CA1085226A - Drive means for desolventizer toaster - Google Patents

Drive means for desolventizer toaster

Info

Publication number
CA1085226A
CA1085226A CA255,040A CA255040A CA1085226A CA 1085226 A CA1085226 A CA 1085226A CA 255040 A CA255040 A CA 255040A CA 1085226 A CA1085226 A CA 1085226A
Authority
CA
Canada
Prior art keywords
steam
pressure steam
desolventizing
turbine
vessel
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA255,040A
Other languages
French (fr)
Inventor
Robert D. Good
Robert J. Kendi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dravo Corp
Original Assignee
Dravo Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dravo Corp filed Critical Dravo Corp
Application granted granted Critical
Publication of CA1085226A publication Critical patent/CA1085226A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/10Production of fats or fatty oils from raw materials by extracting
    • C11B1/108Production of fats or fatty oils from raw materials by extracting after-treatment, e.g. of miscellae
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/14Evaporating with heated gases or vapours or liquids in contact with the liquid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0215Solid material in other stationary receptacles
    • B01D11/0223Moving bed of solid material
    • B01D11/0234Moving bed of solid material using other slow rotating arms or elements, whereby the general transport direction of the solids is not parallel to the rotation axis, e.g. perpendicular
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0215Solid material in other stationary receptacles
    • B01D11/0223Moving bed of solid material
    • B01D11/0242Moving bed of solid material in towers, e.g. comprising contacting elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

Abstract of the Disclosure There is disclosed a desolventizer-toaster having means for admitting sparge steam and shaft means on which sweeps or agitating arms are mounted for agitating the contents. The means for admitting sparge steam may be via sparger elements mounted in the agitating arms or via holes in one or more of the trays of the desolventizer toaster. The shaft is rotatably driven by a steam turbine with sparge steam requirements for the desolven-tizer toaster provided, in part, by low pressure steam withdrawn from the turbine.

Description

This invention relates to a process and apparatus for heating a bulk material to remove recoverable vaporizable components therefrom, and more particularly to a process and apparatus for desolventizing and toasting or cooking solvent-extracted materials, particularly solvent-extracted oleaginous seed material, Oleaginous seed materials, such as soybeans, cotton seeds, peanuts, sesame seeds, sunflower seeds, rapeseed, and the like contain proteinaceous matter of a highly nutritious nature.
Soybeans for example, after oil extraction, have been treated to recover the proteinaceous matter for use in diver~e industrial processes, e. g. in the paper, plastic and food industries. Without limitations as to other uses, the invention will be herein particularly ;~
described in connection with the extraction of oil from soybeans.
In the processing of seeds to extract OL~ by solvent extraction, the seeds are crushed or milled into meal or flakes or otherwise fragmentized and treated with a solvent to extract the oilJ
leaving meal in which vaporizable solvent remains. By heating the meal, using steam both indirectly through a heated surface and/or directly by steam contacting the meal, the solvent is vaporized while the meal itself is cool~ed or toasted to produce an edible substance.
Apparatus for vaporizing the solvent so that it might be recovered ~^
while simultaneously and/or subsequentia y toasting the extracted seed is well known in the art as illustrated, for example, in United States Patents Nos. 1,112,128; 2, 577, 010; 2, 585, 793; 2, 695,459;

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2, 806, 297;3, 018, 564; and 3, 359, 644.
As disclosed in these patents, the material from which solvent is to be removed progresses downwardly through a column which has spaced horizontal plates therein dividing the interior of the column into a vertical series of compartments. In these compartments the material is heated and agitated and the finished material discharged ~
from the bottom of the column. Solvent is removed as an overhead ;
vapor which is then condensed.
Present desolventizing practice is to introduce steam into the desolventizer column directly from a boiler via suitable piping including valves, orifices, etc., to reduce the pressure of the - steam to that necessary for sparging the bed to accomplish desolven-tizing operations. An electric motor is the power source for rotating the sweep arms using sultable speed reduction devices. Typically, steam is supplied to the plant at pressures from 100 to 200 psig. since steam is needed for other operations at such pressures, for example the heating trays of the desolventizer, steam jet ejectors, etc. and at a pressure higher than necessary for sparge steam in the de-solventizer. In the desolventi~er, steam flows into the flakes on the trays via control valves, orifices, meters, etc., with holes being provided in the sparge tray, the sparge arms or similar devices for contact with the flake mass. During steam flow, steam pressure is reduced across the restrictions imposed by such orifices, valves~
meters, etc. to the lower pressure necessary to flow through the holes in the sparging device.

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Objects of this invention are achieved by driving with steam turbine the rotating elements of a desolventizer column with the sparge steam requirement being provided, in part, by low pressure steam withdrawn from the steam turbine.

Thus, in accordance with the present teachings, an improvement is provided in a process for desolventizing a solvent extracted material in a desolventizing vessel formed of a vertical column having a shaft and provided with a plurality of heated trays which define a plurality of zones wherein each zone is provided with sparger arms for introducing low pressure steam into the desolventizing vessel and wherein a vapor includ-ing vaporized solvent and desolventized extracted material are withdrawn from the desolventizing vessel. The improvement which is provided comprises introducing high pressure steam into a steam turbine to provide a source of power for rotating the shaft and passing low pressure steam from the turbine to the desolventizing vessel to provide a portion of the steam requirement for the sparger arms.
In accordance with a further e~bodiment an improved apparatus is provided for desolventizing with low pressure steam a solvent extracted material in a desolventizing vessel formed of a vertical column divided into a plurality of sub-zones by heated trays and wherein the vessel is provided with a shaft on which is disposed ;
a plurality of sparger arms and means are provided for withdraw-ing vaporized solvent and desolventi~ed extracted material. The improvement which is provided includes a turbine drive means for rotating the shaft, a source of high pressure steam for driving the turbine drive means and conduit means for withdrawing low pressure steam from the turbine means and for passing the steam to the vessel to provide sparger steam requirements therefor.

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A better understanding of the present invention as well as other objects and advantages thereof will become apparent upon consideration of the detailed disclosure thereof, especially when taken with the accompanying schematic drawing.
It is to be understood that equipment such as passages, valve~, indicators, and the like have been omitted from the drawing to facilitate the description thereof and the placing of such equipment at appropriate places is deemed to be within the scope of those ~killed in the art. In the drawing, the component parts of my nav el proces9 and apparatus includes a desolventizer column, generally indicated as 10, such as described in U.S, Patent No. 3, 359, 649, a turbine 12 and a flash drum 14.
The desolventizer 10 includes a hollow shell 16 generally cyllndrical in shape having a conical shaped upper portion forming a vertical column which is divided horizontally by steam-heated trays 18 into a vertical series of compartments 20. Each of the trays 18 has an opening or chute (not shown) through which bulk material may be passed dowQwardly from one compartment to the -next in a controlled manner. There is a vertical shaft 22 extending up the center of the column 16. In the lower compartments the shaft 22 is provided with arms 24 which sweep around over the trays 18 to agitate the material whereas in the uppermost compartment, or some of them, the shaft 22 is provided with rotating sparger , , , 3û

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arms 2B. The shaft 22 is driven via a reduction gear 28 by the turbine 12, Steam is introduced by a steam supply conduit 30 through a swivel joint (not shown) into the central shaft 22 for discharge through the sparger arms 26. The top of the vertical column 16 above the uppermost compartment is provided with a dome-shaped portion 32 which is enclosed by a roof portion 34.
Material to be treated is introduced into the desolventizer 10 through an inlet connection 36.
The desolventizer 10 is provided witha vapor out~
let 38 and a scrubber connection 40. A vertical duct 42 is disposed alongside the shell 16 in contiguous relationship thereto for the purpose described in the aforementioned U. S. Patent No. 3, 359, 649.
In operation, high pressure steam, e. g. at a pressure of from 100 to 200 psig. in line 42 is introduced into the turbine 12 and expanded to a pressure of about 15 to 25 psig. to produce the power required to drive the shaft 22 of the desolventizer 10 via the reduction gear 28. Unexpectedly, a turbine operating within such pressure range requires less steam to produce the power re- ~ r quired for rotation than is required for sparging the solvent wet soybean material to be treated. Low pressure steam is withdrawn from turbine 12 by line 44 and is introduced into flash drum 14 from which low pressure steam is withdrawn by line 46 and introduced into the steam supply conduit 30 to provide the sparging steam re-quired. The flash drum 14 permits an opportunity for some vaporization of condensate by heat interchange with higher pressure steam make up as well as removing condensate from Low pressure discharge of the steam turbine 12.

, .;: i . , . .

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Steam (high pressure) for the heated trays 18 is introduced into the trays in a manner known to those skilled in the art. A solvent vapor stream is withdrawn from the desolventizer 10 via vapor outlet 38 for the subsequent recovery of solvent there-from (not shown) with desolventizer solids being withdrawn by chute 48 for processing (not shown) in a rnanner known to those skilled in the art.
High pressure conden9ate from the heated trays 18 is passed by line 50 via a trap 52 to flash tank 14 as an additional source of low pressure steam for sparging. Such condensate in line 50 is mixed in steam drum 14 with turbine outlet steam in line 44 and high pressure steam in line 54, after expansion across a valve - 56. As hereinabove discussed, the low pressure steam requirementsfor ~parging of the material is in excess of that withdrawn from the turbine thereby necessitating the introduction of additional low pressure steam by line 54 into flash drum 14 after expansion of - high pressure steam across valve 56.
Examples of the Invention Each of the following Tables I and II illustrate the benefits and expected steam usage for three plant rates for processing soybeans at 100 and 150 psig., respectively high pressure steam a va ilability.
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Itwill be appreciated that an existing desolventizing unit may be modified in accordance with the present invention, i. e., the existing electric motor including starter, wiring and the like is replaced with a steam turbine, associated piping, flash tank, etc.
with instrumentation being essentially similar. Safety of a plant is enhanced since a steam turbine drive is inherently less hazardous than an electric motor. AdditionaLly, varied rotational speed rates of the arms may be readily accomplished by adjusting the governor -for the turbine thereby providing capabilities for altering process conditions for treating materials which change as the season between harvest progresses.
As hereinabove mentioned, electrical power require- -ments are eliminated with no increase in steam requirements.
Additionally, the introduction of lower pressure steam for sparging effects a reduction in superheat to be given up before condensing into the extracted flakes as compared with high pressure steam reduced in pressure for use via the sparger means thereby making more effective the transfer of heat between condensing water and vaporizing solvent.
While the embodiment of the present invention has been discussed with reference to a desolventizer-toaster including rotating sparger members, it will be understood that the principle of the present invention is applicable to any form of desolventizer-toaster having a shaft including rotating members wherein steam is directly introduced into the meal, e. g., by perforated trays as disclosed in U. S. Patent No. 3, 018, 564 to Kruse. Additionally, 1~352~
:` ,:

it will be understood that turbine efficiency may be varied with regard to variations in steam presssure as well as turbine discharge pressure, etc. as is well known to those skilled in the art.

' ~ ~

Claims (11)

1. In a process for desolventizing a solvent extracted material in a desolventizing vessel formed of a vertical column having a shaft and provided with a plurity of heated trays defining a plurality of zones and wherein each zone is provided with sparger arms for introducing low pressure steam into said desolventizing vessel and wherein a vapor including vaporized solvent and desolventized extracted material are withdrawn from said desolventizing vessel, the improvement comprising:
introducing high pressure steam into a steam turbine to provide the source of power for rotating said shaft; and passing low pressure steam from said turbine to said desolventizing vessel to provide a portion of the steam requirements for said sparger arms.
2. The process as defined in Claim 1 wherein said low pressure steam withdrawn from said turbine is passed to a flash drum and said low pressure steam for sparging is withdrawn from said flash drum.
3. The process as defined in Claim 2 wherein high pressure steam is throttled to said flash drum.
4. The process as defined in Claim 2 wherein said material is passed in indirect contact with steam.
5. The process as defined in Claim 4 wherein high pressure steam condensate is withdrawn from said indirect contact to provide a portion of said sparger steam requirement after being throttled into said flash drum.
6. An improved apparatus for desolventizing with low pressure steam a solvent extracted material in a desolventizing vessel formed of a vertical column and divided into a plurality of sub-zones by heated trays and wherein said vessel is provided with a shaft on which is disposed a plurality of spargers arms, and wherein there are provided means for withdrawing vaporized solvent and desolventized extracted material, the improvement characterized by:
a turbine drive means for rotating said shaft;
a source of high pressure steam for driving said turbine drive means; and conduit means for withdrawing low pressure steam from said; turbine means and for passing said steam to said vessel to provide sparger steam requirements therefor.
7. The improved apparatus as defined in Claim 6 wherein uppermost arms of said plurality of arms includes sparger devices.
8. The improved apparatus as defined in Claim 6 wherein said conduit means includes a flash drum.
9. The improved apparatus as defined in Claim 6 wherein one or more of said uppermost trays include orifices for admitting sparger steam.
10. The improved apparatus as defined in Claim 8 and including a second conduit means for passing high pressure steam to said flash drum.
11. The improved apparatus as defined in Claim 6 including a third conduit means for withdrawing a high pressure steam condensate from said heated trays and for passing and throttling said condensate into said flash drum.
CA255,040A 1975-11-28 1976-06-16 Drive means for desolventizer toaster Expired CA1085226A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US63620575A 1975-11-28 1975-11-28
US636,205 1975-11-28

Publications (1)

Publication Number Publication Date
CA1085226A true CA1085226A (en) 1980-09-09

Family

ID=24550902

Family Applications (1)

Application Number Title Priority Date Filing Date
CA255,040A Expired CA1085226A (en) 1975-11-28 1976-06-16 Drive means for desolventizer toaster

Country Status (10)

Country Link
JP (1) JPS5270983A (en)
AU (1) AU508180B2 (en)
BE (1) BE848701A (en)
BR (1) BR7604989A (en)
CA (1) CA1085226A (en)
DE (1) DE2635049A1 (en)
FR (1) FR2336153A1 (en)
GB (1) GB1541707A (en)
NL (1) NL7607783A (en)
SE (1) SE7608212L (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7156981B2 (en) * 1999-01-25 2007-01-02 Bio Extraction Limited ITFM extraction of oil seeds
CN112717545B (en) * 2020-12-09 2022-07-29 江尔成 Chinese medicinal material solution extraction processing device and Chinese patent medicine preparation method
CN114133947A (en) * 2021-11-08 2022-03-04 中国平煤神马集团平顶山京宝焦化有限公司 Coal tar distillation device
CN117848009B (en) * 2024-03-06 2024-05-07 诸城兴贸玉米开发有限公司 Corn powder dryer for agricultural product treatment

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE378829A (en) *
US3126285A (en) * 1964-03-24 Method of desolventizing and toasting soybean meal
FR1345401A (en) * 1963-01-16 1963-12-06 Metallgesellschaft Ag Method and device for removing solvent from a product previously subjected to extraction
US3359649A (en) * 1966-02-24 1967-12-26 Blaw Knox Co Apparatus for the heating of bulk material and recovery of vaporizable product therefrom
US3966982A (en) * 1973-06-18 1976-06-29 Dravo Corporation Process and apparatus for treating oleaginous seed material

Also Published As

Publication number Publication date
JPS5270983A (en) 1977-06-13
BR7604989A (en) 1977-08-09
FR2336153A1 (en) 1977-07-22
AU1528776A (en) 1978-01-05
NL7607783A (en) 1977-06-01
SE7608212L (en) 1977-05-29
GB1541707A (en) 1979-03-07
AU508180B2 (en) 1980-03-13
BE848701A (en) 1977-03-16
DE2635049A1 (en) 1977-06-02

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