ATE409685T1 - METHOD FOR PRODUCING N-METHYLATED AMINE BY SELECTIVE GAS PHASE AMINATION OF AMINOETHER ALCOHOLS. - Google Patents
METHOD FOR PRODUCING N-METHYLATED AMINE BY SELECTIVE GAS PHASE AMINATION OF AMINOETHER ALCOHOLS.Info
- Publication number
- ATE409685T1 ATE409685T1 AT04018378T AT04018378T ATE409685T1 AT E409685 T1 ATE409685 T1 AT E409685T1 AT 04018378 T AT04018378 T AT 04018378T AT 04018378 T AT04018378 T AT 04018378T AT E409685 T1 ATE409685 T1 AT E409685T1
- Authority
- AT
- Austria
- Prior art keywords
- producing
- gas phase
- selective gas
- methylated amine
- aminoether alcohols
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/10—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C217/00—Compounds containing amino and etherified hydroxy groups bound to the same carbon skeleton
- C07C217/02—Compounds containing amino and etherified hydroxy groups bound to the same carbon skeleton having etherified hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton
- C07C217/04—Compounds containing amino and etherified hydroxy groups bound to the same carbon skeleton having etherified hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
- C07C217/42—Compounds containing amino and etherified hydroxy groups bound to the same carbon skeleton having etherified hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having etherified hydroxy groups and at least two amino groups bound to the carbon skeleton
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
A method for converting amino ether alcohols to amino ether amines by amination in the vapor phase with a catalyst comprising copper and zinc. The catalyst may also comprise an alkali metal, an alkaline earth metal, or a lanthanide element as a promoter.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/634,516 US7009081B2 (en) | 2003-08-04 | 2003-08-04 | N-methylated amines from selective vapor phase amination of amino ether alcohols |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE409685T1 true ATE409685T1 (en) | 2008-10-15 |
Family
ID=33552911
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT04018378T ATE409685T1 (en) | 2003-08-04 | 2004-08-03 | METHOD FOR PRODUCING N-METHYLATED AMINE BY SELECTIVE GAS PHASE AMINATION OF AMINOETHER ALCOHOLS. |
Country Status (9)
Country | Link |
---|---|
US (1) | US7009081B2 (en) |
EP (1) | EP1505059B1 (en) |
JP (1) | JP4105663B2 (en) |
KR (1) | KR100626191B1 (en) |
CN (1) | CN1310871C (en) |
AT (1) | ATE409685T1 (en) |
BR (1) | BRPI0403178A (en) |
DE (1) | DE602004016799D1 (en) |
MX (1) | MXPA04007463A (en) |
Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8143321B2 (en) * | 2006-07-13 | 2012-03-27 | Air Products And Chemicals, Inc. | N,N,N,′-trimethyl-bis-(aminoethyl) ether and its derivatives as catalysts for polyurethanes |
US8290705B2 (en) * | 2007-04-25 | 2012-10-16 | Rio Sisa Idea Farm | Mobile navigation system with graphic crime-risk display |
EP2148742B1 (en) * | 2007-05-08 | 2014-04-16 | Huntsman International LLC | Separation of n,n,n'-trimethylbisaminoethylether from mixtures comprising tertiary amines or tertiary aminoalkylethers |
CN101687972B (en) * | 2007-06-19 | 2012-12-19 | 亨斯迈石油化学有限责任公司 | Reactive amine catalysts for polyurethane foam |
US8563676B2 (en) * | 2007-06-19 | 2013-10-22 | Huntsman Petrochemical Llc | Reactive amine catalysts for polyurethane foam |
ES2427413T3 (en) * | 2009-06-02 | 2013-10-30 | Huntsman Corporation Hungary Zrt. | Method for separating N, N-dialkylbisaminoalkyl ether from mixtures comprising N, N-dialkylbisaminoalkyl ether and at least one of N, N, N'-trialkylbisaminoalkyl ether and N, N, N ', N'-tetraalkylaminoalkyl ether |
CA2874058C (en) * | 2012-07-20 | 2019-10-29 | Koei Chemical Company, Limited | Method for producing 2-(isopropylamino)ethanol |
CN103724210B (en) * | 2012-10-11 | 2016-03-02 | 浙江新化化工股份有限公司 | The production method of N-ethyl-n-butylamine |
EP2862851A1 (en) | 2013-10-15 | 2015-04-22 | Huntsman Corporation Hungary ZRt. | Method for separating N,N,N'-trimethylbisaminoethylether and/or N,N-dimethylbisaminoethylether from a mixture |
FR3013609B1 (en) * | 2013-11-27 | 2017-08-11 | Ifp Energies Now | PROCESS FOR THE CONVERSION OF CARBONYLIC ORGANIC COMPOUNDS AND / OR ALCOHOLS IN THE PRESENCE OF AN ALUMINATE COPPER CATALYST |
CN105837457B (en) * | 2016-03-30 | 2019-04-16 | 河北华茂伟业科技有限公司 | The method that applied metal catalyst synthesizes bis- (dimethylaminoethyl) ethers |
CN107282049A (en) * | 2017-07-06 | 2017-10-24 | 扬州大学 | Al2O3The preparation method and applications of the Cu ZnO interfacial catalysis agent of load |
CN109422902B (en) * | 2017-08-24 | 2021-02-12 | 山东理工大学 | Foaming agent comprising an alkanolamine salt and use in polyurethane continuous panel foam materials |
WO2019120650A1 (en) | 2017-12-20 | 2019-06-27 | Basf Se | Process for the generation of metal-containing films |
CN109761819B (en) * | 2019-01-23 | 2021-12-21 | 浙江新化化工股份有限公司 | Continuous preparation method of N, N-dimethylpropylamine |
CN111205192B (en) * | 2020-01-21 | 2023-01-13 | 新典化学材料(上海)有限公司 | Preparation method of N, N, N' -trimethyl bis (aminoethyl) ether |
CN114433088B (en) * | 2020-10-30 | 2023-07-21 | 中国石油化工股份有限公司 | Catalyst and carrier with function of catalyzing hydro-ammonification of alcohol to generate organic amine, and preparation method and application thereof |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4153581A (en) * | 1977-09-01 | 1979-05-08 | The Dow Chemical Company | Method of producing amines from alcohols, aldehydes, ketones and mixtures thereof |
EP0017651A1 (en) | 1977-08-29 | 1980-10-29 | The Dow Chemical Company | Improved method of producing amines from alcohols, aldehydes, ketones and mixtures thereof and catalyst used |
DE3104738A1 (en) | 1981-02-11 | 1982-08-19 | Basf Ag, 6700 Ludwigshafen | METHOD FOR PRODUCING PERMETHYLATED OLIGOAMINES AND AMINO ALCOHOLS |
JPS59134754A (en) | 1983-01-20 | 1984-08-02 | Nippon Niyuukazai Kk | Preparation of bis(2-(n,n-dimethylamino)ethyl)ether |
US4642381A (en) * | 1983-06-01 | 1987-02-10 | Lehigh University | Catalyst and method for production of methylamines |
US4480131A (en) * | 1983-06-01 | 1984-10-30 | Lehigh University | Process for selective production of di- and tri-alkylamines |
DE3422610A1 (en) | 1984-06-19 | 1985-12-19 | Basf Ag, 6700 Ludwigshafen | METHOD FOR PRODUCING AMINES |
DE3724239A1 (en) * | 1987-07-22 | 1989-02-02 | Basf Ag | METHOD FOR PRODUCING ALIPHATIC N, N-DIALKYL SUBSTITUTED AMINO ALCOHOLS |
JPH0920735A (en) | 1995-07-11 | 1997-01-21 | Tosoh Corp | Amination of alcohol |
US5874483A (en) * | 1995-09-27 | 1999-02-23 | Air Products And Chemicals, Inc. | Aminopropylbis (aminoethyl) ether compositions for the production of polyurethanes |
US5756558A (en) * | 1996-07-03 | 1998-05-26 | Air Products And Chemicals, Inc. | Hydroxyalkylbis(aminoethyl) ether compositions for the production of polyurethanes |
US5824711A (en) * | 1997-05-05 | 1998-10-20 | Air Products And Chemicals, Inc. | N,N,N'-trimethylbis (Aminoethyl) ether substituted urea compostions for the production of polyurethanes |
DE19859776B4 (en) * | 1998-12-23 | 2008-06-19 | Basf Se | Process for the preparation of amines |
US6037496A (en) * | 1999-03-26 | 2000-03-14 | Air Products And Chemicals, Inc. | 3-{N-[2-(N',N'-dimethylamino ethoxy)ethyl]-N-methylamino}propionamide for the production of polyurethanes |
-
2003
- 2003-08-04 US US10/634,516 patent/US7009081B2/en not_active Expired - Fee Related
-
2004
- 2004-07-30 BR BR0403178-4A patent/BRPI0403178A/en not_active IP Right Cessation
- 2004-08-02 MX MXPA04007463A patent/MXPA04007463A/en active IP Right Grant
- 2004-08-02 KR KR1020040060836A patent/KR100626191B1/en not_active IP Right Cessation
- 2004-08-03 AT AT04018378T patent/ATE409685T1/en not_active IP Right Cessation
- 2004-08-03 DE DE602004016799T patent/DE602004016799D1/en active Active
- 2004-08-03 EP EP04018378A patent/EP1505059B1/en not_active Not-in-force
- 2004-08-04 CN CNB2004100558283A patent/CN1310871C/en not_active Expired - Fee Related
- 2004-08-04 JP JP2004228411A patent/JP4105663B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP1505059B1 (en) | 2008-10-01 |
MXPA04007463A (en) | 2005-02-09 |
JP4105663B2 (en) | 2008-06-25 |
KR100626191B1 (en) | 2006-09-20 |
EP1505059A1 (en) | 2005-02-09 |
CN1603303A (en) | 2005-04-06 |
KR20050016092A (en) | 2005-02-21 |
US7009081B2 (en) | 2006-03-07 |
US20050033091A1 (en) | 2005-02-10 |
JP2005053913A (en) | 2005-03-03 |
DE602004016799D1 (en) | 2008-11-13 |
CN1310871C (en) | 2007-04-18 |
BRPI0403178A (en) | 2005-06-14 |
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Legal Events
Date | Code | Title | Description |
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RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |