CA2025937A1 - Beta type zeolithe and process for its preparation - Google Patents

Beta type zeolithe and process for its preparation

Info

Publication number
CA2025937A1
CA2025937A1 CA2025937A CA2025937A CA2025937A1 CA 2025937 A1 CA2025937 A1 CA 2025937A1 CA 2025937 A CA2025937 A CA 2025937A CA 2025937 A CA2025937 A CA 2025937A CA 2025937 A1 CA2025937 A1 CA 2025937A1
Authority
CA
Canada
Prior art keywords
beta type
zeolithe
preparation
zeolite
xsio2
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA2025937A
Other languages
French (fr)
Other versions
CA2025937C (en
Inventor
Philippe Caullet
Jean-Louis Guth
Anne-Catherine Faust
Francis Raatz
Jean-Francois Joly
Jean-Marie Deves
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies Nouvelles IFPEN
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2025937A1 publication Critical patent/CA2025937A1/en
Application granted granted Critical
Publication of CA2025937C publication Critical patent/CA2025937C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7007—Zeolite Beta
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/26—After treatment, characterised by the effect to be obtained to stabilize the total catalyst structure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/42—Addition of matrix or binder particles

Abstract

A synthetic crystalline zeolite of beta type, characterised by: a) the following approximate general formula: M2/nO.Al2O3.xSiO2 where M denotes a proton and/or a metal cation n is the valency of M x is a number between 5 and 800, b) an X-ray diffraction pattern shown in Table I of the description, and c) a fluorine content of between approximately 0.005 and 2.0 % by weight, the said zeolite having been additionally synthesised in a fluoride medium. s
CA002025937A 1989-09-22 1990-09-21 Beta type zeolithe and process for its preparation Expired - Fee Related CA2025937C (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR89/12.556 1989-09-22
FR8912556A FR2652347B1 (en) 1989-09-22 1989-09-22 BETA TYPE ZEOLITE AND ITS PREPARATION PROCESS BY PHILIPPE CAULLET, JEAN-LOUIS GUTH, ANNE-CATHERINE FAUST, FRANCIS RAATZ, JEAN-FRANCOIS JOLY AND JEAN-MARIE DEVES.

Publications (2)

Publication Number Publication Date
CA2025937A1 true CA2025937A1 (en) 1991-03-23
CA2025937C CA2025937C (en) 2000-09-05

Family

ID=9385808

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002025937A Expired - Fee Related CA2025937C (en) 1989-09-22 1990-09-21 Beta type zeolithe and process for its preparation

Country Status (8)

Country Link
EP (1) EP0419334B1 (en)
JP (1) JPH03122009A (en)
AT (1) ATE99648T1 (en)
CA (1) CA2025937C (en)
DE (1) DE69005757T2 (en)
DK (1) DK0419334T3 (en)
ES (1) ES2050400T3 (en)
FR (1) FR2652347B1 (en)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2670772B1 (en) * 1990-12-21 1993-04-09 Inst Francais Du Petrole MTW TYPE ZEOLITE AND PROCESS FOR PREPARING THE SAME.
ATE143652T1 (en) * 1991-11-20 1996-10-15 Dow Chemical Co METHOD FOR GROWING CRYSTALLINE, MICROPOROUS SOLIDS IN A FLUORDIC, ESSENTIALLY NON-AQUEOUS GROWTH MEDIUM
US5389358A (en) * 1993-07-16 1995-02-14 W. R. Grace & Co.-Conn. Zeolite GZS-11 and its dynamic preparation process
EP0766646B1 (en) * 1994-05-10 1998-04-15 Shell Internationale Researchmaatschappij B.V. Process for preparing a large pore molecular sieve
AU2549295A (en) * 1995-03-17 1996-10-08 Chevron U.S.A. Inc. Preparation of zeolites using organic template and amine
DE69613587T2 (en) * 1995-10-13 2002-04-25 K U Leuven Res & Dev Leuven CHIRAL SOLID CATALYST, ITS PRODUCTION AND ITS USE FOR PRODUCING PRACTICAL ENANTIOMER-PURE PRODUCTS
ES2133042B1 (en) * 1996-03-14 2000-05-16 Univ Valencia Politecnica SYNTHESIS OF ZEOLITE AND ISOMORPHIC ZEOTYPES TO ZEOLITE BETA.
US6294150B2 (en) 1997-11-07 2001-09-25 Ngk Insulators, Ltd. Highly heat resistant β-zeolite and absorbent for automobile exhaust gas purification and adsorbent for automobile exhaust gas purification
JP3986186B2 (en) * 1997-11-07 2007-10-03 日本碍子株式会社 High heat-resistant β-zeolite and adsorbent for automobile exhaust gas purification using the same
ES2152143B1 (en) * 1998-02-06 2001-08-16 Univ Valencia Politecnica SYNTHESIS OF ZEOLITES AND ZEOTYPES OF LARGE PORE.
ES2155797B1 (en) * 1999-07-29 2001-12-01 Univ Valencia Politecnica ZEOLITA ITQ-10
CA2581309C (en) 2004-11-12 2010-05-25 Marcus Breuninger Method for the synthesis of zeolite beta with diethylenetriamine
JP4992214B2 (en) * 2005-09-16 2012-08-08 東ソー株式会社 Nitrogen oxide purification catalyst comprising β-type zeolite and nitrogen oxide purification method using the same
JP5124927B2 (en) * 2005-09-16 2013-01-23 東ソー株式会社 Hydrocarbon adsorption / removal agent comprising β-type zeolite and hydrocarbon adsorption / removal method using the same
FR2914636B1 (en) 2007-04-05 2009-06-26 Inst Francais Du Petrole PROCESS FOR THE PREPARATION OF A BETA ZEOLITHE
JP5549839B2 (en) * 2008-08-19 2014-07-16 東ソー株式会社 High heat-resistant β-type zeolite and SCR catalyst using the same
FR2978449A1 (en) 2011-07-28 2013-02-01 IFP Energies Nouvelles OLIGOMERIZING HYDROCRACKING PROCESS USING A CATALYST BASED ON DISPERSEE BETA ZEOLITHE
KR101627953B1 (en) 2012-02-21 2016-06-07 엑손모빌 케미칼 패턴츠 인코포레이티드 Molecular sieve material, its synthesis and use
EP3209606B1 (en) * 2014-10-24 2020-04-29 Chevron U.S.A. Inc. Molecular sieve ssz-102 and synthesis thereof
WO2022047374A1 (en) * 2020-08-31 2022-03-03 Purdue Research Foundation Mfi zeolites using dabco and methylamine reagents

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3308069A (en) * 1964-05-01 1967-03-07 Mobil Oil Corp Catalytic composition of a crystalline zeolite
US4061717A (en) * 1974-10-03 1977-12-06 Mobil Oil Corporation Directed crystallization of synthetic aluminosilicates
DE3167118D1 (en) * 1980-12-19 1984-12-13 Ici Plc Zeolites
US4554145A (en) * 1984-04-16 1985-11-19 Mobil Oil Corporation Preparation of crystalline silicate zeolite Beta

Also Published As

Publication number Publication date
DE69005757D1 (en) 1994-02-17
DE69005757T2 (en) 1994-04-28
DK0419334T3 (en) 1994-05-16
FR2652347B1 (en) 1992-01-10
EP0419334A1 (en) 1991-03-27
ES2050400T3 (en) 1994-05-16
CA2025937C (en) 2000-09-05
EP0419334B1 (en) 1994-01-05
FR2652347A1 (en) 1991-03-29
JPH03122009A (en) 1991-05-24
ATE99648T1 (en) 1994-01-15

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Legal Events

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EEER Examination request
MKLA Lapsed