AU560545B2 - Preparation of glyoxylic ester - Google Patents

Preparation of glyoxylic ester

Info

Publication number
AU560545B2
AU560545B2 AU30007/84A AU3000784A AU560545B2 AU 560545 B2 AU560545 B2 AU 560545B2 AU 30007/84 A AU30007/84 A AU 30007/84A AU 3000784 A AU3000784 A AU 3000784A AU 560545 B2 AU560545 B2 AU 560545B2
Authority
AU
Australia
Prior art keywords
acid ester
preparation
entrainer
reaction mixture
oxidative dehydrogenation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
AU30007/84A
Other versions
AU3000784A (en
Inventor
Herbert Baltes
Robert Kenneth Driscoll
Wolfgang Ebertz
Ernst Ingo Leupold
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst AG filed Critical Hoechst AG
Publication of AU3000784A publication Critical patent/AU3000784A/en
Application granted granted Critical
Publication of AU560545B2 publication Critical patent/AU560545B2/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
    • C07C67/313—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by introduction of doubly bound oxygen containing functional groups, e.g. carboxyl groups

Abstract

1. A process for the preparation of a glyoxylic acid ester by catalytic oxidative dehydrogenation of the corresponding glycolic acid ester in the gas phase, which process is characterized by passing, after metering in an entrainer, the gaseous reaction mixture formed in the oxidative dehydrogenation to the central part of a fractionating column, where-upon the reaction mixture cools rapidly, and the water of reaction and other low boilers distil out together with the entrainer overhead, and the glyoxylic acid ester results as the bottom product.
AU30007/84A 1983-06-29 1984-06-28 Preparation of glyoxylic ester Ceased AU560545B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE3323372A DE3323372A1 (en) 1983-06-29 1983-06-29 METHOD FOR PRODUCING A GLYOXYL ACID ESTER
DE3323372 1983-06-29

Publications (2)

Publication Number Publication Date
AU3000784A AU3000784A (en) 1985-01-03
AU560545B2 true AU560545B2 (en) 1987-04-09

Family

ID=6202655

Family Applications (1)

Application Number Title Priority Date Filing Date
AU30007/84A Ceased AU560545B2 (en) 1983-06-29 1984-06-28 Preparation of glyoxylic ester

Country Status (7)

Country Link
EP (1) EP0130533B1 (en)
JP (1) JPS6023345A (en)
AT (1) ATE18759T1 (en)
AU (1) AU560545B2 (en)
CA (1) CA1224216A (en)
DE (2) DE3323372A1 (en)
ZA (1) ZA844935B (en)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2588866B1 (en) * 1985-10-23 1988-01-15 Hoechst France PROCESS FOR THE MANUFACTURE OF ALKYL GLYOXYLATE
US4820385A (en) * 1988-02-18 1989-04-11 Monsanto Company Purification of alkyl glyoxylate in a continuous column by azeotropic distillation
US4867849A (en) * 1988-07-25 1989-09-19 Cova Dario R Purification of alkyl glyoxylate
US4900864A (en) * 1988-08-09 1990-02-13 Anantaneni Prakasa R Manufacture of alkyl glyoxylates with ferric phosphate catalyst
US5217582A (en) * 1990-06-20 1993-06-08 E. I. Du Pont De Nemours And Company Process for the isolation of alkyl glyoxylate
EP0673914A3 (en) * 1994-03-25 1995-11-22 Ube Industries Preparation of alpha-keto acid ester.
JP3150909B2 (en) * 1996-09-05 2001-03-26 株式会社日本触媒 Purification method of glyoxylates
JP2013027475A (en) 2011-07-27 2013-02-07 Brother Ind Ltd Multi-needle sewing machine
CN112354542B (en) * 2020-11-20 2023-07-11 浙江工业大学 V (V) 2 O 5 -CuO/TiO 2 Catalyst, preparation method and application thereof

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE447838C (en) * 1923-03-06 1927-08-08 Boehringer Sohn Ingelheim Process for the production of oxo acid esters and oxo acids
DE2904775C2 (en) * 1979-02-08 1985-03-21 Hoechst Ag, 6230 Frankfurt Process for the preparation of glyoxylic acid esters

Also Published As

Publication number Publication date
JPS6023345A (en) 1985-02-05
DE3323372A1 (en) 1985-01-10
EP0130533A1 (en) 1985-01-09
CA1224216A (en) 1987-07-14
EP0130533B1 (en) 1986-03-26
AU3000784A (en) 1985-01-03
ZA844935B (en) 1985-02-27
ATE18759T1 (en) 1986-04-15
DE3460060D1 (en) 1986-04-30

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