ATE349T1 - PROCESS FOR THE PREPARATION OF TRIS-(AETHER-AMINE) AND THE TRIS-(AETHER-AMINE) OBTAINED IN THE WAY. - Google Patents
PROCESS FOR THE PREPARATION OF TRIS-(AETHER-AMINE) AND THE TRIS-(AETHER-AMINE) OBTAINED IN THE WAY.Info
- Publication number
- ATE349T1 ATE349T1 AT80400523T AT80400523T ATE349T1 AT E349 T1 ATE349 T1 AT E349T1 AT 80400523 T AT80400523 T AT 80400523T AT 80400523 T AT80400523 T AT 80400523T AT E349 T1 ATE349 T1 AT E349T1
- Authority
- AT
- Austria
- Prior art keywords
- tris
- amine
- aether
- ether
- preparation
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- -1 alkylene glycol Chemical compound 0.000 abstract 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 abstract 2
- RULYNRDLKTTWGC-UHFFFAOYSA-N 2-(2-butoxyethoxy)-n,n-bis[2-(2-butoxyethoxy)ethyl]ethanamine Chemical compound CCCCOCCOCCN(CCOCCOCCCC)CCOCCOCCCC RULYNRDLKTTWGC-UHFFFAOYSA-N 0.000 abstract 1
- XZGIHWAIIZHXKX-UHFFFAOYSA-N 2-(2-ethoxyethoxy)-n,n-bis[2-(2-ethoxyethoxy)ethyl]ethanamine Chemical compound CCOCCOCCN(CCOCCOCC)CCOCCOCC XZGIHWAIIZHXKX-UHFFFAOYSA-N 0.000 abstract 1
- XGLVDUUYFKXKPL-UHFFFAOYSA-N 2-(2-methoxyethoxy)-n,n-bis[2-(2-methoxyethoxy)ethyl]ethanamine Chemical compound COCCOCCN(CCOCCOC)CCOCCOC XGLVDUUYFKXKPL-UHFFFAOYSA-N 0.000 abstract 1
- CAYDJHOYFLLLLM-UHFFFAOYSA-N 2-[2-(2-ethoxyethoxy)ethoxy]-n,n-bis[2-[2-(2-ethoxyethoxy)ethoxy]ethyl]ethanamine Chemical compound CCOCCOCCOCCN(CCOCCOCCOCC)CCOCCOCCOCC CAYDJHOYFLLLLM-UHFFFAOYSA-N 0.000 abstract 1
- 239000004215 Carbon black (E152) Substances 0.000 abstract 1
- 238000005915 ammonolysis reaction Methods 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000006356 dehydrogenation reaction Methods 0.000 abstract 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 1
- 229930195733 hydrocarbon Natural products 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/02—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reactions involving the formation of amino groups from compounds containing hydroxy groups or etherified or esterified hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Glass Compositions (AREA)
- Iron Core Of Rotating Electric Machines (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Abstract
A process of preparing tris-(ether-amines) of the formula: N-[A-O-(B-O)n-R]3 in which R represents a hydrocarbon radical, A and B represent alkanediyl radicals, and n is a whole number between zero and 4, by ammonolysis of an alkylene glycol mono-ether of the formula: HO-A-O-(B-O)n-R in the presence of 10 to 40 percent by weight of a hydrogenation-dehydrogenation catalyst, based on weight of said alkylene glycol monoether. The tris-(ether-amines) produced, such as tris-(3,6-dioxa-octyl)amine, tris-(3,6,9-trioxaundecyl)amine, tris-(3,6-dioxaheptyl)amine, and tris-(3,6-dioxadecyl)amine.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7911100A FR2455570A1 (en) | 1979-05-03 | 1979-05-03 | PROCESS FOR THE PREPARATION OF TRIS (ETHER-AMINES) AND TRIS (ETHER-AMINES) THUS OBTAINED |
| EP80400523A EP0018884B1 (en) | 1979-05-03 | 1980-04-18 | Process for the preparation of tris(ether amines) and so obtained tris(ether amines) |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE349T1 true ATE349T1 (en) | 1981-11-15 |
Family
ID=9224950
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT80400523T ATE349T1 (en) | 1979-05-03 | 1980-04-18 | PROCESS FOR THE PREPARATION OF TRIS-(AETHER-AMINE) AND THE TRIS-(AETHER-AMINE) OBTAINED IN THE WAY. |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US4408075A (en) |
| EP (1) | EP0018884B1 (en) |
| JP (1) | JPS5834464B2 (en) |
| AT (1) | ATE349T1 (en) |
| AU (1) | AU531097B2 (en) |
| BR (1) | BR8002661A (en) |
| CA (1) | CA1133941A (en) |
| DE (1) | DE3060072D1 (en) |
| ES (1) | ES8101036A1 (en) |
| FI (1) | FI801403A7 (en) |
| FR (1) | FR2455570A1 (en) |
| ZA (1) | ZA802564B (en) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5077436A (en) * | 1985-02-22 | 1991-12-31 | Mitsui Toatsu Chemicals, Inc. | Bis(3-aminophenoxy) aromatics and method of preparing the same |
| US4931459A (en) * | 1987-07-14 | 1990-06-05 | Warner-Lambert Company | Method for treating acute respirator distress syndrome |
| US5389134A (en) * | 1994-07-18 | 1995-02-14 | Xerox Corporation | Ink compositions for ink jet printing |
| FR2785607B1 (en) | 1998-11-09 | 2001-02-09 | Rhodia Chimie Sa | PROCESS FOR THE PREPARATION OF TRIS (ETHER-AMINE) |
| US7247606B2 (en) * | 2001-11-05 | 2007-07-24 | Cognis Corporation | Branched reaction products |
| WO2008067857A1 (en) * | 2006-12-06 | 2008-06-12 | Clariant Finance (Bvi) Limited | Process for preparing polyetheramines |
| WO2010139521A1 (en) * | 2009-06-02 | 2010-12-09 | Huntsman Corporation Hungary Zrt. | A method for providing a secondary or tertiary amine |
| US8507704B2 (en) * | 2009-09-08 | 2013-08-13 | Air Products And Chemicals, Inc. | Liquid composition containing aminoether for deposition of metal-containing films |
| CN101948394A (en) * | 2010-09-20 | 2011-01-19 | 浙江博华化学有限公司 | Method for synthesizing tris(dioxa-3,6-heptyl)amine |
| CN108069836B (en) * | 2017-12-19 | 2021-04-13 | 山东博苑医药化学股份有限公司 | Novel method for preparing tri (3, 6-dioxaheptyl) amine |
| CN109289932A (en) * | 2018-10-30 | 2019-02-01 | 中国石油大学(华东) | A kind of nickel-based highly dispersed emulsion catalyst and its preparation method and application |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2285419A (en) * | 1939-03-22 | 1942-06-09 | Eastman Kodak Co | Aliphatic amines |
| US2325514A (en) * | 1941-08-26 | 1943-07-27 | Rohm & Haas | Insecticidal compositions containing polyetheramines |
| US2365721A (en) * | 1941-10-31 | 1944-12-26 | Sharples Chemicals Inc | Manufacture of aliphatic amines |
| US2323658A (en) * | 1942-02-27 | 1943-07-06 | Rohm & Haas | Pyrethrum activated and stabilized with polyetheramines |
| US2355337A (en) * | 1942-08-28 | 1944-08-08 | Rohm & Haas | Preparation of ether amines |
| US2928877A (en) * | 1957-05-10 | 1960-03-15 | Wyandotte Chemicals Corp | Process for preparing oxyalkyleneamines |
| FR1302365A (en) * | 1960-03-04 | 1962-08-31 | Wyandotte Chemicals Corp | Improvements to processes for the amination of glycol ethers |
| US3278598A (en) * | 1963-07-18 | 1966-10-11 | Atlas Chem Ind | Ammonolysis process |
| US3347926A (en) * | 1964-04-15 | 1967-10-17 | Atlas Chem Ind | Ammonolysis process for producing aliphatic amines |
| US4014933A (en) * | 1969-10-23 | 1977-03-29 | Basf Aktiengesellschaft | Production of amines from alcohols |
| DE2555895B2 (en) * | 1975-12-12 | 1978-11-09 | Hoechst Ag, 6000 Frankfurt | Secondary ether amines and processes for their preparation |
-
1979
- 1979-05-03 FR FR7911100A patent/FR2455570A1/en active Granted
-
1980
- 1980-04-18 DE DE8080400523T patent/DE3060072D1/en not_active Expired
- 1980-04-18 AT AT80400523T patent/ATE349T1/en not_active IP Right Cessation
- 1980-04-18 EP EP80400523A patent/EP0018884B1/en not_active Expired
- 1980-04-21 US US06/142,258 patent/US4408075A/en not_active Expired - Lifetime
- 1980-04-29 ZA ZA00802564A patent/ZA802564B/en unknown
- 1980-04-30 BR BR8002661A patent/BR8002661A/en unknown
- 1980-04-30 FI FI801403A patent/FI801403A7/en not_active Application Discontinuation
- 1980-05-01 AU AU57966/80A patent/AU531097B2/en not_active Ceased
- 1980-05-02 ES ES491124A patent/ES8101036A1/en not_active Expired
- 1980-05-02 JP JP55057986A patent/JPS5834464B2/en not_active Expired
- 1980-05-02 CA CA351,183A patent/CA1133941A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| EP0018884B1 (en) | 1981-11-04 |
| CA1133941A (en) | 1982-10-19 |
| US4408075A (en) | 1983-10-04 |
| DE3060072D1 (en) | 1982-01-14 |
| JPS5834464B2 (en) | 1983-07-27 |
| FR2455570A1 (en) | 1980-11-28 |
| EP0018884A1 (en) | 1980-11-12 |
| BR8002661A (en) | 1980-12-09 |
| ES491124A0 (en) | 1980-12-01 |
| AU5796680A (en) | 1980-11-06 |
| FR2455570B1 (en) | 1983-07-22 |
| JPS562943A (en) | 1981-01-13 |
| ES8101036A1 (en) | 1980-12-01 |
| ZA802564B (en) | 1981-05-27 |
| AU531097B2 (en) | 1983-08-11 |
| FI801403A7 (en) | 1980-11-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| UEP | Publication of translation of european patent specification | ||
| REN | Ceased due to non-payment of the annual fee |