ATE459585T1 - METHOD FOR PRODUCING CHLORINATED CARBONYL COMPOUNDS IN JET LOOP REACTORS - Google Patents
METHOD FOR PRODUCING CHLORINATED CARBONYL COMPOUNDS IN JET LOOP REACTORSInfo
- Publication number
- ATE459585T1 ATE459585T1 AT07120030T AT07120030T ATE459585T1 AT E459585 T1 ATE459585 T1 AT E459585T1 AT 07120030 T AT07120030 T AT 07120030T AT 07120030 T AT07120030 T AT 07120030T AT E459585 T1 ATE459585 T1 AT E459585T1
- Authority
- AT
- Austria
- Prior art keywords
- carbonyl compounds
- jet loop
- chlorinated carbonyl
- loop reactors
- producing chlorinated
- Prior art date
Links
- 150000001728 carbonyl compounds Chemical class 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 238000005660 chlorination reaction Methods 0.000 abstract 2
- FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 abstract 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- 125000004122 cyclic group Chemical group 0.000 abstract 1
- 230000005855 radiation Effects 0.000 abstract 1
- YBBRCQOCSYXUOC-UHFFFAOYSA-N sulfuryl dichloride Chemical compound ClS(Cl)(=O)=O YBBRCQOCSYXUOC-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
- C07C67/307—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by introduction of halogen; by substitution of halogen atoms by other halogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/12—Preparation of carboxylic acid amides by reactions not involving the formation of carboxamide groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
- C07C45/63—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by introduction of halogen; by substitution of halogen atoms by other halogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/06—Systems containing only non-condensed rings with a five-membered ring
- C07C2601/08—Systems containing only non-condensed rings with a five-membered ring the ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Chlorinated or partly chlorinated carbonyl compound production involves introducing unchlorinated or partly chlorinated carbonyl compound in a jet loop reactor for reaction with chlorination medium. A radiation zone (1) loop reactor is used, and one or multiple chlorination mediums, containing chlorine, sulfurylchloride and thionylchloride, are used. The unchlorinated or partly chlorinated carbonyl compounds are introduced in straight chains, in branched manner or in cyclic structure.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102006053380A DE102006053380A1 (en) | 2006-11-13 | 2006-11-13 | Chlorinated or partly chlorinated carbonyl compound production for use in pharma and agro industry, involves introducing unchlorinated or partly chlorinated carbonyl compound in jet loop reactor |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE459585T1 true ATE459585T1 (en) | 2010-03-15 |
Family
ID=38983584
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT07120030T ATE459585T1 (en) | 2006-11-13 | 2007-11-06 | METHOD FOR PRODUCING CHLORINATED CARBONYL COMPOUNDS IN JET LOOP REACTORS |
Country Status (6)
Country | Link |
---|---|
US (1) | US7476772B2 (en) |
EP (1) | EP1923379B1 (en) |
JP (1) | JP4651047B2 (en) |
AT (1) | ATE459585T1 (en) |
DE (2) | DE102006053380A1 (en) |
ES (1) | ES2339986T3 (en) |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
MX2013005560A (en) | 2010-11-23 | 2013-08-26 | Lexington Pharmaceuticals Lab Llc | Low temperature chlorination of carbohydrates. |
DE102011005388A1 (en) | 2011-03-10 | 2012-09-13 | Wacker Chemie Ag | Process for the preparation of polymers by emulsion or suspension polymerization |
SG2013049648A (en) | 2011-10-14 | 2014-12-30 | Lexington Pharmaceuticals Lab Llc | Chlorination of carbohydrates and carbohydrate derivatives |
CN103100428B (en) * | 2011-11-09 | 2015-04-15 | 中国石油化工股份有限公司 | Alumina carrier and its preparation method |
JP5980951B2 (en) | 2012-12-05 | 2016-08-31 | Jxエネルギー株式会社 | Working fluid composition for refrigerator |
JP6459709B2 (en) | 2015-03-27 | 2019-01-30 | セントラル硝子株式会社 | Practical production method of 3,3-difluoro-2-hydroxypropionic acid |
JP6569341B2 (en) * | 2015-07-10 | 2019-09-04 | 住友化学株式会社 | Method for producing 2-haloacetoacetamide |
JP2018534315A (en) | 2015-11-18 | 2018-11-22 | エフ エム シー コーポレーションFmc Corporation | Process for the synthesis of intermediates useful for the preparation of 1,3,4-triazine derivatives |
CN105254583B (en) * | 2015-11-20 | 2017-12-26 | 河北德瑞化工有限公司 | The method that the 5-chloromethyl thiazole of 2 chlorine 5 is prepared using injection circulation reactor |
CN105461529A (en) * | 2015-12-29 | 2016-04-06 | 东南大学 | Preparing method for 1,1,3-trichloroacetone |
DE102016209791A1 (en) * | 2016-06-03 | 2017-12-07 | BSH Hausgeräte GmbH | Device for cooling a liquid, and system for producing a beverage by means of a cooled liquid |
CN108727173B (en) * | 2017-04-19 | 2021-01-01 | 江西天新药业股份有限公司 | Method for preparing 1,1, 3-trichloroacetone |
WO2019146508A1 (en) * | 2018-01-26 | 2019-08-01 | 住友化学株式会社 | Method for producing 2-chloroacetoacetamide |
CN108658871B (en) * | 2018-06-19 | 2020-10-30 | 舞阳威森生物医药有限公司 | Preparation method of sulfadoxine intermediate 4, 6-dichloro-5-methoxypyrimidine |
WO2020014211A1 (en) * | 2018-07-09 | 2020-01-16 | Blue Cube Ip Llc | Eductor nozzle to improve gas hold up in gas-liquid reactor |
MX2022015560A (en) * | 2020-06-08 | 2023-04-05 | Upl Ltd | Process for the preparation of fluoxastrobin and intermediates thereof. |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2036016A (en) * | 1978-11-29 | 1980-06-25 | Ici Ltd | Halogenation of Aliphatic Ethers and Ketones |
DE2946789A1 (en) * | 1978-11-29 | 1980-06-12 | Ici Ltd | METHOD FOR SELECTIVELY CHLORINATING OR BROWNING ALIPHATIC ETHERS AND KETONES |
DE3605484A1 (en) * | 1986-02-20 | 1987-08-27 | Wacker Chemie Gmbh | METHOD FOR PRODUCING 1,1,3-TRICHLORACETONE |
US5177275A (en) * | 1989-05-01 | 1993-01-05 | Pcr Group, Inc. | Reaction of substrate compounds with fluorine in an eductor |
DE19842332B4 (en) | 1998-09-16 | 2011-08-11 | A.S.T. Abwassersysteme Systemtechnologie GmbH, 28359 | Device for the biological purification of wastewater |
DE10010594A1 (en) * | 2000-03-03 | 2001-09-06 | Basf Ag | Production of chloroalkanoyl chlorides, used in synthesis of active pharmaceutical and agrochemical compounds, involves adding boron compound in catalytic chlorination of lactone |
US20030028046A1 (en) * | 2000-03-03 | 2003-02-06 | Armin Stamm | Method for producing chlorocarboxylic acid chlorides |
DE10223649C1 (en) * | 2002-05-28 | 2003-08-14 | Bayer Ag | Preparation of triaryl and trialkyl phosphates, used e.g. as flame retardants, plasticizers, extractants or additives, uses technical grade phosphorus oxyhalide halogenated to pentahalide, then reacted with phenol or alkanol |
KR100452233B1 (en) * | 2002-07-19 | 2004-10-12 | 한국과학기술연구원 | production method of trifluoronitrogen using jet-loop reactors |
DE102004063090A1 (en) * | 2004-12-22 | 2006-07-06 | Uhde Gmbh | Process for the preparation of 1,2-dichloroethane by direct chlorination |
-
2006
- 2006-11-13 DE DE102006053380A patent/DE102006053380A1/en not_active Withdrawn
-
2007
- 2007-11-06 AT AT07120030T patent/ATE459585T1/en active
- 2007-11-06 DE DE502007002988T patent/DE502007002988D1/en active Active
- 2007-11-06 EP EP07120030A patent/EP1923379B1/en not_active Not-in-force
- 2007-11-06 ES ES07120030T patent/ES2339986T3/en active Active
- 2007-11-07 JP JP2007289843A patent/JP4651047B2/en not_active Expired - Fee Related
- 2007-11-13 US US11/938,814 patent/US7476772B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
JP2008120802A (en) | 2008-05-29 |
DE102006053380A1 (en) | 2008-05-15 |
EP1923379A1 (en) | 2008-05-21 |
US7476772B2 (en) | 2009-01-13 |
EP1923379B1 (en) | 2010-03-03 |
ES2339986T3 (en) | 2010-05-27 |
JP4651047B2 (en) | 2011-03-16 |
US20080114196A1 (en) | 2008-05-15 |
DE502007002988D1 (en) | 2010-04-15 |
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