AU680044B2

AU680044B2 - Reactor for removing impurities from a liquid

Info

Publication number: AU680044B2
Application number: AU75858/94A
Authority: AU
Inventors: Flavio Magaraggia
Original assignee: Comer SpA
Current assignee: Comer SpA
Priority date: 1994-10-17
Filing date: 1994-10-17
Publication date: 1997-07-17
Anticipated expiration: 2014-10-17
Also published as: AU7585894A

Description

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AUSTRALIA

Patents Act 1990

ORIGINAL

COMPLETE SPECIFICATION STANDARD PATENT ",Reac tor for Removing Impurities from a Liquid" The following statement is a full description of this invention, including the best method of performing it known to me:

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i9 Ie -la- "REACTOR FOR REMOVING IMPURITIES FROM A LIQUID" The present invention concerns a reactor for removing impurities from a liquid, in particular for de-inking suspensions deriving from printed waste paper.

Apparatuses are known for removing impurities from liquids and in particular for de-inking paper suspensions, said apparatuses being based on the flotation method.

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I II For example, US patent No.4186094 concerns an apparatus for eliminating impurities from a liquid by means of flotation, including various flotation cells arranged one on top of the other. The liquid-air mixture is introduced in the lower portion of the lowermost cell, with the subsequent separation of the air bubbles enclosing the impurities of the purified liquid which is taken to the uppermost cell. The separation of the bubbles from the purified liquid takes place in this last cell, in which also air is introduced in addition to the purified liquid, which passes down into the underlying cell and so on for the cells arranged below. In this way, the bubbles loaded with impurities flow downwards from each cell through a drain, while the accepted flows out from each single cell for the use thereof.

This purification system, besides being complicated and expensive has a low purification efficiency mainly due to the fact that the apparatus is made up 2of various cells arranged in series one with respect to the other.

3 .e Other prior art of US 4094783, US 4347128 and DE 4i YS4~L i -ib- 4, cc C Ct C C 10 tc Ce C C t C, C C C

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4. C 4 C 3524071 relate to a separator for removing impurities from a contaminated liquid comprising a tank having an upper and a lower portion; a main inlet in said upper portion, and gas or air inlet means connected to said main inlet, the liquid to be purified being introduced together with gas or air in said tank through said main inlet; an outlet located in the lower portion of said tank to drain off the purified liquid and inlets at different heights in the tank connected to said purified liquid outlet, and gas or inlet means connected to said inlets, a portion of the purified liquid being continuously introduced together with air or gas in the tank at said different heights through said inlets.

The drawback of these patents is that none of them solves the problem of providing a reactor and method for improving the purification efficiency while increasing pulp density and cleaning of the light polluting portions.

The main object of the present invention was to provide an apparatus according to a method such as to improve the purification efficiency, with an increase, in the case of paper mixtures de-inking, in the pulp density and the cleaning of the light polluting portions.

These and other objects are achieved by the present reactor having the main feature of consisting in a single cell in whose upper portion the liquid-air mixture is introduced, the purified liquid flowing out from the cell bottom, a portion of the liquid being directed to the use thereof as accepted while a portion thereof is continuously introduced at i; -Icdifferent levels or washing beds of the cell.

Further, a rotating shaft is arranged inside the cell and carries blades shaped so as to stir the liquid and take it inwards to achieve a better washing of the liquid by means of the air in the various washing beds, at which the purified liquid coming from the cell bottom is introduced mixed with air sucked in at the various liquid inlet Cr 4 t t C C a t t c i) 4 o 4I -2levels.

Further characteristics and advantages of the invention will be apparent from the following detailed description of a preferred but not exclusive embodiment thereof, illustrated merely as a non-limiting example in the annexed figures wherein: Fil.1 is a schematic sectional view of the present reactor; Fir.2 is a schematic horizontal cross section of fig.l; and Fiq.3 is an outer side view of the reactor of fig. 1.

Referring to the figures, the present reactor includes a tank 1 within which, in the upper portion thereof, there is located the main inlet 2 of the liquid to be purified which is introduced mixed with a gas or air sucked in through duct 3 inserted into the inlet duct 2. The foam formed by bubbles enclosing the impurities, e.g. ink contained in the liquid introduced in the reactor, is removed by the rotating skimming blade 4 which directs said foam through the outlet duct 5. The skimming blade 4 is cleaned by water jets 6 located above the blade.

4, In the meanwhile, the purified liquid flows down through the outlet 7 C C located at the center of the lower portion of tank 1.

According to the main feature of the present invention, said tank 1 has inlets 8, 9, 10 at different heights, as it can be seen in fig.3, within which simultaneously flows the purified liquid discharged through outlet 7.

Gas or air is sucked in through ducts 11, 12 and 13, respectively inserted into the liquid inlet ducts 8, 9 and A portion of the purified liquid flowing out through outlet 7 is directed 25 upwards according to arrow 7A towards container 14, provided with an internal wall 15, along which the purified liquid flows out through drain 16 i according to arrow 17.

Said tank 1 includes therein a rotating shaft 18 connected to motor 19 for its rotation. Said shaft 18 is provided with blades 20, 21, 22, 23 positioned at the different tank heights forming the washing beds, within which the liquid together with air or gas is introduced, as described above.

Said blades increase in height when moving downwards, and have the function of breaking up the gas-liquid-fiber phase, in the case of paper mixtures, while their different height is due to the fact that the speed of the downflowing liquid increases when moving downwards, i.e. towards the bottom of tank 1. A further characteristic is that said blades are spiralcurved with the concavity facing the direction of the rotating motion of said I-U1~~~r I; D, I -3shaft 18, i.e. according to arrow 24. Moreover, the blade rotation speed can be changed by means of a speed variator, in order to achieve a control of the chemical-physical reactions inside the reactor.

As it is schematically shown in fig.l, The main inlet 2 of the liquid mixed with the gas or air is controlled by valve 25, while the inlets 8-11, 9- 12, 10-13 of the purified liquid mixed with gas or air are controlled by valve 26.

In brief, the operation of the above-described reactor and consequently the method for removing impurities from a liquid embodied by said reactor includes the steps of introducing the liquid mixed with air or gas in the upper portion of tank 1 and further introducing the purified liquid with air or gas simultaneously and continuously at different heights of tank 1 in the various washing beds, said purified liquid coming according to arrow 72 from outlet 7 of tank 1 and letting out a portion of said purified 15 liquid as accepted liquid through drain 16. Furthermore, the stirring of the liquid by means of blades 20, 21, 22, 23 increases when moving down from the upper portion to the lower portion of tank 1, according to the different blade height, as described above, and the liquid is simultaneously pushed towards the central area of tank 1 by the particular spiral shape of blades 20, 21, 22, 23 in order to carry out the washing of the liquid with air each horizontal section of the tank.

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Claims

4. A reactor for removing impurities from a liquid in particular for de-inking, including: a tank having an upper portion and a lower portion; a main inlet in the upper portion, gas or air inlet means connected to said main inlet, said main inlet operable to introduce the liquid to be purified together with gas or air introduced through said gas or air inlet 0 ovV o .ae 9 9* .9 9 0 9 9 9* 9 a..r U C~ li Oti means; an outlet located in the lower portion of said tank to drain off the purified liquid; -in at different heights in the tank connectei t,~iA 1 purified liquid outlet together with a j_ or air introduced through gas or air inlet means connected to said inlets; a rotary shaft provided with blades having progressively increasing heights when moving from the upper portion towards the lower portion of the tank; wherein said blades are at said different heights of the tank where the liquid together with gas or air is introduced through said inlets.
5. A reactor according to claim 4 wherein said blades are spiral-curved with the concavity facing the direction of the rotating motion of said shaft.
6. A reactor for removing impurities from a liquid, in particular for de-inking, including: a tank having an upper portion and a lower portion; a main inlet in the upper portion; gas or air inlet means connected to said main inlet; an outlet located in the lower portion of said tank to drain off the purified liquid; inlets at different heights in the tank connected to said purified liquid outlet and gas or air inlet means for introducing purified liquid together with a gas or air into said tank; a rotary shaft provided with blades in the tank suitable to stir the liquid; and means to rotate said rotary shaft; wherein said blades are spiral-curved with the concavity facing the direction of the rotating motion of said shaft.
7. A method for removing impurities from a liquid including the steps of: providing a tank having an upper and lower portion, a main inlet in the upper portion, an outlet art I Sr -6- located in the lower portion of said tank; introducing gas or air together with the liquid to be purified through said main inlet; providing inlets at different heights in the tank; introducing into said inlets purified liquid drained off from said outlet together with gas or air; and providing in the tank, mechanical rotating a'stirring element suitable to stir the liquid, wherein r' said mechanical rotating stirring element is at said I:CC different heights of the tank where the liquid t i, together with gas or air is introduced through said inlets.
8. A method according to claim 7 including the step of providing said mechanical rotating stirring s relements with a rotating shaft having blades 20 spiral-curved with the concavity facing the C direction of the rotating motion of said shaft. as r 9. Method according to claim 8 including the step of varying the rotation speed of said shaft.
2510. A method according to claim 8 including the step **sees of providing saidblades with progressively increasing heights when moving from the upper portion dtowrdscthen owter raimtion of a. hft 11. A method for removing impurities from a liquid including the steps of: providing a tank having an upper and a lower portion, a main inlet in the upper portion, an outlet located in the lower portion of said tank; 0 0 cc.. 1.Amtodacrigt li 8icuigtese 10 C C q c, i C c c c c 15 -7- introducing gas or air together with the liquid to be purified through said main inlet; providing inlets at different heights in the tank; introducing into said inlets purified liquid draining off from said outlet and gas or air for introducing purified liquid together with gas or air into said tank; and providing a rotating sh&at provided with blades in the tank suitable to stir the liquid, said blades being spiral-curved with the concavity facing the direction of the rotating motion of said shaft. 12. A method according to claim 7 wherein said impurity is ink in a de-inking process. 13. A method according to claim 11 wherein said impurity is ink in a de-inking process. 14. A reactor for removing impurities from a liquid, in particular for de-inking, substantially as hereinbefore described with reference to Figs 1-3. 15. A method for removing impurities from a liquid substantially as hereinbefore described with reference to Figs 1-3. Dated this 15th day of April 1997 CCr C C CC ec Cc C COMER S.p.A. Patent Attorneys for the Applicant: HALFORD CO "REACTOR FOR REMOVING IMPURITIES FROM A LIQUID" ABSTRACT The present invention concerns a reactor for removing impurities from a liquid, in particular for de-inking, including a tank within which the liquid to be purified together with a gas or air is introduced a drain of the purified accepted through an outlet of said tank inlets (8-11, 9-12, 10-13) at different heights of the tank connected to said purified liquid outlet together with the inlet of gas or air; a rotating shaft (18) inside the tank carrying blades (20, 21, 22, 23) at the different heights of the tank within which the liquid together with gas or air is introduced.; the blades (20, 21, 22, 23) have progressively increasing heights when moving towards the lower portion of the tank The 15 invention also concerns the method embodied by the above-described reactor. 4 ,4 4,4,4,' f t c I n