AU2001267012A1 - Improved process for the purification and recovery of acetonitrile - Google Patents
Improved process for the purification and recovery of acetonitrileInfo
- Publication number
- AU2001267012A1 AU2001267012A1 AU2001267012A AU6701201A AU2001267012A1 AU 2001267012 A1 AU2001267012 A1 AU 2001267012A1 AU 2001267012 A AU2001267012 A AU 2001267012A AU 6701201 A AU6701201 A AU 6701201A AU 2001267012 A1 AU2001267012 A1 AU 2001267012A1
- Authority
- AU
- Australia
- Prior art keywords
- acetonitrile
- purification
- recovery
- improved process
- side draw
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/24—Preparation of carboxylic acid nitriles by ammoxidation of hydrocarbons or substituted hydrocarbons
- C07C253/26—Preparation of carboxylic acid nitriles by ammoxidation of hydrocarbons or substituted hydrocarbons containing carbon-to-carbon multiple bonds, e.g. unsaturated aldehydes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/24—Preparation of carboxylic acid nitriles by ammoxidation of hydrocarbons or substituted hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/32—Separation; Purification; Stabilisation; Use of additives
- C07C253/34—Separation; Purification
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/20—Power plant
Abstract
A method for the purification of crude acetonitrile comprising distilling the crude acetonitrile in a first fractional distillation column at below atmospheric pressure, withdrawing a first side draw fraction comprising acetonitrile, distilling the first side draw fraction in a second fractional distillation column at super atmospheric pressure, and withdrawing from the second distillation a second side draw fraction comprising purified acetonitrile.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US21886500P | 2000-07-18 | 2000-07-18 | |
US60218865 | 2000-07-18 | ||
PCT/US2001/019709 WO2002006212A2 (en) | 2000-07-18 | 2001-06-21 | Process for the purification and recovery of acetonitrile |
Publications (1)
Publication Number | Publication Date |
---|---|
AU2001267012A1 true AU2001267012A1 (en) | 2002-01-30 |
Family
ID=22816795
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AU2001267012A Abandoned AU2001267012A1 (en) | 2000-07-18 | 2001-06-21 | Improved process for the purification and recovery of acetonitrile |
Country Status (17)
Country | Link |
---|---|
US (1) | US6780289B2 (en) |
EP (1) | EP1301471B1 (en) |
JP (1) | JP4750345B2 (en) |
KR (1) | KR100815093B1 (en) |
CN (1) | CN1206208C (en) |
AT (1) | ATE289290T1 (en) |
AU (1) | AU2001267012A1 (en) |
BR (1) | BR0112548B1 (en) |
CA (1) | CA2415395C (en) |
DE (1) | DE60108962T2 (en) |
DZ (1) | DZ3412A1 (en) |
ES (1) | ES2236251T3 (en) |
MX (1) | MXPA03000452A (en) |
RU (1) | RU2267481C2 (en) |
TW (1) | TWI237631B (en) |
WO (1) | WO2002006212A2 (en) |
ZA (1) | ZA200300416B (en) |
Families Citing this family (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10209632A1 (en) * | 2002-03-02 | 2003-09-11 | Basf Ag | Process for working up tetrahydrofuran by distillation |
US7211674B2 (en) * | 2003-01-07 | 2007-05-01 | Ineos Usa Llc | Process for the recovery of oxazole |
US20090171051A1 (en) * | 2005-10-07 | 2009-07-02 | Mitsui Chemicals, Inc. | Method For Producing Amide Compound |
US20080250418A1 (en) * | 2007-02-08 | 2008-10-09 | Karamchedu Murali M | Health care administration system |
CN101570497B (en) * | 2009-06-15 | 2012-10-24 | 天津市康科德科技有限公司 | Method for purifying high-purity organic solvent acetonitrile for research |
CN102527213B (en) * | 2011-12-15 | 2014-06-25 | 惠生工程(中国)有限公司 | Tail gas treatment method for acetonitrile refining process |
CN104024189B (en) | 2011-12-28 | 2016-01-13 | 旭硝子株式会社 | The purification process of 2,3,3,3-tetrafluoeopropene, purification devices and manufacture method |
WO2014123554A1 (en) * | 2013-02-11 | 2014-08-14 | Gtc Technology Us Llc | A method for reducing energy consumption by thermal coupling |
US10336690B2 (en) * | 2014-02-24 | 2019-07-02 | Honeywell International Inc. | Methods and systems for processing an acetonitrile waste stream |
CN105001055B (en) * | 2015-07-17 | 2017-06-23 | 济南大学 | Based on mixed solvent as extractant isopropanol acetonitrile azeotropic mixture distillation and separation method |
CN106492495A (en) * | 2015-09-07 | 2017-03-15 | 中国石油化工股份有限公司 | Improved vacuum distillation tower and acetonitrile refining system |
WO2020102289A1 (en) | 2018-11-13 | 2020-05-22 | Ascend Performance Materials Operations Llc | Process for recovering acetonitrile from acrylonitrile waste streams |
JP2023542488A (en) * | 2020-09-03 | 2023-10-10 | アセンド・パフォーマンス・マテリアルズ・オペレーションズ・リミテッド・ライアビリティ・カンパニー | How to recover acetonitrile |
KR20230061501A (en) * | 2020-09-04 | 2023-05-08 | 어센드 퍼포먼스 머티리얼즈 오퍼레이션즈 엘엘씨 | How to separate acetonitrile |
KR20220034443A (en) | 2020-09-11 | 2022-03-18 | 주식회사 엘지화학 | Nitrile-based monomer recovery method and solvent recovery apparatus |
CN112479929A (en) * | 2020-12-20 | 2021-03-12 | 湖北佰智昂生物化工有限公司 | Comprehensive utilization method of acetonitrile waste solution |
TW202237560A (en) | 2021-02-11 | 2022-10-01 | 美商阿散德性能材料營運公司 | Acetonitrile separation process |
TW202330462A (en) | 2021-12-20 | 2023-08-01 | 美商阿散德性能材料營運公司 | Acetonitrile separation process |
CN115180756A (en) * | 2022-06-10 | 2022-10-14 | 武汉北湖云峰环保科技有限公司 | Acetonitrile waste liquid purification and recovery device and method |
Family Cites Families (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3073753A (en) * | 1957-10-10 | 1963-01-15 | Distillers Co Yeast Ltd | Recovery of acrylonitrile |
US3196085A (en) * | 1962-02-12 | 1965-07-20 | Du Pont | Process for purifying acrylonitrile |
DE2102886B2 (en) * | 1971-01-22 | 1974-03-14 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Process for obtaining pure acetonitrile |
US4119497A (en) * | 1975-12-01 | 1978-10-10 | Instituto Mexicano Del Petroleo | Process for the purification of acetonitrile |
JPS55104244A (en) * | 1979-02-02 | 1980-08-09 | Asahi Chem Ind Co Ltd | Separation and incineration of crude olefinic unsaturated acetonitrile |
JPS55129257A (en) * | 1979-03-28 | 1980-10-06 | Asahi Chem Ind Co Ltd | Purification of acetonitrile containing hydrogen cyanide |
US4269667A (en) * | 1979-08-02 | 1981-05-26 | Standard Oil Company | Acrylonitrile purification by extractive distillation |
US4362603A (en) * | 1981-01-02 | 1982-12-07 | The Standard Oil Company | Continuous acetonitrile recovery process |
JPS58124751A (en) * | 1982-01-20 | 1983-07-25 | ザ・スタンダ−ド・オイル・カンパニ− | Continuous acetonitrile recovery |
DE3334321A1 (en) * | 1983-09-22 | 1985-04-11 | Lentia GmbH Chem. u. pharm. Erzeugnisse - Industriebedarf, 8000 München | Process for the purification of crude acetonitrile with the recovery of pure prussic acid |
DE3710434A1 (en) * | 1987-03-28 | 1988-10-06 | Basf Ag | METHOD FOR OBTAINING 1,3-BUTADIENE |
JPH1135542A (en) * | 1997-07-09 | 1999-02-09 | Standard Oil Co:The | Purification of acetonitrile by distilling recovery by distillation and ion exchange resin treatment process |
ES2197578T3 (en) * | 1998-02-23 | 2004-01-01 | The Standard Oil Company | IMPROVED PURIFICATION AND RECOVERY OF ACETONITRILE. |
US5869730A (en) * | 1998-05-13 | 1999-02-09 | The Standard Oil Company | Oxidant reduction by manipulation and/or treatment of aqueous acrylonitrile process streams |
US6395142B1 (en) * | 1999-10-14 | 2002-05-28 | Chemcycles, Inc. | Method and apparatus for purifying low grade acetonitrile and other constituents from hazardous waste |
-
2001
- 2001-06-21 CN CNB018129579A patent/CN1206208C/en not_active Expired - Lifetime
- 2001-06-21 EP EP01944621A patent/EP1301471B1/en not_active Expired - Lifetime
- 2001-06-21 KR KR1020037000579A patent/KR100815093B1/en active IP Right Grant
- 2001-06-21 MX MXPA03000452A patent/MXPA03000452A/en active IP Right Grant
- 2001-06-21 AU AU2001267012A patent/AU2001267012A1/en not_active Abandoned
- 2001-06-21 CA CA002415395A patent/CA2415395C/en not_active Expired - Fee Related
- 2001-06-21 BR BRPI0112548-6A patent/BR0112548B1/en not_active IP Right Cessation
- 2001-06-21 AT AT01944621T patent/ATE289290T1/en not_active IP Right Cessation
- 2001-06-21 DE DE60108962T patent/DE60108962T2/en not_active Expired - Lifetime
- 2001-06-21 DZ DZ013412A patent/DZ3412A1/en active
- 2001-06-21 JP JP2002512118A patent/JP4750345B2/en not_active Expired - Fee Related
- 2001-06-21 ES ES01944621T patent/ES2236251T3/en not_active Expired - Lifetime
- 2001-06-21 WO PCT/US2001/019709 patent/WO2002006212A2/en active IP Right Grant
- 2001-06-21 RU RU2003103295/04A patent/RU2267481C2/en active
- 2001-07-12 TW TW090117062A patent/TWI237631B/en not_active IP Right Cessation
- 2001-07-16 US US09/906,299 patent/US6780289B2/en not_active Expired - Lifetime
-
2003
- 2003-01-15 ZA ZA200300416A patent/ZA200300416B/en unknown
Also Published As
Publication number | Publication date |
---|---|
EP1301471B1 (en) | 2005-02-16 |
WO2002006212A2 (en) | 2002-01-24 |
CN1443157A (en) | 2003-09-17 |
KR100815093B1 (en) | 2008-03-20 |
BR0112548A (en) | 2003-09-09 |
WO2002006212A3 (en) | 2002-05-23 |
CA2415395C (en) | 2009-12-01 |
MXPA03000452A (en) | 2004-04-05 |
CN1206208C (en) | 2005-06-15 |
TWI237631B (en) | 2005-08-11 |
ES2236251T3 (en) | 2005-07-16 |
DZ3412A1 (en) | 2002-01-24 |
DE60108962D1 (en) | 2005-03-24 |
KR20030029619A (en) | 2003-04-14 |
EP1301471A2 (en) | 2003-04-16 |
RU2267481C2 (en) | 2006-01-10 |
BR0112548B1 (en) | 2012-07-10 |
US20020043455A1 (en) | 2002-04-18 |
CA2415395A1 (en) | 2002-01-24 |
ZA200300416B (en) | 2003-11-07 |
JP4750345B2 (en) | 2011-08-17 |
JP2004504293A (en) | 2004-02-12 |
DE60108962T2 (en) | 2006-04-06 |
ATE289290T1 (en) | 2005-03-15 |
US6780289B2 (en) | 2004-08-24 |
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