CA1288541C - Dental application fluid for the inspection of tooth contacts and prosthetic works - Google Patents

Dental application fluid for the inspection of tooth contacts and prosthetic works

Info

Publication number
CA1288541C
CA1288541C CA000512748A CA512748A CA1288541C CA 1288541 C CA1288541 C CA 1288541C CA 000512748 A CA000512748 A CA 000512748A CA 512748 A CA512748 A CA 512748A CA 1288541 C CA1288541 C CA 1288541C
Authority
CA
Canada
Prior art keywords
fluid
application fluid
application
cited
weight percent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CA000512748A
Other languages
French (fr)
Inventor
Jens M. Hansen
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
PRODENT GES fur ZAHNMED BEDARFSARTIKEL MBH
Original Assignee
PRODENT GES fur ZAHNMED BEDARFSARTIKEL MBH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE19843403118 external-priority patent/DE3403118A1/en
Application filed by PRODENT GES fur ZAHNMED BEDARFSARTIKEL MBH filed Critical PRODENT GES fur ZAHNMED BEDARFSARTIKEL MBH
Priority to CA000512748A priority Critical patent/CA1288541C/en
Application granted granted Critical
Publication of CA1288541C publication Critical patent/CA1288541C/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Landscapes

  • Dental Preparations (AREA)

Abstract

ABSTRACT OF THE DISCLOSURE
There is disclosed a dental application fluid for prosthetic work that is a directly applicable fluid, which, in contrast to known silicon-based compounds, requires no prior preparation by means of a catalyst. The product is non-viscous and may be applied and distributed without difficulty by means of forceps and a ball of cotton. The application fluid drys fast;
the drying time equals only about 5 to 10 seconds and can even be shortened with the use of a hand blower. The application fluid adheres to all materials which are used in the dental profession including tooth materials. The application fluid thereby allows an unusually exact determination of pressure and contact points.
The marking of contacts and early contacts is very distinct. The application fluid is easily and economically measured out, because of its non-viscous consistency and composition. A significantly greater number of crown coatings is therefore achieved in contrast to occlusion sprays (improvement equals about 350%). The fluid is neither toxic nor does it irritate the pulp. After use, the appli-cation fluid is quickly and well-removed from the teeth, crowns and the like with a solvent fluid. String formation and clumping, because of contact with saliva, do not occur during use. Such a dental application fluid is directly applicable, non-viscous fast drying and comprises: (a) 0.5 to 10 parts by weight of an organic polymer adhesive, (b) 35 to 65 parts by weight of a massive component, (c) 0.1 to 10 parts by weight of a coloured pigment and (d) 30 to 70 parts by weight of a physiologically harmless alcoholic fluid, components (a), (b) and (c) being dis-solved or respectively dispersed in fluid (d).

Description

354~

DENTAL APPLICATION FLUID FOR THE
INSPECrION OF TOOTH CONTACTS
AND PROSTHETIC WORKS

The invention relates to a new application fluid for dental purposes . The invention may be used by dentists ~ dental tech-nicians, and other dental heslth care professionals to determine and check occlusions ~contact points), and to form and control approxi-mate contacts and prosthetic works, including inlays, crowns, bridges and the like. The invention may be particularly used for controlling and producing an exact fit for all fixed prosthetic works.
It is known to use a silicon-based compound, which may be packed in tubes, for checking and producing the precision of fit of fixed prosthetic works. The known compound is mi~ed with a catalyst on a neutral background, such as a glass plate or graduated block. The known eompound is then usually introduced into the crown as a viscous, elasti~ mass by means of ~ spatulR.
Subsequently, the crown is set on the stump and pressed tightly.
After a setting time of about seven minutes, the application com-pound becomes hard. This available silicon-based compound requires a considerable expenditure of time and labor in its application;
moreover~ the available compound is only difficultly measured out.
Occlusion papers, in the form of larger film sheets, or in the form of bQnds of àiffering color have been proposed for the
2 5 inspection and formation of approxim~te ~ontacts in the occlusion .
The colors of these film$ should represent their strength ~ - .

: ' ' .: ~ ' 354~

( thickness) . Thick films are used for the rough formation of occlusion points and thinner films are used for finely shaping the occlusion points and articulation points ( i . e ., those points in con-tact during lateral and advancing movements of the jaw). Contact points may be determined and inspected by biting down on the teeth and by means of articulation movements. However, occlusion papers of this kind are unsuited for the production and inspection of prosthetic works.
Furthermore, so-called occlusion WAXeS, available in the form of small plates, are known and have been proposed for the bite (abduction), that is, the occlusion. These occlusion waxes are suited neither for the determination of articulation move~.ents nor for the production and inspection of prosthetic works.
In addition, so-called occlusion sprays with a powdered consistency are known which msy be dispensed from a spray can.
The granularity of the powder is between 10 and 20 micrometers.
Even though occlusion sprays of this kind offer distinct advantages in use, they also have a series of disadvant~ges. It is hardly possible with occlusion sprays of this kind to achieve an even 2 o distribution, because the applicstion would then be too thick .
- Additionally, these powders lack sufficient adhesive strength on metal, which leads to the résult that, even though the powders adhere to the tooth stump, they show insufficient adhesion to the prosthetic metal parts. For this reason, the pressure points may 2 5 only be very inaccurately determined because the powder already loses its adhesiveness after the slightest contact, and is therefore only actually usable with extremely early contacts. A further disadvantage is that the powder becomes stringy and forms lumpy deposits after the unavoidable contect with saliva, and is thereafter unusable. The occlusion spray is not particularly well removed with water. The powder gives off much dust when applied, so that fingers, hands, and even the local environment are heavily con-taminated .

... .

" ''~ '' . ' , ' .
. - ~ . .

354~

SUMMARY OF THE INVENTION
.
It is an object of the invention to provide an application compound which is ready to use and therefore directly Rpplicable, non-Yiscous, fast-drying, and strongly adhesive to metal as well as tooth material. The application compound should be sensitive to contact, easily measured out, compatible with saliva, and yet easily removable. The handling and application of the compound should af~ord the most economical expenditure of material possible.
This compound should be suitable for the control and ~ inspection of tooth contacts and prosthetic works for all of the above reasons.
To achieve this object, the invention proposes an applica-tion fluid which comprises a directly applicable, non-viscous, quick-drying compound, in which an organic 9 polymeric adhesiYe, Q
massive component, and a colored pigment, are dispersed or dissolved in an alcoholic solvent.
The application fluid according to the invention is a directly applicable fluid, which, in contrast to the above-mentioned silicon-based compounds, requires no prior preparation by means of 2 0 a catalyst The product is non-viscous and may be applied and distributed without difficulty by means of forceps and a ball of cot-ton. The applicstion fluid drys fast; the drying time equals only about S to 10 seconds and can even be shortened with the use of a hand blower. The application fluid according to the invention adheres to all materials which are used in the dental profession, including tooth materials. The application fluid thereby allows an unusually exact determination of pressure and contact points. The marking of contacts and early contacts is very distinct. The appllcation fluid accoPding to the invention is easily and economi-cally measured out because o~ its non-viscous consistency end com-position. A significantly greater number of crown co~tings is therefore achieved in contrast to the above-mentioned occlusion sprays ~improvement equaIs about 35~6). The fluid is neither toxic nor does it irritate the pulp. After use, the application 1uid is guickly and well-removed from the teeth, crowns and the like with ~3--~ ~38541 a solvent fluid. String formation and clumping, because of contact with saliva, do not occur during use.
The numerous advantages of the application fluid according to the invention, when compared with the above-mentioned occlu-sion spray, are represented in the following table.
Table -Application ~uid Occlusion Spray according to the __ __ ~ __ _ invention 10Ag~regate _Powder fluid Soluble in water: moderately alcohol: ver~ _ Granularity _ 10-20~m under 10~m D in tim* None _5-10 s ry ~ _ -lS Adhesion to_Metalls insufficient good Distribution insufficient good Properties in con- string formation no negativè
t~ct with saliva _ and clumpin~ Properties Contact recognition insufficier~t, good only for ex-tremely early contacts Neatness not neat, creates neatly used brushing3 per pack-~inP unit ~ , Further objects, features and advantages of the present invention will become appareslt from the detailed description o~ pre-ferred embodiment3 which ~ollows, when considered together with the several non-limiting examples.
DESCRIPTION OF PREFElRRED EMBODIMENTS
, The application fluid according to the invention contains an organic, polymeric adhesive in dispersed or dissolved form;

' : : ' ~ '. ., . -.
, :', ~ : ' ~.28854~

respectively. The granularity of the adhesive is preferably smaller than 10 micrometers. The ~dhesive is preferably a natural resin, particulnrly a resin from the group of shellac resins, colophonium resins, and modified colophonium resins. Another suitable group of s adhesives are represented by the group of alkyd resins, polyvinyl acetaldehydes, polyvinyl alcohols, polyvinyl acetates, polyacrylates and ketone resins.
The proportion of organic, polymeric adhesive totals pre-ferably from about 0.596 to about 1096 by weight, particularly from about 1% to about 5% by weight, in each case with respect to the total mass.
The massive component is a powdered constituent with a granularity of preferably under 10 micrometers, more preferably 5 to 7 micrometers. The massive component is preferably selected from the group of inert, pharmaceutically compatible pigments.
Titanium dioxide, in the form of titanium white, for example, is very much preferred~ Titanium whitet according to BIN55192 (November, 1960), is Q pigment whose color-determining consti-tuent is tit~nium dioxide . Aside from titanium dioxide ~ titanium 2 0 white additionally contains sulfates and carbonates of barium ~
calcium, and magnesium, and, additionally, for reasons of painting technology, up to 1096 zinc oxide (depending on the intended use).
The titanium oxide fraction, however, lies above 2~% in each case.
Anatase and rutile are also contemplated as titanium oxide 2 ~ materials. The fraction of massive component in the application fluid comprises preferably from 35% to 65% by weight, especially 40~6 to 60% by weight, with respect to the total quantity in each case .
The application fluid according to the invention contains a colored~pigment, similar to the above-mentioned silicon compounds, for the visu~l recognition of contact points. The colored pigment is chosen from the group of physiologically harmless color pigments;
and a green ~ red, or preferably blue color, is produced by con-tacts. Pigments from the heliogen series are preferably used, i.e.,
3 5 phthalocysnine-based colored pigments . Heliogen blue is a par-ticularly suited pigment. The concentration of the colored pigment .

.
.

38~;4~

is dependent on the intended use, so that dosaging may be carried out in the usual menner. The colored pigment content preferably lies in the range from 0.01% to 1~6 by weight, preferably 0.196 to 2% by weight, with respect to the total mass in each case.
In addition to the Qbove mentioned significant components of the ~pplication fluid, further common components of dental ~pplication compounds may be contained, if necessary, which keep the application f~uid antiseptic, pyrogen free, and sterile.
,The alcoholic solvent of the application fluid is pre~erably ~ an alcohol, particul~rly ethanol of cosmetic quality or pure ethanol.
Furtherrnore, other physiologically harmless fluids may be used with alcohol as long as they do not impair the consistency of the appli-cation fluid. Consequently, the composition of the applieation nu~d is as follows:
parts by wei~ht Particularly Preferred Preferred Adhesive0 . 5 - 10 1 - 5 Massive Component 35 - 65 4n - 60 Colored Pigment 0 . 01 - 10 0 .1 - 2 Solvent30 - 70 40 - 60 Examples for individuaI preferred compositions of the application fluid according to the invention, and one example each for their use in the exarnination of the occlusion, the articulation and in the inspection and production of a precise ~it in prosthetic works follow.
Example 1 ~; ~ Production of the applicstion uid.
3.63 part~ by weight shell~c (Gombal OD2) are dissolved in 20 parts by weight ethanol, with s~rring. In each case, O . 06 parts by weight Bentone W and Bentone,,~34 (dispersing agents), 48 parts by weight titanium dioxide (RN 56) and 11.25 parts by weight heliogen blue are added to this solution with stirring. The resulting paste is dispersed for 30 rninutes in a high speed dissolver. After achieving the desired granual size (C 10 /um)3 the remaining quan-~c~ c~ clr¦~

- , . .~
.

.
. . .

~ ~8~4~

tity of eth~nol (28 parts by weight) is added. A non-viscous application fluid results.
Exampl 2 Directed ~ of the inner surface and s surfaces of inlays crowns and the like.
The applic~tion fluid OI example 1 is purposefully applied to the approximate and chew surfaces by means of forceps and a cotton pellet. After a drying time of about 5 to 10 seconds, the prosthetic replacement is correspondingly inserted, pressed on and agairl removed.
Early contacts, as well as the precision of fit are visible at the points in which the dried application fluid has been pushed away cr is missing, respectively. Grinding work is necessary in these exactly signified points (early contacts) for the production of an optimal precision of fit (removal of the early contacts).
Contamination of hands and instruments is easily removed by means of an alcoholic solvent, ethanol for example.
Example 3 Inspection or orrection ~ ~ respectively of the occlusiYe relationships.
The application fluid of example ï is applied to the chewing surface of natural teeth. After the drying time, the patient is allowed to bite down or effect articulation movements (lsteral movements), respectively. The occlusion contacts or arti-culation contacts, respectively, are visible at those points in which the dried application fluid is pushed away. These points aLlow the even filing in (production of an equalized occlusion and articulation) of individual tooth crowns ~s well as the entire denture.
~e~
3 o Directed inspection of the bite hei~ht with smalgam ~ings.
After the filling is replaced, it is painted with the appli-catlon fluid of example 1. The patient is allowed to bite down -- ' , ' ' ' ' ~ : , : . , 38sa~

after the drying time. Should individual larger contact surfaces thereafter be visible on the filling, then these must be reduced with appropriate carving instruments.
Example S
sDirected ins~ction and_rmetion of the a~eroximate sur-faces OI crowns, bridges ~nd the like.
The application fluid of exflmple 1 is applied to the entire approximate surface. The prosthetic replacement is correspondingly set in after ~ying. After removal of the prosthesis, and by means 10of the size and contour shape of the surface which is pushed away, the contact surface or contact point, respectively, may be inspected and, if necessary, reforme~ by filing.

..
- . , .

Claims (13)

THE EMBODIMENTS OF THE INVENTION IN WHICH AN EXCLUSIVE
PROPERTY OR PRIVILEGE IS CLAIMED ARE DEFINED AS FOLLOWS:
1. Directly applicable, nonviscous, fast-drying dental application fluid comprising (a) 0.5 to 10 by weight percent of an organic polymeric adhesive, (b) 35 to 65 by weight percent of a massive component (c) 0.1 to 10 by weight percent of a colored pigment and (d) 30 to 70 by weight percent of a physiologically harmless alcoholic fluid said components (a), (b) and (c) being dissolved or respectively dispersed in said fluid (d).
2. An application fluid as cited in claim 1, wherein 30 to 70 weight percent of the total application fluid are solids having a granularity of less than 10 microns.
3. An application fluid as cited in claim 1 or 2, wherein said adhesive is selected from the group consisting of natural resins and modified natural resins.
4. An application fluid as cited in claim 1 or 2, wherein said adhesive is selected from the group consisting of shellac, colophonium resins, and modified colophonium resins.
5. An application fluid as cited in claim 1 or 2, wherein said adhesive is selected from the group consisting of alkyd resins, polyvinyl acetaldehydes, polyvinyl alcohols, polyvinyl acetates, polyacrylates and ketone resins.
6. An application fluid as cited in claim 1, wherein said massive component comprises titanium dioxide.
7. An application fluid as cited in claim 1, wherein said colored pigment comprises a blue phthalocyanine pigment.
8. An application fluid as cited in claim 1, wherein said fluid comprises from about 1% to about 5% polymeric adhesive, from about 40% to about 60% massive component, from about 0.1% to about 2% colored pigment, and from about 40% to about 60% alcoholic fluid, wherein said percentages are calculated by weight with respect to the total weight of the solution.
9. An application fluid as cited in claim 8, wherein said polymeric adhesive comprises shellac, wherein said massive component comprises titanium dioxide, wherein said colored pigment comprises heliogen blue, and wherein said alcoholic fluid comprises ethanol.
10. An application fluid as cited in claim 1, wherein said polymeric adhesive comprises shellac.
11. An application fluid as cited in claim 1 wherein component (b) is TiO2 and component (d) is Ethanol.
12. Directly applicable, nonviscous, fast-drying dental application fluid comprising (a) an organic polymeric adhesive (b) a titanium dioxide component (c) a colored pigment said components (a), (b) and (c) being dissolved or respectively dispersed in a physiologically harmless ethanol fluid, wherein said dental application fluid contains 0.5 to 10 weight percent of the adhesive, 35 to 65 weight percent of the titanium dioxide, 0.01 to 10 weight percent of the colored pigment and 30 to 70 weight percent of the ethanol fluid, and wherein the solids content of the application fluid is 30 to 70 weight percent.
13. A process for dental inspection, comprising the steps of:
CA000512748A 1984-01-30 1986-06-30 Dental application fluid for the inspection of tooth contacts and prosthetic works Expired - Fee Related CA1288541C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CA000512748A CA1288541C (en) 1984-01-30 1986-06-30 Dental application fluid for the inspection of tooth contacts and prosthetic works

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19843403118 DE3403118A1 (en) 1984-01-30 1984-01-30 DENTAL APPLICATION LIQUID FOR CONTROLLING TOOTH CONTACTS AND PROSTHETIC WORKS
CA000512748A CA1288541C (en) 1984-01-30 1986-06-30 Dental application fluid for the inspection of tooth contacts and prosthetic works

Publications (1)

Publication Number Publication Date
CA1288541C true CA1288541C (en) 1991-09-03

Family

ID=25671039

Family Applications (1)

Application Number Title Priority Date Filing Date
CA000512748A Expired - Fee Related CA1288541C (en) 1984-01-30 1986-06-30 Dental application fluid for the inspection of tooth contacts and prosthetic works

Country Status (1)

Country Link
CA (1) CA1288541C (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110151563A (en) * 2019-06-21 2019-08-23 山西医科大学口腔医院 A kind of oral cavity reconciles cream and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110151563A (en) * 2019-06-21 2019-08-23 山西医科大学口腔医院 A kind of oral cavity reconciles cream and preparation method thereof

Similar Documents

Publication Publication Date Title
Attar et al. Fluoride release and uptake capacities of fluoride-releasing restorative materials
Stein et al. A dentist and a dental technologist analyze current ceramo-metal procedures
US4738722A (en) Dental compositions incorporating glass ionomers
Hickel et al. New direct restorative materials
JP4527666B2 (en) Tooth application composition
AU775954B2 (en) Tooth coating composition
RU2395269C2 (en) Compositions and methods for changing tooth colour
JPH09100215A (en) Tooth coating liquid
Santini et al. Microleakage of composite restorations bonded with three new dentin bonding agents
US4643678A (en) Dental application fluid for the inspection of tooth contacts and prosthetic works
CA2302281A1 (en) Protective varnish for dentin
Fink Materials, chemicals and methods for dental applications
CN111163744B (en) Fluorine coating agent having improved dentinal tubule penetration and coating retention and method for preparing the same
USRE33100E (en) Dental compositions incorporating glass ionomers
CA1288541C (en) Dental application fluid for the inspection of tooth contacts and prosthetic works
JP4002996B2 (en) Method for attaching temporary denture apparatus using glass ionomer cement and kit therefor
CA2077943C (en) Aesthetic, opalescent cold-polymerizable dental restorative
US3992515A (en) Composition for indicating and method of removing dental undercuts and the like
EP0198930B1 (en) Dental application solution to check teeth contacts and prosthetic fitting operations
DE60311226T2 (en) Light-curing lacquer resin for adjusting the shades
JP4184939B2 (en) Light-curing paint resin for shade adjustment
Ben-Amar et al. The effect on marginal microleakage of using a combination of cavity varnishes and calcium hydroxide intermediary bases-an in vitro study.
SWARTZ Dental cements and restorative resins
AU696562B2 (en) Aesthetic, opalescent cold-polymerizable dental restorative
EP2883527A1 (en) Dental material

Legal Events

Date Code Title Description
MKLA Lapsed