AU5225893A - Synthesis of fluoromethyl ether - Google Patents

Synthesis of fluoromethyl ether

Info

Publication number
AU5225893A
AU5225893A AU52258/93A AU5225893A AU5225893A AU 5225893 A AU5225893 A AU 5225893A AU 52258/93 A AU52258/93 A AU 52258/93A AU 5225893 A AU5225893 A AU 5225893A AU 5225893 A AU5225893 A AU 5225893A
Authority
AU
Australia
Prior art keywords
chlorodifluoromethane
methanol
synthesis
ether
solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
AU52258/93A
Other versions
AU661621B2 (en
Inventor
Robert J. Bulka
Gerald J. O'neill
Felix B. Popper
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hampshire Chemical Corp
Original Assignee
Hampshire Chemical Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hampshire Chemical Corp filed Critical Hampshire Chemical Corp
Publication of AU5225893A publication Critical patent/AU5225893A/en
Application granted granted Critical
Publication of AU661621B2 publication Critical patent/AU661621B2/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/16—Preparation of ethers by reaction of esters of mineral or organic acids with hydroxy or O-metal groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00—Ethers; Compounds having groups, groups or groups
    • C07C43/02—Ethers
    • C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
    • C07C43/04—Saturated ethers
    • C07C43/12—Saturated ethers containing halogen
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

A process for synthesizing difluoromethyl methyl ether for use for example as refrigerants and blowing agents is disclosed. This process involves (1) feeding chlorodifluoromethane through a solution of sodium methoxide in methanol or basic ion exchange resin in methanol at a rate from about 0.5 to 5 grams of feed gas per gram of solution per minute; (2) removing the gaseous product and the unreacted chlorodifluoromethane continuously; and (3) separating difluoromethyl ether from the unreacted chlorodifluoromethane.
AU52258/93A 1992-12-18 1993-12-09 Synthesis of fluoromethyl ether Ceased AU661621B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US07/993,150 US5324864A (en) 1992-12-18 1992-12-18 Synthesis of fluoromethyl ether
US993150 2001-11-06

Publications (2)

Publication Number Publication Date
AU5225893A true AU5225893A (en) 1994-06-30
AU661621B2 AU661621B2 (en) 1995-07-27

Family

ID=25539157

Family Applications (1)

Application Number Title Priority Date Filing Date
AU52258/93A Ceased AU661621B2 (en) 1992-12-18 1993-12-09 Synthesis of fluoromethyl ether

Country Status (15)

Country Link
US (1) US5324864A (en)
EP (1) EP0603002B1 (en)
JP (1) JPH06234685A (en)
KR (1) KR100291046B1 (en)
CN (1) CN1037173C (en)
AT (1) ATE160139T1 (en)
AU (1) AU661621B2 (en)
BR (1) BR9305110A (en)
CA (1) CA2111762A1 (en)
DE (1) DE69315185T2 (en)
ES (1) ES2110580T3 (en)
HU (1) HU216341B (en)
MY (1) MY109614A (en)
TW (1) TW283142B (en)
ZA (1) ZA939297B (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5959158A (en) * 1996-04-12 1999-09-28 Gammill; Ben Method and system for bisphenol a production using water
KR100287364B1 (en) * 1998-09-25 2001-04-16 박호군 Method for producing difluoromethylmethyl ether
CN112552148B (en) * 2020-12-31 2022-05-20 浙江诺亚氟化工有限公司 Resource utilization method of byproduct 2-chloro-1, 1,1,3,3, 3-hexafluoropropane in production process of perfluorohexanone

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2052553A1 (en) * 1990-10-02 1992-04-03 Hampshire Chemical Corp. Synthesis of fluorinated dimethyl ethers
US5278342A (en) * 1992-03-25 1994-01-11 Hampshire Chemical Corp. Vapor phase chlorination of difluoromethyl methyl ether

Also Published As

Publication number Publication date
KR100291046B1 (en) 2001-09-17
AU661621B2 (en) 1995-07-27
HU216341B (en) 1999-06-28
JPH06234685A (en) 1994-08-23
HUT66355A (en) 1994-11-28
DE69315185D1 (en) 1997-12-18
BR9305110A (en) 1994-06-28
CA2111762A1 (en) 1994-06-19
ES2110580T3 (en) 1998-02-16
US5324864A (en) 1994-06-28
ATE160139T1 (en) 1997-11-15
ZA939297B (en) 1994-10-24
DE69315185T2 (en) 1998-03-05
EP0603002A1 (en) 1994-06-22
EP0603002B1 (en) 1997-11-12
CN1037173C (en) 1998-01-28
HU9303620D0 (en) 1994-04-28
KR940014284A (en) 1994-07-18
MY109614A (en) 1997-03-31
CN1096027A (en) 1994-12-07
TW283142B (en) 1996-08-11

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Legal Events

Date Code Title Description
MK14 Patent ceased section 143(a) (annual fees not paid) or expired