ATE3879T1 - PRODUCTION OF FRUCTOSE AND USEFUL BY-PRODUCTS. - Google Patents

PRODUCTION OF FRUCTOSE AND USEFUL BY-PRODUCTS.

Info

Publication number
ATE3879T1
ATE3879T1 AT80105981T AT80105981T ATE3879T1 AT E3879 T1 ATE3879 T1 AT E3879T1 AT 80105981 T AT80105981 T AT 80105981T AT 80105981 T AT80105981 T AT 80105981T AT E3879 T1 ATE3879 T1 AT E3879T1
Authority
AT
Austria
Prior art keywords
fructose
calcium
useful
products
treated
Prior art date
Application number
AT80105981T
Other languages
German (de)
Inventor
Stanley Edward Bichsel
Yueh Wang
Andrew M. Sandre
Original Assignee
American Crystal Sugar Company
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by American Crystal Sugar Company filed Critical American Crystal Sugar Company
Application granted granted Critical
Publication of ATE3879T1 publication Critical patent/ATE3879T1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K3/00—Invert sugar; Separation of glucose or fructose from invert sugar
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K11/00—Fructose
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S426/00—Food or edible material: processes, compositions, and products
    • Y10S426/807—Poultry or ruminant feed

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Saccharide Compounds (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

A process for obtaining fructose solutions or solid fructose, a raw material containing sucrose and/or similar fructofuranosides is hydrolyzed to fructose and glucose and treated with a calcium base (e.g. calcium oxide or hydroxide) to precipitate calcium-sugar complexes. The precipitate is slurried in water and then treated with phosphoric acid to liberate (e.g. at a pH of 5.5 to 9) a fructose solution of high purity (i.e. de-complex the calcium-fructose complex), with precipitation of useful calcium phosphate salts. Phosphoric acid has been found to have significant advantages over carbonic acid or carbon dioxide as the fructose-liberating (de-complexing) agent, e.g. better yields and more useful by-products. Solid fructose can be obtained from the fructose solution in a known manner. The filtrate from the calcium-sugar complexing step can be acidified to yield stable, useful, fructose-depleted by-products.
AT80105981T 1979-10-12 1980-10-03 PRODUCTION OF FRUCTOSE AND USEFUL BY-PRODUCTS. ATE3879T1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US06/084,178 US4263052A (en) 1979-10-12 1979-10-12 Production of fructose and useful by-products
EP80105981A EP0028317B1 (en) 1979-10-12 1980-10-03 Production of fructose and useful by-products

Publications (1)

Publication Number Publication Date
ATE3879T1 true ATE3879T1 (en) 1983-07-15

Family

ID=22183328

Family Applications (1)

Application Number Title Priority Date Filing Date
AT80105981T ATE3879T1 (en) 1979-10-12 1980-10-03 PRODUCTION OF FRUCTOSE AND USEFUL BY-PRODUCTS.

Country Status (6)

Country Link
US (1) US4263052A (en)
EP (1) EP0028317B1 (en)
JP (1) JPS5699800A (en)
AT (1) ATE3879T1 (en)
CA (1) CA1146102A (en)
DE (1) DE3063910D1 (en)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4659390A (en) * 1982-07-26 1987-04-21 General Foods Corporation Method and manufacture for moisture-stable, inorganic, microporous saccharide salts
CA1246556A (en) * 1984-07-24 1988-12-13 Hiroshi Yamazaki Production of fructose syrup
US5656094A (en) * 1987-02-02 1997-08-12 A.E. Staley Manufacturing Company Integrated process for producing crystalline fructose and a high-fructose, liquid phase sweetener
US5234503A (en) * 1987-02-02 1993-08-10 A.E. Saley Manufacturing Co. Integrated process for producing crystalline fructose and a high-fructose, liquid-phase sweetener
US5230742A (en) * 1987-02-02 1993-07-27 A. E. Staley Manufacturing Co. Integrated process for producing crystalline fructose and high-fructose, liquid-phase sweetener
US5350456A (en) * 1987-02-02 1994-09-27 A. E. Staley Manufacturing Company Integrated process for producing crystalline fructose and a high fructose, liquid-phase sweetener
US5039346A (en) * 1988-03-25 1991-08-13 A. E. Staley Manufacturing Company Fructose syrups and sweetened beverages
CA2016709A1 (en) * 1989-05-15 1990-11-15 University Of Cincinnati Stable aqueous solution having high concentrations of calcium and phosphate ions and solid complex
US5110363A (en) * 1991-01-17 1992-05-05 The Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College Composition, and method for the clarification of sugar-bearing juices, and related products
CA2122863C (en) * 1994-05-04 1997-05-20 Jacques Jalbert Animal food supplement briquette
US5952205A (en) 1998-02-06 1999-09-14 Neose Technologies, Inc. Process for processing sucrose into glucose and fructose
US5998177A (en) * 1998-11-19 1999-12-07 Neose Technologies, Inc. Process for processing sucrose into glucose
CN100385016C (en) * 2006-06-28 2008-04-30 山东西王糖业有限公司 Crystal fructose production process by corn starch
US8273181B2 (en) * 2007-08-30 2012-09-25 Iogen Energy Corporation Process of removing calcium and obtaining sulfate salts from an aqueous sugar solution
CN101638695B (en) * 2009-08-24 2011-12-14 安徽丰原发酵技术工程研究有限公司 Preparation method of crystalline fructose
MX2017010860A (en) 2015-02-24 2018-01-23 Tate & Lyle Ingredients Americas Llc Allulose syrups.

Family Cites Families (45)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US710413A (en) * 1901-01-18 1902-10-07 Jules Adolphe Besson Process of defecating sugar-juice.
US1699449A (en) * 1922-05-03 1929-01-15 Carbide & Carbon Chem Corp Process and composition for purifying liquids
US1573733A (en) * 1925-06-29 1926-02-16 Ernest R Theriot Process for clarifying saccharine liquors
US1746994A (en) * 1925-10-08 1930-02-11 Sun Maid Raisin Growers Of Cal Raisin sirup and process for making the same
US2007971A (en) * 1926-11-29 1935-07-16 Richard F Jackson Process of making sugar products
US2018869A (en) * 1931-08-15 1935-10-29 California Packing Corp Process of treating sugar solutions
US2227813A (en) * 1939-04-27 1941-01-07 Applied Sugar Lab Inc Treating candy scrap
US2354664A (en) * 1940-08-03 1944-08-01 Corn Product Refining Company Conversion of dextrose to levulose
US2381090A (en) * 1941-02-26 1945-08-07 Mathieson Alkali Works Inc Decolorization of sugar melts
US2362357A (en) * 1941-08-20 1944-11-07 Johns Manville Method for treatment of sugar liquors
US2402960A (en) * 1942-07-22 1946-07-02 Infilco Inc Process of clarifying sugar solutions
US2421376A (en) * 1942-09-11 1947-06-03 Barron Gray Packing Company Preparation of sweetening medium from fruit
US2408418A (en) * 1942-09-11 1946-10-01 Barron Gray Packing Company Fruit treatment
US2416682A (en) * 1942-12-16 1947-03-04 Barron Gray Packing Company Sugar recovery process
US2337853A (en) * 1943-03-15 1943-12-28 Clinton Company Manufacture of dextrose
US2470332A (en) * 1945-09-29 1949-05-17 Great Lakes Carbon Corp Decolorization and clarification of sugar liquors
US2534560A (en) * 1948-07-07 1950-12-19 Int Minerals & Chem Corp Saccharate-ion exchange process
US2668128A (en) * 1949-10-19 1954-02-02 Great Western Sugar Co Process of producing brown sugar
US2588449A (en) * 1950-03-03 1952-03-11 Us Agriculture Levulose dihydrate
US2729587A (en) * 1952-03-11 1956-01-03 Harold J Koepsell Production of fructose
US2813810A (en) * 1954-06-01 1957-11-19 Univ Minnesota Separation of d-glucose and d-fructose
US2949389A (en) * 1958-03-17 1960-08-16 Dawe S Lab Inc Production of levulose
US3050444A (en) * 1959-04-03 1962-08-21 Dawes Lab Inc Method for the production of levulose
US3098766A (en) * 1959-07-20 1963-07-23 Payet Peel Rene Process for clarifying sugar juices by addition of a buffer
US3044905A (en) * 1960-02-15 1962-07-17 Dow Chemical Co Separation of fructose from glucose using cation exchange resin salts
US3044904A (en) * 1960-02-15 1962-07-17 Central Aguirre Sugar Company Separation of dextrose and levulose
NL285289A (en) * 1961-11-11
US3194682A (en) * 1963-04-03 1965-07-13 American Sugar Sugar product and method of producing same
US3306752A (en) * 1963-05-20 1967-02-28 Ueda Kiyomoto Process for producing fructose by fermentation
US3416961A (en) * 1964-01-07 1968-12-17 Colonial Sugar Refining Co Process for the separation of fructose and glucose
US3290173A (en) * 1964-02-03 1966-12-06 Corn Products Co Process for refining unwashed raw cane sugar
US3340093A (en) * 1964-08-20 1967-09-05 Colonial Sugar Refining Co Process for removal of non-sugars from syrups comprising sugars and purified syrups produced thereby
DE1567325C3 (en) * 1965-08-05 1975-06-19 Boehringer Mannheim Gmbh, 6800 Mannheim Process for the production of pure fructose and glucose from sucrose or sucrose-containing invert sugars
US3298865A (en) * 1966-04-18 1967-01-17 Bode Harold Eli Crude sugar liquor defecation process
US3812010A (en) * 1968-03-15 1974-05-21 Laevosan Gmbh & Co Kg Method of producing fructose and glucose from sucrose
US3567512A (en) * 1968-06-17 1971-03-02 Monsanto Co Process for the purification of sugar beet diffusion juice
US3666647A (en) * 1969-02-17 1972-05-30 Tetsujiro Kubo Separation of fructose and glucose
JPS5339492B1 (en) * 1970-02-06 1978-10-21
JPS5420578B1 (en) * 1970-12-09 1979-07-24
US3832284A (en) * 1972-03-30 1974-08-27 Agency Ind Science Techn Method for manufacture of alpha-galactosidase by microorganisms
GB1417344A (en) * 1973-05-11 1975-12-10 Tate & Lyle Ltd Recovery of sucrose
US4040906A (en) * 1976-04-23 1977-08-09 Ajinomoto Co., Inc. Method of producing carbon source for citric acid fermentation
JPS52133915A (en) * 1976-04-30 1977-11-09 Ajinomoto Co Inc Separation method of fructose
GB1585174A (en) * 1976-06-16 1981-02-25 Ici Ltd Separation of sugars from mixtures
US4081288A (en) * 1976-12-13 1978-03-28 Fabcon International, Inc. Sugar clarifying composition

Also Published As

Publication number Publication date
EP0028317A1 (en) 1981-05-13
US4263052A (en) 1981-04-21
DE3063910D1 (en) 1983-07-28
EP0028317B1 (en) 1983-06-22
CA1146102A (en) 1983-05-10
JPS5699800A (en) 1981-08-11

Similar Documents

Publication Publication Date Title
ATE3879T1 (en) PRODUCTION OF FRUCTOSE AND USEFUL BY-PRODUCTS.
SU572201A3 (en) Method of preparing methyl ester of 5-propyltio-2-benzimidazolcarbamic acid
DE3069914D1 (en) Process for the production of d-glucosone and d-fructose
EP0464325A3 (en) Process for the preparation of l-ornithine salts
NO870962L (en) PROCEDURE FOR PREPARING DERMATAN SULPHATE OF HIGH PURITY.
GB1421228A (en) Method for producing sodium citrate dihydrate
KR100214903B1 (en) Process for producing aminomethanephosphonic acid and aminomethylphosphinic acids
GB1439907A (en) Process for the purification of lithium hexafluoroarsenate
NO874346D0 (en) PROCEDURE FOR THE PREPARATION OF BAA HYDROXIC ACID ACID AND SALTS THEREOF.
GB1514807A (en) Process for preparing sulphur dioxide
ES457558A1 (en) Process for the preparation of aminonitrophenols
GB1479731A (en) Process for the production of crystals of monosodium glutamate pentahydrate
GB1394849A (en) 5-dihydrocoriolin c and process for producing the same
ES432505A2 (en) Process for the production of berlin blue
GB1269873A (en) Process for producing ferrous sulphate
GB869948A (en) Process for producing glutamic acid from fermentation broth
ES387549A1 (en) Process for making sodium perborate tetrahydrate
GB1310788A (en) Process for the production of dopa
GB939905A (en) A process for preparing a penillic acid and salts thereof
SU1690317A1 (en) METHOD OF OBTAINING IODIC ACID
GB1530127A (en) Preparation of carboxymethyloxysuccinic acid
GB795941A (en) New streptomycin salt
GB733886A (en) Process of producing glucoheptonic acid and/or calcium glucoheptonate for the preparation of derivatives thereof
PT85759A (en) Process for preparing dimethilglycil-gluconic acid and salts thereof
ES433671A1 (en) Continuous procedure for the production of sodium carbonate peroxide. (Machine-translation by Google Translate, not legally binding)