BR0108300A - Determinação das propriedades de uma solução ou sólido ao se empregar coeficientes de raman - Google Patents
Determinação das propriedades de uma solução ou sólido ao se empregar coeficientes de ramanInfo
- Publication number
- BR0108300A BR0108300A BR0108300-7A BR0108300A BR0108300A BR 0108300 A BR0108300 A BR 0108300A BR 0108300 A BR0108300 A BR 0108300A BR 0108300 A BR0108300 A BR 0108300A
- Authority
- BR
- Brazil
- Prior art keywords
- raman
- coefficients
- properties
- solid
- solution
- Prior art date
Links
- 238000001069 Raman spectroscopy Methods 0.000 title abstract 9
- 239000007787 solid Substances 0.000 title abstract 5
- 238000000034 method Methods 0.000 abstract 3
- 239000006185 dispersion Substances 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- 229920002488 Hemicellulose Polymers 0.000 abstract 1
- 229910002651 NO3 Inorganic materials 0.000 abstract 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 abstract 1
- 229910019142 PO4 Inorganic materials 0.000 abstract 1
- 238000001237 Raman spectrum Methods 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 238000001311 chemical methods and process Methods 0.000 abstract 1
- QBWCMBCROVPCKQ-UHFFFAOYSA-N chlorous acid Chemical compound OCl=O QBWCMBCROVPCKQ-UHFFFAOYSA-N 0.000 abstract 1
- 229940077239 chlorous acid Drugs 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- -1 hemicellulose Chemical class 0.000 abstract 1
- QWPPOHNGKGFGJK-UHFFFAOYSA-N hypochlorous acid Chemical compound ClO QWPPOHNGKGFGJK-UHFFFAOYSA-N 0.000 abstract 1
- 150000002500 ions Chemical class 0.000 abstract 1
- 150000002605 large molecules Chemical class 0.000 abstract 1
- 229920002521 macromolecule Polymers 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 150000002826 nitrites Chemical class 0.000 abstract 1
- 230000033116 oxidation-reduction process Effects 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 239000000575 pesticide Substances 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract 1
- 239000010452 phosphate Substances 0.000 abstract 1
- 238000006116 polymerization reaction Methods 0.000 abstract 1
- 150000004760 silicates Chemical class 0.000 abstract 1
- 150000003384 small molecules Chemical class 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 abstract 1
- 230000003595 spectral effect Effects 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/34—Paper
- G01N33/343—Paper pulp
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C7/00—Digesters
- D21C7/12—Devices for regulating or controlling
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
- G01N21/65—Raman scattering
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
Abstract
"DETERMINAçãO DAS PROPRIEDADES DE UMA SOLUçãO OU SóLIDO AO SE EMPREGAR COEFICIENTES DE RAMAN" a invenção se refere ao uso de coeficientes, produtos e funções não lineares de adsorção, emissão ou difusão da luz como variáveís em técnicas de regressão e quimiométricas padrão para predizer uma característica ou propriedade de um sólido ou líquido, o uso de uma ou mais funções não lineares dentro de um relação entre propriedades espectrais medidas e propriedades características de soluções e sólidos fornece um meio aperfeiçoado para determinar uma propriedade quando as intensidades representam estão relacionadas com componentes que são colineares ou interrelacionados devido às restrições associadas com a composição, os processos químicos, ou a estrutura molecular; ao uso de coeficientes de intensidades de pico de Raman para predizer as propriedades de uma solução ou um sólido tal como polpa que é processada com a solução; a intensidade da luz deslocada de Raman é utilizada para criar coeficientes de intensidade de pico de Raman; essas intensidades de Raman estão relacionadas com a concentração da espécie dissolvida no líquido; os espectros de Raman são corrigidos na linha base e a dispersão de uma fonte de ãgua é subtraída antes da extração das intensidades para os coeficientes de intensidades de pico de Raman;as intensidades de dispersão de Raman fornecem uma boa medida da concentração de moléculas oxigenadas pequenas; o potencial de um processo de oxidação-redução é determinado convenientemente ao se utilizar coeficientes de intensidade de pico de Raman; as moléculas pequenas e os íons complexo relevantes na indústria de papel e celulose incluem S042-, S032-, H202, CIO2, HCIO,3, silicatos, ácido acótico, HCIO3, Ciorato C103-, ácido Cloroso HCi02, Ciorito C102-, ácido Hipocioroso HCIO, Hipociorito CIO-, fosfato, nitrato, nitrítos; o método também pode ser utilizado para determinar uma propriedade relacionada com o tamanho relativo, o grau de polimerização, a ramíficação ou formação de rede de espécies de complexos ou polimerizadas; o método também pode ser utilizado para medir moléculas grandes tais como hemicelulose, extrativos e substâncias péctícas.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/499,450 US6774992B1 (en) | 1997-03-10 | 2000-02-07 | Determination of the property of a solution or solid using raman ratios |
| PCT/CA2001/000123 WO2001059437A1 (en) | 2000-02-07 | 2001-02-05 | Determination of the properties of a solution or solid using raman ratios |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BR0108300A true BR0108300A (pt) | 2003-03-11 |
Family
ID=23985290
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR0108300-7A BR0108300A (pt) | 2000-02-07 | 2001-02-05 | Determinação das propriedades de uma solução ou sólido ao se empregar coeficientes de raman |
Country Status (5)
| Country | Link |
|---|---|
| EP (1) | EP1254363A1 (pt) |
| BR (1) | BR0108300A (pt) |
| CA (1) | CA2403008C (pt) |
| NO (1) | NO20023720L (pt) |
| WO (1) | WO2001059437A1 (pt) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7521254B2 (en) | 2004-04-12 | 2009-04-21 | Transform Pharmaceuticals, Inc. | Quantitative measurements of concentration and solubility using Raman spectroscopy |
| FI122238B (fi) | 2006-02-09 | 2011-10-31 | Metso Automation Oy | Menetelmä ja laitteisto massasuspension kokonaisperoksidipitoisuuden määrittämiseksi |
| US8009277B2 (en) | 2007-10-26 | 2011-08-30 | International Paper Company | Sensor technique for black liquor oxidation control |
| WO2009117823A1 (en) * | 2008-03-25 | 2009-10-01 | Alberta Research Council Inc. | Continuous measurement of amine loading in gas processing plants using raman spectroscopy |
| EP3230520A4 (en) | 2014-12-12 | 2018-08-15 | Canfor Pulp Ltd | Method and apparatus for controlling a cellulosic pulp process |
| CN111751510A (zh) * | 2020-08-13 | 2020-10-09 | 北京雪域飞虹环保科技有限公司 | 一种多路感应降噪补偿还原算法的toc检测方法 |
| CN112362636A (zh) * | 2020-11-04 | 2021-02-12 | 西安建筑科技大学 | 一种基于拉曼光谱的绿泥石矿物种类鉴定方法 |
| CN115290562A (zh) * | 2022-08-09 | 2022-11-04 | 江苏经贸职业技术学院 | 一种5-羟甲基糠醛的sers检测方法 |
| CN116785967B (zh) * | 2023-04-28 | 2024-03-08 | 福建省龙德新能源有限公司 | 用于电子级六氟磷酸锂制备的自动配料系统 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5139334A (en) * | 1990-09-17 | 1992-08-18 | Boston Advanced Technologies, Inc. | Hydrocarbon analysis based on low resolution raman spectral analysis |
| EP0714025A1 (en) * | 1994-11-25 | 1996-05-29 | Kyoto Dai-ichi Kagaku Co., Ltd. | Method of and apparatus for determining hydrogen peroxide by Raman scattering |
| US5999255A (en) * | 1997-10-09 | 1999-12-07 | Solutia Inc. | Method and apparatus for measuring Raman spectra and physical properties in-situ |
| DE19814385C1 (de) * | 1998-03-31 | 1999-10-07 | Siemens Ag | Verfahren und Vorrichtung zur Prozeßführung und zur Prozeßoptimierung der Chemikalienrückgewinnung bei der Herstellung von Zellstoff |
-
2001
- 2001-02-05 CA CA2403008A patent/CA2403008C/en not_active Expired - Fee Related
- 2001-02-05 EP EP01903539A patent/EP1254363A1/en not_active Withdrawn
- 2001-02-05 BR BR0108300-7A patent/BR0108300A/pt not_active Application Discontinuation
- 2001-02-05 WO PCT/CA2001/000123 patent/WO2001059437A1/en not_active Application Discontinuation
-
2002
- 2002-08-06 NO NO20023720A patent/NO20023720L/no not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| CA2403008C (en) | 2011-11-01 |
| EP1254363A1 (en) | 2002-11-06 |
| NO20023720L (no) | 2002-10-07 |
| NO20023720D0 (no) | 2002-08-06 |
| CA2403008A1 (en) | 2001-02-05 |
| WO2001059437A1 (en) | 2001-08-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B25C | Requirement related to requested transfer of rights |
Owner name: ALBERTA RESEARCH COUNCIL INC. (CA) Free format text: A FIM DE ATENDER A TRANSFERENCIA REQUERIDA ATRAVES DA PETICAO NO 018110041895/SP DE 27/10/2011, E NECESSARIO APRESENTAR O DOCUMENTO COM A DEVIDA LEGALIZACAO CONSULAR, ALEM DA GUIA DE CUMPRIMENTO DE EXIGENCIA. |
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| B25A | Requested transfer of rights approved |
Owner name: ALBERTA INNOVATES - TECHNOLOGY FUTURES (CA) Free format text: TRANSFERIDO DE: ALBERTA RESEARCH COUNCIL INC. |
|
| B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
| B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: INDEFIRO O PEDIDO DE ACORDO COM ART. 25 DA LPI |
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| B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: MANTIDO O INDEFERIMENTO UMA VEZ QUE NAO FOI APRESENTADO RECURSO DENTRO DO PRAZO LEGAL. |