another areca quid is that in which a fresh areca is cracked up at one side of it and a small amount of areca food additive is pasted. A chop of betel fruit or betel stem is added onto it.
3. Still areca quid is first to spread a small amount of areca food additive S on a piece of betel leaf. A piece of areca is wrapped inside the leaf with the areca food additive face inside.
4. The still areca quid is prepared by using a piece of areca seed in stead of the areca in method 3.
5. The still areca quid is conducted in the sarne way as methods 1 and 2 1 0 but without betel fruit or betel stem.
Davis reported of the relationship existing between areca quid chewing and the higher incidence.of oral cancer [ J. A. M. A., 64: 711-718, 1915; J. Tropical Med., 27: 274-278, 1924 ]. The active agent is lime of the chew .
1 ~ The so-called "crude drugs", including areca, areca seed, gambir, betel leaf, betel fruit and betel stem contain a large quantity of polyphenolic compounds which are the taste of astringent and cause harm to the tissue of oral mucosa; forming a leather like compound and being associated with oral and esophageal cancer and other diseases [ Bhide et al.,l984;
2 0 Publication No.57; IARC,1984, pp 851857; Brunneman et al, 1985 J. Agric, Food chem. 1985,vol. 33, 1178-1181 ]. The efficiency of lime is very poor even though people use lime to improve the effects of polyphenolic cornpounds. The high alkaline property of lime, in addition to that, also produces many bad results, such as:
2 5 1. The lime in areca food additive makes the pH value of higher than 12.5, which would corrode the oral mucosa of chewer. The part corroded by lime would tan when the release of polyphenolic compounds existed from the crude drug during chewing and could not completely react with lime at the moment of release. Leathering or induce oral cancer would 3 0 consequently occur;
2. The bad odor of lime is uncomfortable;
3. The teeth of the areca quid chewer are damaged by the high alkaline lime, which cannot stand the heat, acidity and rapid change of temperature. The foods belong to these conditions which are not 3 5 enjoyable for areca quid chewer;
4. The spitting of the bright red chewing juice is one of the environmental pollutions in society;
5. Swallowing a great amount of lime reduces the acidity of stomach and increases the chance of cancer occurring.
~83~
Many methods proposed for improving the bad effects of areca food additive currently exist, such as those being disclosed in the patent gazette No. 7010610 and No. 7112377 of Taiwan R.O.C.. Those methods did not use lime and gambir. The problems caused by the polyphenolic 5 compounds still remain, al~hough the problem of the bright red juice could be improYed. A series of eatable neutral calcium salts; and compounds containing at least one of the following functional groups selected from the group consisting of -NH2, =NH, ~N,-NH-,-CONH-, -HCO-, -CO-, -COOR-, -S-, and their salts; especially, protein, derivatives of 10 protein and food containing protein; show excellent properties in comparison with lime. The astringent, tastes and harms caused by the polyphenolic compounds of areca quid could be improved. The disease of quid chewer could be decreased and the problem of environmental pollution could be improved completely.
BRIEF SUMMARY OF THE ~NVENTION:
1. Accordingly, it is therefore a general object of the invention to provide a novel composition of areca food additive which dose not contain lime;
2 0 2.1t is an object of the present invention to provide a new method of preparing areca food additive which would use neutral calcium salt to react with the polyphenolic compounds contained in crude drugs -instead of reacting with a high alkaline lime which causes many diseases to the areca quid chewer;
2 5 3. Another object of the present invention is to provide a novel composition of arecn food udditive comprising crude drug, compound containing at least one of the functional group selected from the group consisting of -NH2, =NH, ~N, -NH-, -CONH-,-HCO-, -CO-, -COOR-, -S-, and their salts; especially, protein, derivatives of protein and food containing 3 0 protein; and modifier selected from the group of sweetener, perfume, preserver, stabilizer, color pigment, Chinese herbs and fillers;
4. A still more specific object of the present invention is to provide a novel areca quid which uses eatable neutral calcium salts of organic acids. Reacting with the polyphenolic compounds of crude drugs, instead 3 5 of high alkalinc lirne, is the goal;
5. Yet another object of the present invention is to accordingly provide a novel method for preparation of areca quid which uses food contain functional group selected from the group consisting of NH2, =NH, ~N, -NH-, -CONH-, -HCO-, -CO-, -COOR-, -S-, and their salts; especially, protein, 3~
derivatives of protein and food containing protein; this would be in order to react with the polyphenolic compounds of crude drugs instead of high alkaline lime;
Davis reported of the relationship existing between areca quid chewing and the higher incidence.of oral cancer [ J. A. M. A., 64: 711-718, 1915; J. Tropical Med., 27: 274-278, 1924 ]. The active agent is lime of the chew .
1 ~ The so-called "crude drugs", including areca, areca seed, gambir, betel leaf, betel fruit and betel stem contain a large quantity of polyphenolic compounds which are the taste of astringent and cause harm to the tissue of oral mucosa; forming a leather like compound and being associated with oral and esophageal cancer and other diseases [ Bhide et al.,l984;
2 0 Publication No.57; IARC,1984, pp 851857; Brunneman et al, 1985 J. Agric, Food chem. 1985,vol. 33, 1178-1181 ]. The efficiency of lime is very poor even though people use lime to improve the effects of polyphenolic cornpounds. The high alkaline property of lime, in addition to that, also produces many bad results, such as:
2 5 1. The lime in areca food additive makes the pH value of higher than 12.5, which would corrode the oral mucosa of chewer. The part corroded by lime would tan when the release of polyphenolic compounds existed from the crude drug during chewing and could not completely react with lime at the moment of release. Leathering or induce oral cancer would 3 0 consequently occur;
2. The bad odor of lime is uncomfortable;
3. The teeth of the areca quid chewer are damaged by the high alkaline lime, which cannot stand the heat, acidity and rapid change of temperature. The foods belong to these conditions which are not 3 5 enjoyable for areca quid chewer;
4. The spitting of the bright red chewing juice is one of the environmental pollutions in society;
5. Swallowing a great amount of lime reduces the acidity of stomach and increases the chance of cancer occurring.
~83~
Many methods proposed for improving the bad effects of areca food additive currently exist, such as those being disclosed in the patent gazette No. 7010610 and No. 7112377 of Taiwan R.O.C.. Those methods did not use lime and gambir. The problems caused by the polyphenolic 5 compounds still remain, al~hough the problem of the bright red juice could be improYed. A series of eatable neutral calcium salts; and compounds containing at least one of the following functional groups selected from the group consisting of -NH2, =NH, ~N,-NH-,-CONH-, -HCO-, -CO-, -COOR-, -S-, and their salts; especially, protein, derivatives of 10 protein and food containing protein; show excellent properties in comparison with lime. The astringent, tastes and harms caused by the polyphenolic compounds of areca quid could be improved. The disease of quid chewer could be decreased and the problem of environmental pollution could be improved completely.
BRIEF SUMMARY OF THE ~NVENTION:
1. Accordingly, it is therefore a general object of the invention to provide a novel composition of areca food additive which dose not contain lime;
2 0 2.1t is an object of the present invention to provide a new method of preparing areca food additive which would use neutral calcium salt to react with the polyphenolic compounds contained in crude drugs -instead of reacting with a high alkaline lime which causes many diseases to the areca quid chewer;
2 5 3. Another object of the present invention is to provide a novel composition of arecn food udditive comprising crude drug, compound containing at least one of the functional group selected from the group consisting of -NH2, =NH, ~N, -NH-, -CONH-,-HCO-, -CO-, -COOR-, -S-, and their salts; especially, protein, derivatives of protein and food containing 3 0 protein; and modifier selected from the group of sweetener, perfume, preserver, stabilizer, color pigment, Chinese herbs and fillers;
4. A still more specific object of the present invention is to provide a novel areca quid which uses eatable neutral calcium salts of organic acids. Reacting with the polyphenolic compounds of crude drugs, instead 3 5 of high alkalinc lirne, is the goal;
5. Yet another object of the present invention is to accordingly provide a novel method for preparation of areca quid which uses food contain functional group selected from the group consisting of NH2, =NH, ~N, -NH-, -CONH-, -HCO-, -CO-, -COOR-, -S-, and their salts; especially, protein, 3~
derivatives of protein and food containing protein; this would be in order to react with the polyphenolic compounds of crude drugs instead of high alkaline lime;
6. Still another object of the present invention is to provide novel 5 foods, such as beverages, biscuits, candy, cake, chewing gum, and throat lozengers all of which would contain the areca or the component of areca;
7. A general object of this invention is to provide areca quid which are eatable and will improve the environmental pollution caused by the 10 spitting of a bright red juice.
Other and further objects, features and advantages of the invention will nppear more from the following description.
DETAILED DESCRIPTIOND
15 A series of eatable compounds for preparation areca food additive, which have an excellent effect for reaction with polyphenolic compounds, has been devised by the inventor. This series of eatable compounds is superior to the traditional lime compound and could improve all the present disadvantages in areca food.
2 0 The eatable foods include; salts of calcium organic acid, such as calcium formate, calcium fumarate, calcium glautamete, calcium glycerophosphate, culcium lactate, calcium malate, calcium maleate, calcium succinate, calcium tartrate, calcium citrate and calcium glutamate; food which contains at least one of the following functional 25 groups selected from the group consisting of -NH2, =NH, ..N, -NH-, -CONH-, -HCO-, -CO-, -COOR-, -S-, and their salts; particularly, protein, hydrolyzed products of protein and foods containing protein.
Specific examples which contain the functionnl group selected from the group consisting of -NH2, =NH, I.N,-NH-,-CONH-,-HCO-,-CO-, -COOR-, 3 0 -S- are pure proteins, such as hemialbumin, albumin, histone, gelatin, protamine, albuminoid; complex proteins, such as nucleoproteid, glycoproteid, phosphoproteid and liporoteid; derivative proteins, such as m-protein and peptone; hydrolyzed protein, such as gelatine, polypeptide and amino acid; and their mixture compounds.
3 5 The special examples which contain -CONH- group are fibroin, keratin, and low molecule weight of nylon. The special examples which contain -HCO-, -CO- are reducing compounds, such as rhamnose, galactose and lactose. The special examples contain -COOR- are synthetic polyethers, such as methly cellulose, Tweens, and poly-N-vinyl-pyrolidine.
Most of the compounds previously mentioned could be produced from foods, including foods of vegetable and animal. These the foods, especially those containing protein or amino acids, show good properties for reaction of polyphenolic compounds. The properties are based on the quantity of protein and/or amino acid of which they are borne. These discoverings are very useful to this invention. The vegetables including various kind of grain foods, seeds, and their products, such as soy bean, green bean, nzuki bean, peanut, germs, soy bean crude, sesame seed, hemp seed, natto, kidney bean, radish, walnut; and animal foods, such as milk, sea foods, egg, tissues of animals, yeast, meat all belong to food.
The compounds for the areca food additive would be better in a state of fine particle in order for an effect of reaction.
The modifier to be used in areca food additive is selected from the group consisting of sweeteners, perfumes, preservers, stabili~ers, color pigments, herbs and fillers. They are compounds of sweeteners such as honey, maltose, sugar, fructose, glycyrrhizin, saccrin, d-sorbital and d-mannitol; perfumes, such as mint and essential oils; preservatives, such as benzoate, sodium benzoate, calcium propinate, sorbitar, dehydroacetic acid and its salts, sorbic acid; stabilizers, such as CMC, pectin, arabic gum, 2 0 and locust bean gum; color pigment, such as chlorophyll and green No. I;
Chinese herbs, such as licorice root, cinnamon, coffee and cocoa. They are used in a favorable amount and according to the food regulations.
The compounds and their amounts for the requirement of reaction with polyphenolic compounds of areca quid are not strictly confined to 2 5 one kind of compounds and a specific amount. They, however, depend on the quantity of total polyphenolic compounds contained. The equivalent of chemical reaction is usually greater than the equivalent of polyphenolic compounds. The composition of crude drug depends on the season of their harvests and the degree of reap. Their content of 3 0 polyphenolic compounds then varies over a wide range.
7 ~33% of d-catechin and 22~50% of gambir tanning contained in gambir exist. The seed of area bears approximately 40% of the polyphenolic compounds in green and is reduced to appro?cimately 20%
after ripening. The fruit of areca has only 2~8%. The stem, fruit and leaf 3 5 of areca betel, respectively, bears 2~5%, 1~3%, and 1~2% in weight of polyphenolic compounds.
The preparation method of areca food is not limited to using fresh crude drugs. That methvd also uses the crude drugs which can be grounded into powder or into a state of paste; can be extracted for s ~3g3~
components by water or organic solvents, such as hexane, alcohol and ether, to remove the fibre; and can be separated the effective components from the extracts.
The areca food additive may be in the form of paste, powder in package, 5 solid produced from drying the paste, and in liquid.
The areca food additive compounds with foods and other crude drugs, stabilizers, pigments, preservative agents, perfumes and sweeteners in the proper quantity in order to form a state of chewing gum, cake, biscuits, lozengers, beverages or candy. That is good for packing and 1 0 storage.
The invention will be understood more readily with reference to the following examples. These examples, however, are intended to illustrate the invention and are not be meant to limit the scope of the invention.
Traditional art examples 1.
After dissolving 0.04 g of pictin in 14 g of water, 0.02 g of benzoic acid, 0.4 g of cinnamon, 10 g of honey and 8 g of gambir are added into the solution, and pasted by homogenizer to form a areca food additive.
Traditional art example 2.
The same example as traditional art example 1, except 8 g of lime, is 20 compounded in it.
Traditional example 3.
The same example as traditional art example 1, except 10 g of calcium carbonate, is compound in it.
Example 1.
2 5 The same example as traditional art example 1, except 12 B of casein powder, is compounded in it.
Example 2.
After dissolving 0.08 g of arabic gum in 30 g of water, 0.006 g of benzoic acid, 0.02 g apple essence, I g of sugar and 24 g of radish powder are 3 0 added into the solution in turn, and pasted by a homogenizer to form a areca food additive.
Example 3.
After dissolving 0.0~ g locust bean in 30 g of water, 0.2 g of sodium propinate, 0.02 g of peppermint, 12 g of molasses and 12 g soybean lees 3 5 powder are added into the solution in turn, and pasted by a homogenizer to form a areca food additive.
Example 4.
After dissolving 0.04 g of ester of p-hydroxybenzoic acid in 16 g of water, 0.2 g of D-mantol, 8 g of gambir and 14 g of glutathione are added 2.~8~
into the solution, and pasted by a homogenizer in order to form a areca food additive.
Example 5.
2 g of Aspartame, 10 g of m-protein and 8 g oî water are pasted by a S homogenizer to form a areca food additive.
Example 6.
20 g of water, 6 g of gambir, 8 g of soybean powder and 8 g of soybean Iees powder are pasted by a homogenizer in order to form a areca food additive.
Example 7.
40 g of bean paste, 10 g of rice bran, 8 g of soybean lees powder and 0.08 g of DHA(dehydroacetic acid) are pasted by a homogenizer in order to form a areca food additive.
Example 8.
60 g of fermented bean curd are pasted by a homogenizer in order to form a areca food addi~ive.
Example 9.
60 g of fermented bean curd, 20 g of sugared bean and 8 g of coffee powder are pasted by a homogenizer in order to form a areca food 2 0 additive.
Example 10.
16 g of honey and 20 g green bean are pasted by a homogenizer in order to form a areca food additive.
Example 1 1.
After dissolving 0.04 g of DHA in 20 g of water, 6 g of honey, 6 B of lave and 16 g milk powder ure pasted by a homogenizer in order to form a areca food additive.
Example 12.
After dissolving 6 B of gelatine in 40 g of water, 0.8 g alcohol, 0.2 g of 3 0 cinnamon, 10 g of gambir and 8 g of fish powder are pasted by a homogenizer to form a areca food additive.
Example 13.
2 g of Aspartume and 20 g of calcium glycerophosphate are pasted in 20 g of water by a homogenizer in order to form a areca food additive.
3 5 Experimental testing 1.
All the pastes of areca food additives products made in traditional art examples ~rom 1 to 3. Examples from 1 to 13 are respectively divided into 20 equal parts.
Each kind of pastes 4 parts are respectively, as previously done, into a 100 ml beaker. A volume of 70 ml of water is added into each beaker and mixed with a mixer for 10 minutes. The mixture is filtered and the color of solution i9 recorded. The free amount of polyphenolic compounds are S analyzed and the results are shown in Ta~le 1.
Table 1 Item color of amount of Item color of llmount 10solution polyphcnol solution polyphenol Tra~ Exam. I Bnght red much Exumple 6 Light none Trad. Exsm. I Bright redmuch Example 7 Light none Trad. Exam. I BrJght redmuch Example 8 Light none Example I Light noneExample 9 Light none Example 2 Light noneExample 10 Light none Exnmple 3 Light . noneExample 11 Light none Ex~nple 4 Light noneExample 12 Light none Example S Light noneExample 13 Light none ____________________________________._____________________ ______ The color of solutions made from the invention are obviously all not shown in a bright red color like those of the traditional art examples. No free polyphenolic compounds being detected from the solutions of the 2 5 invention existed..
Traditional art example 4.
15 pieces of Taiwan areca, the average weight being 4 g, are cracked from longitudinal side in half way. Put one part of paste of areca food additive made from traditional art example I in the crack, and a chop of 3 0 betel fruit i9 mounted on the paste, respectively.
Traditional art example 5.
The same as traditional art example 5, except for the paste of areca food additive, is done by using the one made from traditional art example 2.
Traditional art exnmple 6.
3 5 The same as traditional art example 4 ,except for the paste areca food additive, is done by using the one made from traditional art example 3.
Example 14.
The same as traditional art example 4 except the paste of areca food additive is using the one made from example 1.
3 ~ ~ ~
Example 15.
15 pieces of betel leave, which have an average weight of 2.8 g, are spread one part of pastes from an areca food additive made from an example on the up side and wrapped up a piece of Taiwan areca of S approximately 4 g weight, respectively, to form an areca quid.
Example 16.
The paste made from example 3 is mixed with 10 g of tobacco and is divided into 20 parts. IS pieces of Taiwan betel leave, having an average weight of 2.8 g, a}e spread with one part of pastes of areca food additive 10 as previously made, and a piece of Taiwan areca is respectively wrapped up in order to produce areca quids.
Example 17.
15 pieces of Taiwan areca, having an average weight of 8 g, are cracked from a longitudinal side in a half way. One part of paste of areca l S food additive made from example 4 is put in the crack. A chop of 0.7 g of betel fruit is respectively added onto it. The areca quids are then produced.
Example 1 8.
The same as exarnple 17, except the average weight of areca is 4 g and 2 0 the pastes of areca food additive are using the ones made from example 5.
Example 19.
The same as exumple 18, except the pastes of areca food additive are made from example 6.
Example 20.
25 The same as example 15, except the average weight of betel leave is 2.1 g and the paste of areca food additive is made from example 7.
Example 2 1.
The same as example 20, except an average weight of l.S g of Taiwan areca seed is instead of betel fruit, and the paste of areca food additive is 3 0 made from example 8.
Example 22.
The same as example 17, except the average weight of areca is 4.2 g, and 0.3 g of betel stem instead of the betel fruit and the paste of a}eca food additive is made from example 9.
3 S Example 23.
The same as example 18, except the average weight of areca is 4.1 g, the paste of areca food additive is made from example 11 and the betel fruit is l.S g instead.
Example 24.
g 2~3~8 The same as example 17, except the average weight of areca is 8.1 g, thc paste of areca food additive is made from example 12 and the betel fruit is 1 g.
Experimental testing 2.
5 Taking IS pieces of product out of each of the comparison, examples from 4 to 6 and examples from 14 to 24, are crushed by crush the machine and 200 ml of water is respectively added into n 300 ml beaker mixing for 10 minutes. The procedure as described in experimental testing I is to be followed with the results being shown in Table 2.
Table 2 Itcm color of amount Or Item color ot ~mount solution polyphenol solutlon polyphenol ___________________________ ___________________________ l S _Trad. Exam. 4 Bright red much Example 18 Light none Trad. Exam. 5 Bright red much Example 19 Light none Trad. Exam. 6 Bright red much Example 20 Light none Example 14 Light none Example 21 LiBht none Example 15 Light none Example 22 Light none 2 0 Example 16 Light none Example 23 Light none Exarnple 17 Light none Example 24 Light none __________________________________________________.______________ The products made by present invention are obviously similar to 2 5 results as shown in experimental testing 1. The traditional ones are, meanwhile, shown in bright red in the solution with much of the free polyphenolic compounds having remained.
Experimental testing 3.
The taste testings are performed by distribution of one piece of S quids 3 0 as produced from each of traditional art examples from 4 to 6 and examples from 14 to 24, to one of S persons for chewing, respectively.
The color of chewing liquid and taste are recorded. The results are shown in Table 3.
2 ~
T~lble 3 ___________,_______ _____.___._____________________________________ Item color or ta~tc o~ Itcm ~olor of taste of solution chewing ~41ut~on chcwiDg __________________________. ___________ ________________ Trad. Exam. 4 Bright red ashingentExample 18 Light good Trad. Exam. 5 Bright red astlingent Example 19 Light good Trad.Exam.6 Bri8ht redastringent Example 20 Light 80~d Example 14 Light good Ex~mple 21 Light good 1 0 Example IS Light good Example 22 Light good Example 16 Light good Example 23 Light good Example 17 Light good Example 24 Light good ____ _ ____ _____ _ _____ ____ _____ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _____ Example 25.
l S 80 pieces of areca quit made from example 23 are crushed, dried and grounded into powder. 130 g of chicle gum, 215 g of powder sugar and 25 g of malt are molten and mixed in a pot.
The prepared dry powder is added to the molted compound 1 g of mint.
After mixing, rolling, extruding, und cutting, a chewing gum product 2 0 with a si~e of 2 x 7.5 x 2 cm is finally manufactured.
Example 26.
50 pieces of areca quid made from example 19 are crushed and grounded. They are then added into a pot where a transparent molten product exists, which is made from dissolving 6 g of starch, 100 g of 2 5 sugar, 100 g of malt and 30 g of water, and mixed at IOO~IOS C.
At the conditions of concentration at 90 % and temperature at 110 C, lS
g of butter is added, and the operation of heating and mixing is continued. When the temperature of product reaches 120 C, the betel product is slowly added. The mixing is then speeded up, at 110 C, until 3 0 the water content reaches at 8 %. The the candy containing areca is then produced by steps of pulling, rolling, cutting and packing.
Example 27.
35 g of sugar, 6 g of millet jelly and 1 g of sodium alginate are dissolved into a 310 g of milk at 60 C. 35 g of powder areca are added, homogenized, 3 S packed in a can, and, finally, heat treated at 105 C for 20 minutes. The drink containing areca component is made.
Example 28.
30 g of areca seed are crushed and grounded into mud. It is then added into a pot where 200 g of egg are splashed by an egg mixer. The 20 g of ~83~ 98 power sugar and 1 g of lemon essence are added. Mixing continues for awhile, with 50 g of wheat powder and 50 g of starch being added and mixed. The resulting mass is formed into a size of thick 5 mm, length 4 cm nnd width 5 cm on a oven plate where a layer of salad oil is spread. A little 5 milk is sprayed on . it, and baked at 190 C for 20 minutes in order to manufacture a biscuits containing areca component.
Example 29.
400 g areca are crushed, being extracted with 500 g of water at 90 C for 20 minutes. 30 g of soybean lees is added. The solution is filtered after 10 mixing for 10 minutes.
10 g of alcohol, 180 g of sugar, 120 g of glucose, 2 g of phosphoric acid, 0.8 g of lemon essence and 3000 g water are mixed with the filtrate.
The resulting solution is degassed and filled with CO2 gas at the conditions of 40 C and at 70 Ib pressure with a carbonator. It is then 15 packed into a 250 ml bottle and capped.
Experimentnl testing 4.
The products produced from Examples from 25 to 29 are respectively tasted by a group of S persons for each food.
The products are all shown to be non astringent and good tasting and 2 0 the people feel well feeling.
The form of this invention herein shown and described is understood to be taken as a preferred example of the same. Various changes in the shape, size and arrangement of parts may be resorted to without departing from the spirit of this invention or the scope of the subjoined 2 5 claims.
Other and further objects, features and advantages of the invention will nppear more from the following description.
DETAILED DESCRIPTIOND
15 A series of eatable compounds for preparation areca food additive, which have an excellent effect for reaction with polyphenolic compounds, has been devised by the inventor. This series of eatable compounds is superior to the traditional lime compound and could improve all the present disadvantages in areca food.
2 0 The eatable foods include; salts of calcium organic acid, such as calcium formate, calcium fumarate, calcium glautamete, calcium glycerophosphate, culcium lactate, calcium malate, calcium maleate, calcium succinate, calcium tartrate, calcium citrate and calcium glutamate; food which contains at least one of the following functional 25 groups selected from the group consisting of -NH2, =NH, ..N, -NH-, -CONH-, -HCO-, -CO-, -COOR-, -S-, and their salts; particularly, protein, hydrolyzed products of protein and foods containing protein.
Specific examples which contain the functionnl group selected from the group consisting of -NH2, =NH, I.N,-NH-,-CONH-,-HCO-,-CO-, -COOR-, 3 0 -S- are pure proteins, such as hemialbumin, albumin, histone, gelatin, protamine, albuminoid; complex proteins, such as nucleoproteid, glycoproteid, phosphoproteid and liporoteid; derivative proteins, such as m-protein and peptone; hydrolyzed protein, such as gelatine, polypeptide and amino acid; and their mixture compounds.
3 5 The special examples which contain -CONH- group are fibroin, keratin, and low molecule weight of nylon. The special examples which contain -HCO-, -CO- are reducing compounds, such as rhamnose, galactose and lactose. The special examples contain -COOR- are synthetic polyethers, such as methly cellulose, Tweens, and poly-N-vinyl-pyrolidine.
Most of the compounds previously mentioned could be produced from foods, including foods of vegetable and animal. These the foods, especially those containing protein or amino acids, show good properties for reaction of polyphenolic compounds. The properties are based on the quantity of protein and/or amino acid of which they are borne. These discoverings are very useful to this invention. The vegetables including various kind of grain foods, seeds, and their products, such as soy bean, green bean, nzuki bean, peanut, germs, soy bean crude, sesame seed, hemp seed, natto, kidney bean, radish, walnut; and animal foods, such as milk, sea foods, egg, tissues of animals, yeast, meat all belong to food.
The compounds for the areca food additive would be better in a state of fine particle in order for an effect of reaction.
The modifier to be used in areca food additive is selected from the group consisting of sweeteners, perfumes, preservers, stabili~ers, color pigments, herbs and fillers. They are compounds of sweeteners such as honey, maltose, sugar, fructose, glycyrrhizin, saccrin, d-sorbital and d-mannitol; perfumes, such as mint and essential oils; preservatives, such as benzoate, sodium benzoate, calcium propinate, sorbitar, dehydroacetic acid and its salts, sorbic acid; stabilizers, such as CMC, pectin, arabic gum, 2 0 and locust bean gum; color pigment, such as chlorophyll and green No. I;
Chinese herbs, such as licorice root, cinnamon, coffee and cocoa. They are used in a favorable amount and according to the food regulations.
The compounds and their amounts for the requirement of reaction with polyphenolic compounds of areca quid are not strictly confined to 2 5 one kind of compounds and a specific amount. They, however, depend on the quantity of total polyphenolic compounds contained. The equivalent of chemical reaction is usually greater than the equivalent of polyphenolic compounds. The composition of crude drug depends on the season of their harvests and the degree of reap. Their content of 3 0 polyphenolic compounds then varies over a wide range.
7 ~33% of d-catechin and 22~50% of gambir tanning contained in gambir exist. The seed of area bears approximately 40% of the polyphenolic compounds in green and is reduced to appro?cimately 20%
after ripening. The fruit of areca has only 2~8%. The stem, fruit and leaf 3 5 of areca betel, respectively, bears 2~5%, 1~3%, and 1~2% in weight of polyphenolic compounds.
The preparation method of areca food is not limited to using fresh crude drugs. That methvd also uses the crude drugs which can be grounded into powder or into a state of paste; can be extracted for s ~3g3~
components by water or organic solvents, such as hexane, alcohol and ether, to remove the fibre; and can be separated the effective components from the extracts.
The areca food additive may be in the form of paste, powder in package, 5 solid produced from drying the paste, and in liquid.
The areca food additive compounds with foods and other crude drugs, stabilizers, pigments, preservative agents, perfumes and sweeteners in the proper quantity in order to form a state of chewing gum, cake, biscuits, lozengers, beverages or candy. That is good for packing and 1 0 storage.
The invention will be understood more readily with reference to the following examples. These examples, however, are intended to illustrate the invention and are not be meant to limit the scope of the invention.
Traditional art examples 1.
After dissolving 0.04 g of pictin in 14 g of water, 0.02 g of benzoic acid, 0.4 g of cinnamon, 10 g of honey and 8 g of gambir are added into the solution, and pasted by homogenizer to form a areca food additive.
Traditional art example 2.
The same example as traditional art example 1, except 8 g of lime, is 20 compounded in it.
Traditional example 3.
The same example as traditional art example 1, except 10 g of calcium carbonate, is compound in it.
Example 1.
2 5 The same example as traditional art example 1, except 12 B of casein powder, is compounded in it.
Example 2.
After dissolving 0.08 g of arabic gum in 30 g of water, 0.006 g of benzoic acid, 0.02 g apple essence, I g of sugar and 24 g of radish powder are 3 0 added into the solution in turn, and pasted by a homogenizer to form a areca food additive.
Example 3.
After dissolving 0.0~ g locust bean in 30 g of water, 0.2 g of sodium propinate, 0.02 g of peppermint, 12 g of molasses and 12 g soybean lees 3 5 powder are added into the solution in turn, and pasted by a homogenizer to form a areca food additive.
Example 4.
After dissolving 0.04 g of ester of p-hydroxybenzoic acid in 16 g of water, 0.2 g of D-mantol, 8 g of gambir and 14 g of glutathione are added 2.~8~
into the solution, and pasted by a homogenizer in order to form a areca food additive.
Example 5.
2 g of Aspartame, 10 g of m-protein and 8 g oî water are pasted by a S homogenizer to form a areca food additive.
Example 6.
20 g of water, 6 g of gambir, 8 g of soybean powder and 8 g of soybean Iees powder are pasted by a homogenizer in order to form a areca food additive.
Example 7.
40 g of bean paste, 10 g of rice bran, 8 g of soybean lees powder and 0.08 g of DHA(dehydroacetic acid) are pasted by a homogenizer in order to form a areca food additive.
Example 8.
60 g of fermented bean curd are pasted by a homogenizer in order to form a areca food addi~ive.
Example 9.
60 g of fermented bean curd, 20 g of sugared bean and 8 g of coffee powder are pasted by a homogenizer in order to form a areca food 2 0 additive.
Example 10.
16 g of honey and 20 g green bean are pasted by a homogenizer in order to form a areca food additive.
Example 1 1.
After dissolving 0.04 g of DHA in 20 g of water, 6 g of honey, 6 B of lave and 16 g milk powder ure pasted by a homogenizer in order to form a areca food additive.
Example 12.
After dissolving 6 B of gelatine in 40 g of water, 0.8 g alcohol, 0.2 g of 3 0 cinnamon, 10 g of gambir and 8 g of fish powder are pasted by a homogenizer to form a areca food additive.
Example 13.
2 g of Aspartume and 20 g of calcium glycerophosphate are pasted in 20 g of water by a homogenizer in order to form a areca food additive.
3 5 Experimental testing 1.
All the pastes of areca food additives products made in traditional art examples ~rom 1 to 3. Examples from 1 to 13 are respectively divided into 20 equal parts.
Each kind of pastes 4 parts are respectively, as previously done, into a 100 ml beaker. A volume of 70 ml of water is added into each beaker and mixed with a mixer for 10 minutes. The mixture is filtered and the color of solution i9 recorded. The free amount of polyphenolic compounds are S analyzed and the results are shown in Ta~le 1.
Table 1 Item color of amount of Item color of llmount 10solution polyphcnol solution polyphenol Tra~ Exam. I Bnght red much Exumple 6 Light none Trad. Exsm. I Bright redmuch Example 7 Light none Trad. Exam. I BrJght redmuch Example 8 Light none Example I Light noneExample 9 Light none Example 2 Light noneExample 10 Light none Exnmple 3 Light . noneExample 11 Light none Ex~nple 4 Light noneExample 12 Light none Example S Light noneExample 13 Light none ____________________________________._____________________ ______ The color of solutions made from the invention are obviously all not shown in a bright red color like those of the traditional art examples. No free polyphenolic compounds being detected from the solutions of the 2 5 invention existed..
Traditional art example 4.
15 pieces of Taiwan areca, the average weight being 4 g, are cracked from longitudinal side in half way. Put one part of paste of areca food additive made from traditional art example I in the crack, and a chop of 3 0 betel fruit i9 mounted on the paste, respectively.
Traditional art example 5.
The same as traditional art example 5, except for the paste of areca food additive, is done by using the one made from traditional art example 2.
Traditional art exnmple 6.
3 5 The same as traditional art example 4 ,except for the paste areca food additive, is done by using the one made from traditional art example 3.
Example 14.
The same as traditional art example 4 except the paste of areca food additive is using the one made from example 1.
3 ~ ~ ~
Example 15.
15 pieces of betel leave, which have an average weight of 2.8 g, are spread one part of pastes from an areca food additive made from an example on the up side and wrapped up a piece of Taiwan areca of S approximately 4 g weight, respectively, to form an areca quid.
Example 16.
The paste made from example 3 is mixed with 10 g of tobacco and is divided into 20 parts. IS pieces of Taiwan betel leave, having an average weight of 2.8 g, a}e spread with one part of pastes of areca food additive 10 as previously made, and a piece of Taiwan areca is respectively wrapped up in order to produce areca quids.
Example 17.
15 pieces of Taiwan areca, having an average weight of 8 g, are cracked from a longitudinal side in a half way. One part of paste of areca l S food additive made from example 4 is put in the crack. A chop of 0.7 g of betel fruit is respectively added onto it. The areca quids are then produced.
Example 1 8.
The same as exarnple 17, except the average weight of areca is 4 g and 2 0 the pastes of areca food additive are using the ones made from example 5.
Example 19.
The same as exumple 18, except the pastes of areca food additive are made from example 6.
Example 20.
25 The same as example 15, except the average weight of betel leave is 2.1 g and the paste of areca food additive is made from example 7.
Example 2 1.
The same as example 20, except an average weight of l.S g of Taiwan areca seed is instead of betel fruit, and the paste of areca food additive is 3 0 made from example 8.
Example 22.
The same as example 17, except the average weight of areca is 4.2 g, and 0.3 g of betel stem instead of the betel fruit and the paste of a}eca food additive is made from example 9.
3 S Example 23.
The same as example 18, except the average weight of areca is 4.1 g, the paste of areca food additive is made from example 11 and the betel fruit is l.S g instead.
Example 24.
g 2~3~8 The same as example 17, except the average weight of areca is 8.1 g, thc paste of areca food additive is made from example 12 and the betel fruit is 1 g.
Experimental testing 2.
5 Taking IS pieces of product out of each of the comparison, examples from 4 to 6 and examples from 14 to 24, are crushed by crush the machine and 200 ml of water is respectively added into n 300 ml beaker mixing for 10 minutes. The procedure as described in experimental testing I is to be followed with the results being shown in Table 2.
Table 2 Itcm color of amount Or Item color ot ~mount solution polyphenol solutlon polyphenol ___________________________ ___________________________ l S _Trad. Exam. 4 Bright red much Example 18 Light none Trad. Exam. 5 Bright red much Example 19 Light none Trad. Exam. 6 Bright red much Example 20 Light none Example 14 Light none Example 21 LiBht none Example 15 Light none Example 22 Light none 2 0 Example 16 Light none Example 23 Light none Exarnple 17 Light none Example 24 Light none __________________________________________________.______________ The products made by present invention are obviously similar to 2 5 results as shown in experimental testing 1. The traditional ones are, meanwhile, shown in bright red in the solution with much of the free polyphenolic compounds having remained.
Experimental testing 3.
The taste testings are performed by distribution of one piece of S quids 3 0 as produced from each of traditional art examples from 4 to 6 and examples from 14 to 24, to one of S persons for chewing, respectively.
The color of chewing liquid and taste are recorded. The results are shown in Table 3.
2 ~
T~lble 3 ___________,_______ _____.___._____________________________________ Item color or ta~tc o~ Itcm ~olor of taste of solution chewing ~41ut~on chcwiDg __________________________. ___________ ________________ Trad. Exam. 4 Bright red ashingentExample 18 Light good Trad. Exam. 5 Bright red astlingent Example 19 Light good Trad.Exam.6 Bri8ht redastringent Example 20 Light 80~d Example 14 Light good Ex~mple 21 Light good 1 0 Example IS Light good Example 22 Light good Example 16 Light good Example 23 Light good Example 17 Light good Example 24 Light good ____ _ ____ _____ _ _____ ____ _____ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _____ Example 25.
l S 80 pieces of areca quit made from example 23 are crushed, dried and grounded into powder. 130 g of chicle gum, 215 g of powder sugar and 25 g of malt are molten and mixed in a pot.
The prepared dry powder is added to the molted compound 1 g of mint.
After mixing, rolling, extruding, und cutting, a chewing gum product 2 0 with a si~e of 2 x 7.5 x 2 cm is finally manufactured.
Example 26.
50 pieces of areca quid made from example 19 are crushed and grounded. They are then added into a pot where a transparent molten product exists, which is made from dissolving 6 g of starch, 100 g of 2 5 sugar, 100 g of malt and 30 g of water, and mixed at IOO~IOS C.
At the conditions of concentration at 90 % and temperature at 110 C, lS
g of butter is added, and the operation of heating and mixing is continued. When the temperature of product reaches 120 C, the betel product is slowly added. The mixing is then speeded up, at 110 C, until 3 0 the water content reaches at 8 %. The the candy containing areca is then produced by steps of pulling, rolling, cutting and packing.
Example 27.
35 g of sugar, 6 g of millet jelly and 1 g of sodium alginate are dissolved into a 310 g of milk at 60 C. 35 g of powder areca are added, homogenized, 3 S packed in a can, and, finally, heat treated at 105 C for 20 minutes. The drink containing areca component is made.
Example 28.
30 g of areca seed are crushed and grounded into mud. It is then added into a pot where 200 g of egg are splashed by an egg mixer. The 20 g of ~83~ 98 power sugar and 1 g of lemon essence are added. Mixing continues for awhile, with 50 g of wheat powder and 50 g of starch being added and mixed. The resulting mass is formed into a size of thick 5 mm, length 4 cm nnd width 5 cm on a oven plate where a layer of salad oil is spread. A little 5 milk is sprayed on . it, and baked at 190 C for 20 minutes in order to manufacture a biscuits containing areca component.
Example 29.
400 g areca are crushed, being extracted with 500 g of water at 90 C for 20 minutes. 30 g of soybean lees is added. The solution is filtered after 10 mixing for 10 minutes.
10 g of alcohol, 180 g of sugar, 120 g of glucose, 2 g of phosphoric acid, 0.8 g of lemon essence and 3000 g water are mixed with the filtrate.
The resulting solution is degassed and filled with CO2 gas at the conditions of 40 C and at 70 Ib pressure with a carbonator. It is then 15 packed into a 250 ml bottle and capped.
Experimentnl testing 4.
The products produced from Examples from 25 to 29 are respectively tasted by a group of S persons for each food.
The products are all shown to be non astringent and good tasting and 2 0 the people feel well feeling.
The form of this invention herein shown and described is understood to be taken as a preferred example of the same. Various changes in the shape, size and arrangement of parts may be resorted to without departing from the spirit of this invention or the scope of the subjoined 2 5 claims.
Claims (13)
1. An areca food additive mainly comprises of:
(1). at least one components selected from the group consisting of calcium salt of organic acid and food which contains at least one of the following functional groups selected from the group consisting of -NH2, =NH, .N, -NH-, -CONH-, -HCO-, -CO-, -COOR-, -S-, and their salts;
particularly, protein, hydrolyzed products of protein and foods containing protein; and without/or with (2). at least one components selected from the group consisting of crude drugs, such as gambir, tobacco; modifiers, such as sweetener, preservative agent, stabilizer, perfume, Chinese herb and pigment;
(1). at least one components selected from the group consisting of calcium salt of organic acid and food which contains at least one of the following functional groups selected from the group consisting of -NH2, =NH, .N, -NH-, -CONH-, -HCO-, -CO-, -COOR-, -S-, and their salts;
particularly, protein, hydrolyzed products of protein and foods containing protein; and without/or with (2). at least one components selected from the group consisting of crude drugs, such as gambir, tobacco; modifiers, such as sweetener, preservative agent, stabilizer, perfume, Chinese herb and pigment;
2. As claimed in claim 1 the calcium salts of organic acid are selected from the group consisting of calcium formate, calcium fumarate, calcium glycerophosphate, calcium lactate, calcium malate, calcium maleate, calcium succinate, calcium tartrate, calcium citrate and calcium glutamate.
3. As claimed in claim I the protein, derivatives of protein and food containing protein are selected from the group consisting of pure proteins, such as albumin; complex proteins, such as nucleoproteid, glycoproteid; derivative proteins, such as m-protein and peptone;
hydrolyzed protein, such as gelatin, polypeptide and amino acid; the special examples which contain -CONH- group, such as fibroin, and low molecule weight of nylon; the special examples which contain -HCO-, -CO-are reducing compounds, such as rhamnose; the special examples which contain -COOR- are synthetic polyethers, such as Tweens; foods including vegetable foods of various kind of grain foods, seeds, and their products, such as soy bean, azuki bean, soy bean crude, radish; and animal foods, such as milk, egg, tissues of animals.
hydrolyzed protein, such as gelatin, polypeptide and amino acid; the special examples which contain -CONH- group, such as fibroin, and low molecule weight of nylon; the special examples which contain -HCO-, -CO-are reducing compounds, such as rhamnose; the special examples which contain -COOR- are synthetic polyethers, such as Tweens; foods including vegetable foods of various kind of grain foods, seeds, and their products, such as soy bean, azuki bean, soy bean crude, radish; and animal foods, such as milk, egg, tissues of animals.
4. As claimed in claim 1 the modifiers are selected from the group consisting of sweeteners, perfumes, preservers, stabilizers, color pigments, herbs and fillers, they are compounds of sweeteners such as honey, maltose, sugar, fructose, glycyrrhizin, saccrin, d-sorbital and d-mannitol; perfumes, such as mint and essential oils; preservatives, such as benzoate, sodium benzoate, calcium propinate, sorbitar, dehydroacetic acid and its salts, sorbic acid; stabilizers, such as CMC, pectin, arabic gum, and locust bean gum; color pigment, such as chlorophyll and green No.1;
Chinese herbs, such as licorice root, cinnamon, coffee and cocoa.
Chinese herbs, such as licorice root, cinnamon, coffee and cocoa.
5. Areca quid mainly comprises of the composition of areca or areca seed, and areca food additive; it may be with other components selected from the group consisting of betel leave, betel fruit, Chinese herb, and betel stem.
6. Foods containing areca component comprise the traditional art food with the component of areca and the areca food additive in the state of homogeneously; the polyphenolic compounds of the crude drug completely react with the areca food additives.
7. Foods containing areca component comprise the traditional art food with the component of areca in the state of homogeneously; in which the polyphenolic compounds of said areca component was removed in advance by the treatment of areca food additive.
8. Production of food containing areca component comprises of homogeneously mixing the traditional art food with the component of areca and the areca food additive; the polyphenolic compounds of the crude drug are completely react the with food .
9. As claimed in claims 6, 7 and 8, the areca component is selected from a group consisting of powder of areca, powder of areca seed, paste of areca, paste of areca seed, extracts of areca or areca seed by water or organic solvent, and the effective compound separated from the extracts.
10. As claimed in claims 6, 7 and 8, the food containing areca component is selected from the group consisting of candy, cake, biscuits, chewing gum, beverages and lozenges.
11. A new food additive, substantially as herein described.
12. A new food, substantially as herein described.
13. A new method of preparing food, substantially as herein described.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
LK1036192 | 1992-02-24 | ||
LK10361 | 1992-02-24 |
Publications (1)
Publication Number | Publication Date |
---|---|
CA2083198A1 true CA2083198A1 (en) | 1993-08-25 |
Family
ID=19720960
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002083198A Abandoned CA2083198A1 (en) | 1992-02-24 | 1992-11-18 | Areca food additives and its foods |
Country Status (2)
Country | Link |
---|---|
CA (1) | CA2083198A1 (en) |
IN (1) | IN175198B (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1050609C (en) * | 1994-06-01 | 2000-03-22 | 何家庆 | Biochemical method for preparing glucomannan from fresh Amorphophallus rivieri |
WO2003061399A1 (en) * | 2002-01-25 | 2003-07-31 | De Abhijit | Chewing gum composition and a process for preparing the same |
CN103704715A (en) * | 2013-10-18 | 2014-04-09 | 宋交愚 | Additive composition for mixing in dry betel nut fruit, preparation thereof, selenium-rich dry betel nut fruit and selenium-rich dry betel nut fruit processing method |
EP4129982A4 (en) * | 2020-03-27 | 2023-08-09 | Shenzhen Icybetel Biological Technology Co., Ltd | Areca nut-flavored product |
-
1992
- 1992-10-15 IN IN744CA1992 patent/IN175198B/en unknown
- 1992-11-18 CA CA002083198A patent/CA2083198A1/en not_active Abandoned
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1050609C (en) * | 1994-06-01 | 2000-03-22 | 何家庆 | Biochemical method for preparing glucomannan from fresh Amorphophallus rivieri |
WO2003061399A1 (en) * | 2002-01-25 | 2003-07-31 | De Abhijit | Chewing gum composition and a process for preparing the same |
CN103704715A (en) * | 2013-10-18 | 2014-04-09 | 宋交愚 | Additive composition for mixing in dry betel nut fruit, preparation thereof, selenium-rich dry betel nut fruit and selenium-rich dry betel nut fruit processing method |
CN103704715B (en) * | 2013-10-18 | 2015-05-06 | 宋交愚 | Additive composition for mixing in dry betel nut fruit, preparation thereof, selenium-rich dry betel nut fruit and selenium-rich dry betel nut fruit processing method |
EP4129982A4 (en) * | 2020-03-27 | 2023-08-09 | Shenzhen Icybetel Biological Technology Co., Ltd | Areca nut-flavored product |
Also Published As
Publication number | Publication date |
---|---|
IN175198B (en) | 1995-05-20 |
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