AU2021102102A4 - Device for Preparing Polymer Powder - Google Patents

Device for Preparing Polymer Powder Download PDF

Info

Publication number
AU2021102102A4
AU2021102102A4 AU2021102102A AU2021102102A AU2021102102A4 AU 2021102102 A4 AU2021102102 A4 AU 2021102102A4 AU 2021102102 A AU2021102102 A AU 2021102102A AU 2021102102 A AU2021102102 A AU 2021102102A AU 2021102102 A4 AU2021102102 A4 AU 2021102102A4
Authority
AU
Australia
Prior art keywords
smashing chamber
polymer powder
preparing polymer
stated
smashing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
AU2021102102A
Inventor
Yiying Bei
Ling Chen
Narenchaogetu He
Xiaoxun Jin
Fengsheng Li
Miaomiao LI
Jie Liu
Shishuo Liu
Deqi Wang
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Aerospace Chemical Engineering Application Research Institute
Nanjing University of Science and Technology
Hubei Institute of Aerospace Chemical Technology
Original Assignee
Hubei Institute Of Aerospace Chemical Tech
Shanghai Aerospace Chemical Engineering Application Res Institute
Nanjing University of Science and Technology
Hubei Institute of Aerospace Chemical Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hubei Institute Of Aerospace Chemical Tech, Shanghai Aerospace Chemical Engineering Application Res Institute, Nanjing University of Science and Technology, Hubei Institute of Aerospace Chemical Technology filed Critical Hubei Institute Of Aerospace Chemical Tech
Priority to AU2021102102A priority Critical patent/AU2021102102A4/en
Application granted granted Critical
Publication of AU2021102102A4 publication Critical patent/AU2021102102A4/en
Ceased legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C23/00Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
    • B02C23/18Adding fluid, other than for crushing or disintegrating by fluid energy
    • B02C23/24Passing gas through crushing or disintegrating zone
    • B02C23/30Passing gas through crushing or disintegrating zone the applied gas acting to effect material separation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C13/00Disintegrating by mills having rotary beater elements ; Hammer mills
    • B02C13/14Disintegrating by mills having rotary beater elements ; Hammer mills with vertical rotor shaft, e.g. combined with sifting devices
    • B02C13/18Disintegrating by mills having rotary beater elements ; Hammer mills with vertical rotor shaft, e.g. combined with sifting devices with beaters rigidly connected to the rotor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C13/00Disintegrating by mills having rotary beater elements ; Hammer mills
    • B02C13/26Details
    • B02C13/288Ventilating, or influencing air circulation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C23/00Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
    • B02C23/08Separating or sorting of material, associated with crushing or disintegrating
    • B02C23/10Separating or sorting of material, associated with crushing or disintegrating with separator arranged in discharge path of crushing or disintegrating zone
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C23/00Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
    • B02C23/08Separating or sorting of material, associated with crushing or disintegrating
    • B02C23/14Separating or sorting of material, associated with crushing or disintegrating with more than one separator
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/12Powdering or granulating
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2381/00Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing sulfur with or without nitrogen, oxygen, or carbon only; Polysulfones; Derivatives of such polymers
    • C08J2381/04Polysulfides

Landscapes

  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Crushing And Pulverization Processes (AREA)

Abstract

The invention relates to a device for preparing polymer powder, which specifically comprises a smashing chamber, two driving motors, a base, a classification impeller, a cyclone separator, a bag filter, a blower, an induced draft fan and a plumbing installation. The blower is connected to the bottom of the side wall of the smashing chamber and the bottom of the smashing chamber is provided with a base. Besides, the first drive motor is installed inside the base. A connecting shaft is arranged inside the smashing chamber, which passes through the outer wall of the smashing chamber and is connected with the rotating shaft of the first driving motor. The connecting shaft is provided with a pulverizing blade. On the side wall of the smashing chamber, a feed inlet is arranged. The top of the smashing chamber is equipped with a classification impeller, which is connected with the second driving motor below. The classification impeller is further connected to the cyclone separator through a pipe, and the air outlet of the cyclone separator is connected to the bag filter. The device of the invention is simple to operate and easy to realize engineering amplification. FIGURES 1/2 9 12 d7 1 2 3 1 10 6 5 Figure 1 A schematic diagram of the device for preparing ultrafine polymer powder according to the present invention. Figure 2 The SEM image of PPS after comminution in Embodiment 1.

Description

FIGURES
1/2
9 12
12
d7 3 1 10 6 5
Figure 1 A schematic diagram of the device for preparing ultrafine polymer powder
according to the present invention.
Figure 2 The SEM image of PPS after comminution in Embodiment 1.
Device for Preparing Polymer Powder
TECHNICAL FIELD
The invention relates to the technical field of pulverizers, in particular to a preparation
device of polymer powder.
BACKGROUND
In the processing and use of polymer materials, it is often necessary to smash them before
use. Using the dispersibility and processability of polymer powders, it is possible to realize
the compounding of polymer powders with different functions, thereby designing,
researching, and manufacturing high-performance and functional new materials. At
present, as the application field of polymer powder becomes extensive, the requirements
for its particle size and particle size distribution are also increasingly higher. The current
pulverizer can smash some common polymer materials, such as plastic products based on
polypropylene (PP), polyvinyl chloride (PVC), etc. However, there are deficiencies in the
smashed products such as large particle size and wide distribution range. Besides, it cannot
meet the smashing requirements of special polymer materials such as polyphenylene
sulfide (PPS), polyimide (PI), and polyether ether ketone (PEEK). It is much more difficult
to carry out ultrafine comminution of fibers or rubber products.
In addition, the particle size of current device is usually over 100 microns, which cannot
meet the requirements of high-performance structural materials, display devices, high-end
fillers and coatings, new functional materials and other new process materials (such as 3D
printing raw materials). Therefore, it is urgent to develop a device for preparing ultrafine
polymer powder which can prepare high-quality ultrafine polymer powder with average particle size less than 50 microns or even less than 10 microns, so as to meet the needs of new functional materials and structural materials.
SUMMARY
The purpose of the invention is to provide a device for preparing polymer powder.
The technical scheme adopted by the invention is described below.
A device for preparing ultrafine polymer powder is disclosed in the invention, which
specifically comprises a smashing chamber, two driving motors, a base, a classification
impeller, a cyclone separator, a bag filter, a blower, an induced draft fan and a plumbing
installation. The blower is connected to the bottom of the side wall of the smashing
chamber and the bottom of the smashing chamber is provided with a base. Besides, the first
driving motor is installed inside the base. A connecting shaft is arranged inside the
smashing chamber, which passes through the outer wall of the smashing chamber and is
connected with the rotating shaft of the driving motor. The connecting shaft is provided
with a pulverizing blade. On the side wall of the smashing chamber, a feed inlet is arranged.
The top of the smashing chamber is equipped with a classification impeller, which is
connected with the second driving motor below. The classification impeller is further
connected to the cyclone separator through a pipe, and the air outlet of the cyclone separator
is connected to the bag filter.
The basic principle of the invention is as follows. The principle of strong shear
comminution is adopted, and the high-speed rotating blade generates a strong shear
comminution force field, so that the polymer material is rapidly smashed and refined in the
smashing chamber. The refined sample is driven by the air flow to the classification impeller. After separation by the classification impeller, the large particle material falls back to the smashing chamber and is smashed again. The qualified fine powder enters a cyclone separator along with airflow and is separated from air, then is discharged from a discharge port as finished product.
Compared with the existing technology, the invention has following obvious advantages.
1. After being smashed, the polymer material of the invention is sorted by a classification
impeller, so that the uniformity of product granularity can be improved.
2. The airflow from the cyclone separator is dedusted by the bag filter, which improves the
product yield and reduces the dust pollution to the environment.
3. The device of the present invention is multifunctional, which can be used for ultrafine
comminution of plastic polymer materials, as well as ultrafine comminution of fiber and
rubber polymer materials.
4. The device is simple to operate and easy to realize engineering amplification.
BRIEF DESCRIPTION OF THE FIGURES
Figure 1 is a schematic diagram of the device for preparing ultrafine polymer powder
according to the present invention.
Figure 2 is the SEM image of PPS after comminution in Embodiment 1.
Figure 3 is the SEM image of PPS after comminution in Embodiment 2.
In figures, 1- smashing chamber, 2- pulverizing blade, 3- rotating shaft; 4- thefirst driving
motor, 5- base, 6- blower, 7- feed inlet, 8- the second driving motor, 9- classification
impeller, 10- cyclone separator, 11- bag filter, 12- induced draft fan.
DESCRIPTION OF THE INVENTION
The invention will be further described in combination with figures and embodiments
below.
As shown in Fig. 1, the specific embodiment adopts the following technical scheme.
It includes a smashing chamber (1), wherein the bottom of the side wall of the smashing
chamber (1) is connected to a blower (6) through a pipeline. The smashing chamber (1) is
further fixed on a base (5), and the first driving motor (4) is installed inside the base (5).
Inside the smashing chamber (1), a connecting shaft (3) is installed and passes through the
outside wall of the smashing chamber (1) to connect with the shaft of the first driving motor
(4). There is a pulverizing blade (2) arranged on the connecting shaft (3). On the top of the
smashing chamber (1), a classification impeller (9) is installed, and the second driving
motor (8) is connected under the classification impeller (9). A feed inlet (7) is installed on
the side wall of the smashing chamber (1). The classification impeller (9) is connected to
the air inlet of a cyclone separator (10) through a pipe. Moreover, the air outlet of the
cyclone separator (10) is connected with the air inlet of a bag filter (11) through a pipe, and
the air outlet of the bag filter (11) is connected with an induced draft fan (12) through a
pipe.
Further, the outer cylinder of the smashing chamber (1) has a jacket structure, and the
indoor temperature can be controlled by heat conducting liquid.
Moreover, the rotating speed of the classification impeller (9) is adjustable from 0 to
5000rpm, which can classify powder samples with different particle sizes.
Besides, the junction of the connecting shaft (3) and the first driving motor (4) can be
cooled by cooling liquid.
Furthermore, the material of the pulverizing blade (2) can be stainless steel, copper,
aluminium or high-strength alloy, the structure can be serrated, blunt or sharp, and the
rotating speed can be controlled and adjusted at 0-30000rpm.
Ulteriorly, the air supply capacity of the blower (6) and the air induce capacity of the
induced draft fan (12) can be adjusted precisely according to the need.
Besides, the blower (6) can be an air cooler, which controls the temperature of the smashing
chamber and the smashed material.
Further, the cyclone separator (10) can be set in a one-stage or multi-stage series mode.
Furthermore, a vibrating feeder or a screw feeder can be arranged on the feed inlet (7) to
realize the quantitative transportation of materials.
Embodiment 1
1. Weighing 2kg of raw material PPS and adding it into the smashing chamber by a feeder.
2. Starting the pulverizer, wherein the pulverizing blade is made of high-strength alloy, and
the rotating speed of the pulverizing blade is adjusted to 12000rpm to smash PPS.
3. Starting the cooling device and the material temperature during the smashing process is
controlled to be always below 50°C.
4. Starting the classification impeller and adjusting the rotating speed of the classification
impeller to 3500rpm.
5. Starting the blower and induced draft fan, then collecting the smashed materials with a
particle size of about 60 microns.
Embodiment 2
1. Weighing 2kg of raw material PPS and adding it into the smashing chamber by a feeder.
2. Starting the pulverizer, wherein the pulverizing blade is made of high-strength alloy, and
the rotating speed of the pulverizing blade is adjusted to 22000rpm to smash PPS.
3. Starting the cooling device and the material temperature during the smashing process is
controlled to be always below 50°C.
4. Starting the classification impeller and adjusting the rotating speed of the classification
impeller to 4500rpm.
5. Starting the blower and induced draft fan, then collecting the smashed materials with a
particle size of about 20 microns.

Claims (8)

THE CLAIMS DEFINING THE INVENTION ARE AS FOLLOWS:
1. A device for preparing polymer powder, characterized by comprising a smashing
chamber (1), wherein the bottom of the side wall of the smashing chamber (1) is connected
to a blower (6) through a pipeline. The smashing chamber (1) is further fixed on a base (5),
and the first driving motor (4) is installed inside the base (5). Inside the smashing chamber
(1), a connecting shaft (3) is installed and passes through the outside wall of the smashing
chamber (1) to connect with the shaft of the first driving motor (4). There is a pulverizing
blade (2) arranged on the connecting shaft (3). On the top of the smashing chamber (1), a
classification impeller (9) is installed, and the second driving motor (8) is connected under
the classification impeller (9). A feed inlet (7) is installed on the side wall of the smashing
chamber (1). The classification impeller (9) is connected to the air inlet of a cyclone
separator (10) through a pipe. Moreover, the air outlet of the cyclone separator (10) is
connected with the air inlet of a bag filter (11) through a pipe, and the air outlet of the bag
filter (11) is connected with an induced draft fan (12) through a pipe.
2. The device for preparing polymer powder as stated in Claim 1, characterized in that the
outer cylinder of the smashing chamber (1) has a jacket structure, and the indoor
temperature can be controlled by heat conducting liquid.
3. The device for preparing polymer powder as stated in Claim 1, characterized in that the
rotating speed of the classification impeller (9) is adjustable from 0 to 5000rpm, which can
classify powder samples with different particle sizes.
4. The device for preparing polymer powder as stated in Claim 1, characterized in that the
junction of the connecting shaft (3) and the first driving motor (4) can be cooled by cooling
liquid.
5. The device for preparing polymer powder as stated in Claim 1, characterized in that the
material of the pulverizing blade (2) can be stainless steel, copper, aluminium or high
strength alloy, the structure can be serrated, blunt or sharp, and the rotating speed can be
controlled and adjusted at 0-30000rpm.
6. The device for preparing polymer powder as stated in Claim 1, characterized in that the
blower (6) can be an air cooler, which controls the temperature of the smashing chamber
and the smashed material.
7. The device for preparing polymer powder as stated in Claim 1, characterized in that the
cyclone separator (10) can be set in a one-stage or multi-stage series mode.
8. The device for preparing polymer powder as stated in Claim 1, characterized in that a
vibrating feeder or a screw feeder can be arranged on the feed inlet (7) to realize the
quantitative transportation of materials.
FIGURES 21 Apr 2021
1/2 2021102102
Figure 1 A schematic diagram of the device for preparing ultrafine polymer powder
according to the present invention.
Figure 2 The SEM image of PPS after comminution in Embodiment 1.
AU2021102102A 2021-04-21 2021-04-21 Device for Preparing Polymer Powder Ceased AU2021102102A4 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AU2021102102A AU2021102102A4 (en) 2021-04-21 2021-04-21 Device for Preparing Polymer Powder

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
AU2021102102A AU2021102102A4 (en) 2021-04-21 2021-04-21 Device for Preparing Polymer Powder

Publications (1)

Publication Number Publication Date
AU2021102102A4 true AU2021102102A4 (en) 2021-06-24

Family

ID=76442162

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2021102102A Ceased AU2021102102A4 (en) 2021-04-21 2021-04-21 Device for Preparing Polymer Powder

Country Status (1)

Country Link
AU (1) AU2021102102A4 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117797936A (en) * 2024-02-28 2024-04-02 河南亿源建设有限公司 Waste treatment device for construction site

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117797936A (en) * 2024-02-28 2024-04-02 河南亿源建设有限公司 Waste treatment device for construction site
CN117797936B (en) * 2024-02-28 2024-05-03 河南亿源建设有限公司 Waste treatment device for construction site

Similar Documents

Publication Publication Date Title
CN205500791U (en) Shear complete sets who peels off hierarchical preparation graphite alkene in succession
CN103100473B (en) Classification type efficient ultrafine grinder
CN101905186B (en) Cooling Raymond mill and preparation method of powder for pressing graphite products
CN203874876U (en) Low-temperature crushing system
AU2021102102A4 (en) Device for Preparing Polymer Powder
CN111841828A (en) Airflow type lithium hydroxide monohydrate ultrafine grinding equipment and grinding process
CN203108626U (en) Classification type efficient superfine pulverizer
CN209317843U (en) A kind of preparation facilities of high molecular material powder
CN102151538B (en) Self-priming reactor for dispersing nano powder
CN109013007A (en) A kind of preparation facilities of high molecular material powder
CN205129600U (en) Circulating carborundum granule plastic equipment
CN209885960U (en) Hierarchical formula neodymium iron boron fluid energy mill of high accuracy
CN208427168U (en) Discarded cable recovering apparatus
CN110548587A (en) Polycarbonate sheet grinding system and grinding process thereof
CN213434957U (en) Discharge mechanism for superfine pulverizer
CN205392639U (en) Circulated particle crushing equipment of improved generation
JP2003265975A (en) Dry media stirring type pulverizer
CN201482549U (en) Novel powdered rubber pulverizing equipment
CN212974837U (en) Processing equipment for preparing superfine slurry on large scale
CN114289151A (en) High-speed gas crushing device for carbon nano tube
CN210045365U (en) Airflow grading crushing device for laboratory
CN202876883U (en) Totally-enclosed continuous production device for mixed powder material of binder of brake pad
CN2285684Y (en) Plastic powder pulverizator
CN216137342U (en) Environment-friendly is little rubbing crusher for rubbing crusher group
CN212759022U (en) Hierarchical formula impact mill of cereal class food superfine powder

Legal Events

Date Code Title Description
DA3 Amendments made section 104

Free format text: THE NATURE OF THE AMENDMENT IS: AMEND THE NAME OF THE INVENTOR TO READ LIU, JIE; LI, MIAOMIAO; HE, NARENCHAOGETU; BEI, YIYING; JIN, XIAOXUN; WANG, DEQI; CHEN, LING; LIU, SHISHUO AND LI, FENGSHENG

FGI Letters patent sealed or granted (innovation patent)
MK22 Patent ceased section 143a(d), or expired - non payment of renewal fee or expiry