AU2002220693A1 - Method of producing silanes - Google Patents

Method of producing silanes

Info

Publication number
AU2002220693A1
AU2002220693A1 AU2002220693A AU2069302A AU2002220693A1 AU 2002220693 A1 AU2002220693 A1 AU 2002220693A1 AU 2002220693 A AU2002220693 A AU 2002220693A AU 2069302 A AU2069302 A AU 2069302A AU 2002220693 A1 AU2002220693 A1 AU 2002220693A1
Authority
AU
Australia
Prior art keywords
catalyst
disproportionation
methanol
hydrochlorosilanes
reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2002220693A
Inventor
Dr. Hans-Dieter Block
Werner Dick
Stephan Klein
Hans-Joachim Leimkuhler
Dirk Muller
Johannes-Peter Schafer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SolarWorld AG
Original Assignee
SolarWorld AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SolarWorld AG filed Critical SolarWorld AG
Publication of AU2002220693A1 publication Critical patent/AU2002220693A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/04Hydrides of silicon
    • C01B33/043Monosilane
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/08Compounds containing halogen
    • C01B33/107Halogenated silanes
    • C01B33/10773Halogenated silanes obtained by disproportionation and molecular rearrangement of halogenated silanes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)
  • Silicon Polymers (AREA)
  • Silicon Compounds (AREA)

Abstract

The invention relates to a method of producing silane or hydrochlorosilanes by disproportionation of a higher chlorinated hydrochlorosilane or a mixture of said hydrochlorosilanes in the presence of a catalyst. Before the catalyst is used, it is a) washed with hyper-pure water in one or several steps; b) transferred in the water-moist state to the reactor in which the disproportionation is to proceed; c) treated in the reactor with boiling methanol or rinsed with anhydrous methanol; and d) the methanol is removed from the catalyst by evacuation and/or stripping with inert gas. The invention further relates to a method for treating disproportionation catalysts.
AU2002220693A 2000-11-21 2001-11-09 Method of producing silanes Abandoned AU2002220693A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10057519A DE10057519A1 (en) 2000-11-21 2000-11-21 Pretreatment of a catalyst for hydrochlorosilane disproportionation comprises washing with water and treatment with methanol in the disproportionation reactor
DE10057519 2000-11-21
PCT/EP2001/012970 WO2002042206A1 (en) 2000-11-21 2001-11-09 Method of producing silanes

Publications (1)

Publication Number Publication Date
AU2002220693A1 true AU2002220693A1 (en) 2002-06-03

Family

ID=7663967

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2002220693A Abandoned AU2002220693A1 (en) 2000-11-21 2001-11-09 Method of producing silanes

Country Status (6)

Country Link
US (1) US7323155B2 (en)
EP (1) EP1339639B1 (en)
AT (1) ATE276970T1 (en)
AU (1) AU2002220693A1 (en)
DE (2) DE10057519A1 (en)
WO (1) WO2002042206A1 (en)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007059170A1 (en) * 2007-12-06 2009-06-10 Evonik Degussa Gmbh Catalyst and process for dismutating hydrogen halosilanes
RU2011130894A (en) * 2008-12-25 2013-01-27 Токуяма Корпорейшн METHOD FOR PRODUCING CHLOROSILANE
DE102009027728A1 (en) * 2009-07-15 2011-01-20 Evonik Degussa Gmbh Process for the treatment of catalyst precursors
DE102009027730A1 (en) * 2009-07-15 2011-01-27 Evonik Degussa Gmbh Procedure and use of amino-functional resins for dismutation of halosilanes and for removal of foreign metals
US8298490B2 (en) * 2009-11-06 2012-10-30 Gtat Corporation Systems and methods of producing trichlorosilane
WO2012087795A1 (en) 2010-12-20 2012-06-28 Memc Electronic Materials, Inc. Production of polycrystalline silicon in substantially closed-loop processes that involve disproportionation operations
US9352971B2 (en) 2013-06-14 2016-05-31 Rec Silicon Inc Method and apparatus for production of silane and hydrohalosilanes
CN106865553B (en) * 2017-02-16 2019-02-01 亚洲硅业(青海)有限公司 A kind of activation method for the resin catalyst preparing trichlorosilane

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3968199A (en) * 1974-02-25 1976-07-06 Union Carbide Corporation Process for making silane
US4701430A (en) * 1984-05-17 1987-10-20 Korea Advance Institute Of Science & Technology Hydrogenation catalyst and methods for its preparation and use to convert silicon tetrachloride to chlorosilane and silane
JPH0628734B2 (en) * 1985-02-15 1994-04-20 三井東圧化学株式会社 Method for producing halogenated silane disproportionation catalyst
US4725420A (en) * 1985-09-25 1988-02-16 Toa Nenryo Kogyo Kabushiki Kaisha Process for the production of silanes
DE3711444A1 (en) * 1987-04-04 1988-10-13 Huels Troisdorf METHOD AND DEVICE FOR PRODUCING DICHLORSILANE

Also Published As

Publication number Publication date
US7323155B2 (en) 2008-01-29
EP1339639A1 (en) 2003-09-03
EP1339639B1 (en) 2004-09-22
DE50103804D1 (en) 2004-10-28
WO2002042206A1 (en) 2002-05-30
US20040030171A1 (en) 2004-02-12
DE10057519A1 (en) 2002-05-23
ATE276970T1 (en) 2004-10-15

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