CA1049748A - Hydroxy-aluminum nitrate polymer production from aluminum nitrate and urea - Google Patents
Hydroxy-aluminum nitrate polymer production from aluminum nitrate and ureaInfo
- Publication number
- CA1049748A CA1049748A CA208,103A CA208103A CA1049748A CA 1049748 A CA1049748 A CA 1049748A CA 208103 A CA208103 A CA 208103A CA 1049748 A CA1049748 A CA 1049748A
- Authority
- CA
- Canada
- Prior art keywords
- aluminum nitrate
- urea
- aluminum
- hydroxy
- varies
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 title claims abstract description 30
- 239000004202 carbamide Substances 0.000 title claims abstract description 29
- BNGXYYYYKUGPPF-UHFFFAOYSA-M (3-methylphenyl)methyl-triphenylphosphanium;chloride Chemical compound [Cl-].CC1=CC=CC(C[P+](C=2C=CC=CC=2)(C=2C=CC=CC=2)C=2C=CC=CC=2)=C1 BNGXYYYYKUGPPF-UHFFFAOYSA-M 0.000 title claims abstract description 18
- 229920000642 polymer Polymers 0.000 title claims abstract description 18
- HIZLQUSEDILRSC-UHFFFAOYSA-M [N+](=O)([O-])[O-].O[Al+2].[N+](=O)([O-])[O-] Chemical compound [N+](=O)([O-])[O-].O[Al+2].[N+](=O)([O-])[O-] HIZLQUSEDILRSC-UHFFFAOYSA-M 0.000 title claims abstract description 12
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000007864 aqueous solution Substances 0.000 claims abstract description 7
- 238000000034 method Methods 0.000 claims description 22
- 229910052782 aluminium Inorganic materials 0.000 claims description 13
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 12
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- RKFMOTBTFHXWCM-UHFFFAOYSA-M [AlH2]O Chemical compound [AlH2]O RKFMOTBTFHXWCM-UHFFFAOYSA-M 0.000 claims description 7
- XNDZQQSKSQTQQD-UHFFFAOYSA-N 3-methylcyclohex-2-en-1-ol Chemical group CC1=CC(O)CCC1 XNDZQQSKSQTQQD-UHFFFAOYSA-N 0.000 claims description 5
- 229910018626 Al(OH) Inorganic materials 0.000 claims description 5
- 229910002651 NO3 Inorganic materials 0.000 claims description 4
- 238000010992 reflux Methods 0.000 claims description 4
- JLDSOYXADOWAKB-UHFFFAOYSA-N aluminium nitrate Chemical compound [Al+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O JLDSOYXADOWAKB-UHFFFAOYSA-N 0.000 claims description 3
- 150000004690 nonahydrates Chemical class 0.000 claims 1
- 239000000203 mixture Substances 0.000 abstract description 7
- 239000003337 fertilizer Substances 0.000 abstract description 4
- 239000002689 soil Substances 0.000 abstract description 4
- 150000003863 ammonium salts Chemical class 0.000 abstract description 2
- 238000011084 recovery Methods 0.000 abstract description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 10
- 239000000243 solution Substances 0.000 description 9
- 239000000376 reactant Substances 0.000 description 6
- 229960005419 nitrogen Drugs 0.000 description 5
- 229910052757 nitrogen Inorganic materials 0.000 description 5
- 239000013078 crystal Substances 0.000 description 4
- -1 e.g. Substances 0.000 description 4
- 239000003517 fume Substances 0.000 description 4
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 239000000654 additive Substances 0.000 description 2
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000007596 consolidation process Methods 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical class [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- IRXRGVFLQOSHOH-UHFFFAOYSA-L dipotassium;oxalate Chemical compound [K+].[K+].[O-]C(=O)C([O-])=O IRXRGVFLQOSHOH-UHFFFAOYSA-L 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/66—Nitrates, with or without other cations besides aluminium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/20—Nitrogen oxides; Oxyacids of nitrogen; Salts thereof
- C01B21/38—Nitric acid
- C01B21/46—Purification; Separation ; Stabilisation
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C1/00—Ammonium nitrate fertilisers
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fertilizers (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US458631A US3925428A (en) | 1974-04-08 | 1974-04-08 | Hydroxy-aluminum nitrate polymer production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1049748A true CA1049748A (en) | 1979-03-06 |
Family
ID=23821519
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA208,103A Expired CA1049748A (en) | 1974-04-08 | 1974-08-29 | Hydroxy-aluminum nitrate polymer production from aluminum nitrate and urea |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3925428A (OSRAM) |
| CA (1) | CA1049748A (OSRAM) |
| FR (1) | FR2266658B1 (OSRAM) |
| GB (1) | GB1462729A (OSRAM) |
| NO (1) | NO139434C (OSRAM) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4069299A (en) * | 1976-05-05 | 1978-01-17 | Chevron Research Company | Hydroxy-aluminum chloride and sulfate polymer production |
| GB2307475B (en) * | 1995-11-23 | 1998-07-29 | Sandoz Ltd | Cement acceleration process |
| FR2741616B1 (fr) * | 1995-11-23 | 2000-03-10 | Sandoz Sa | Accelerateurs du ciment |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3457127A (en) * | 1968-03-18 | 1969-07-22 | Melvin Cook | Explosive composition containing an additional product of urea and nitric acid and method of preparing same |
| US3816590A (en) * | 1971-03-18 | 1974-06-11 | Little Inc A | Method and apparatus for providing a pure concentrated aqueous solution of aluminum nitrate |
| US3783053A (en) * | 1972-01-19 | 1974-01-01 | Gulf Oil Corp | Process for manufacturing gasentrained aqueous gel explosive |
-
1974
- 1974-04-08 US US458631A patent/US3925428A/en not_active Expired - Lifetime
- 1974-08-29 CA CA208,103A patent/CA1049748A/en not_active Expired
- 1974-10-17 GB GB4511074A patent/GB1462729A/en not_active Expired
-
1975
- 1975-03-20 NO NO750959A patent/NO139434C/no unknown
- 1975-04-01 FR FR757510114A patent/FR2266658B1/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| NO139434B (no) | 1978-12-04 |
| NO750959L (OSRAM) | 1975-10-09 |
| DE2456274A1 (de) | 1975-10-16 |
| GB1462729A (en) | 1977-01-26 |
| FR2266658B1 (OSRAM) | 1979-02-09 |
| DE2456274B2 (de) | 1977-04-14 |
| NO139434C (no) | 1979-03-14 |
| FR2266658A1 (OSRAM) | 1975-10-31 |
| US3925428A (en) | 1975-12-09 |
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