ATE282030T1 - RECOVERY AND PURIFICATION OF 3,4 EPOXY 1 BUTENE - Google Patents

RECOVERY AND PURIFICATION OF 3,4 EPOXY 1 BUTENE

Info

Publication number
ATE282030T1
ATE282030T1 AT02765815T AT02765815T ATE282030T1 AT E282030 T1 ATE282030 T1 AT E282030T1 AT 02765815 T AT02765815 T AT 02765815T AT 02765815 T AT02765815 T AT 02765815T AT E282030 T1 ATE282030 T1 AT E282030T1
Authority
AT
Austria
Prior art keywords
epoxybutene
butene
epoxy
recovery
recovering
Prior art date
Application number
AT02765815T
Other languages
German (de)
Inventor
Scott Donald Barnicki
Jerome Leonard Stavinoha Jr
Robert Sterling Kline
Jackie Lee Hamilton
Original Assignee
Eastman Chem Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eastman Chem Co filed Critical Eastman Chem Co
Application granted granted Critical
Publication of ATE282030T1 publication Critical patent/ATE282030T1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/32—Separation; Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • C07D301/10—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Epoxy Compounds (AREA)
  • Gas Separation By Absorption (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Disclosed is a method of recovering and purifying 3,4-epoxy-1-butene (epoxybutene) from a reaction product gas, obtained by the vapor phase catalytic partial oxidation of 1,3-butadiene with oxygen over a silver catalyst. The recovery and purification comprises absorption of the epoxybutene into a water-miscible solvent followed by separation of the absorbed epoxybutene from the absorbent by extraction into a water-immiscible solvent. A method of recovering and purifying epoxybutene from the extraction solvent and other reaction by-products by a novel combination of distillation and decantation steps also is disclosed.
AT02765815T 2001-07-20 2002-07-09 RECOVERY AND PURIFICATION OF 3,4 EPOXY 1 BUTENE ATE282030T1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US09/910,359 US6395913B1 (en) 2001-07-20 2001-07-20 Recovery and purification of 3,4-epoxy-1-butene
PCT/US2002/021584 WO2003008400A1 (en) 2001-07-20 2002-07-09 Recovery and purification of 3,4-epoxy-1-butene

Publications (1)

Publication Number Publication Date
ATE282030T1 true ATE282030T1 (en) 2004-11-15

Family

ID=25428661

Family Applications (1)

Application Number Title Priority Date Filing Date
AT02765815T ATE282030T1 (en) 2001-07-20 2002-07-09 RECOVERY AND PURIFICATION OF 3,4 EPOXY 1 BUTENE

Country Status (7)

Country Link
US (1) US6395913B1 (en)
EP (1) EP1409469B1 (en)
CN (1) CN1533383A (en)
AT (1) ATE282030T1 (en)
DE (1) DE60201916T2 (en)
TW (1) TW574217B (en)
WO (1) WO2003008400A1 (en)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6596882B2 (en) 2001-07-20 2003-07-22 Eastman Chemical Company Recovery and purification of 3,4-epoxy-1-butene using water-miscible solvents
US7475288B2 (en) * 2004-10-05 2009-01-06 Hans Erich Multhaup Accelerated hardware emulation environment for processor-based systems
FR2912416A1 (en) * 2007-02-12 2008-08-15 Primo Pack USE OF A PLASTICIZING RESIN FOR THE PROTECTION OF SURFACES.
US7666299B2 (en) * 2007-08-10 2010-02-23 Amt International, Inc. Extractive distillation process for recovering aromatics from petroleum streams
DE102008028760B9 (en) * 2008-06-17 2010-09-30 Zylum Beteiligungsgesellschaft Mbh & Co. Patente Ii Kg Process for the separation of NOx from an epoxide-containing gas stream
WO2011000830A1 (en) * 2009-06-29 2011-01-06 Shell Internationale Research Maatschappij B.V. Process for the production of ethylene glycol
CN111116516B (en) * 2018-10-30 2022-10-11 中国石油化工股份有限公司 Process for the recovery of alkylene oxide
CN111116518A (en) * 2018-10-30 2020-05-08 中国石油化工股份有限公司 Method for recycling alkylene oxide
CN111116515B (en) * 2018-10-30 2022-11-04 中国石油化工股份有限公司 Alkylene oxide recovery process
US10844295B1 (en) 2019-10-11 2020-11-24 Saudi Arabian Oil Company Systems and processes to deolefinate aromatic-rich hydrocarbon streams
CN114133618B (en) * 2021-10-28 2023-08-22 金发科技股份有限公司 Method for purifying cycloolefin copolymer from plastic reclaimed material

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2773844A (en) 1953-06-12 1956-12-11 Shell Dev Method for making supported silver catalysts
US3418338A (en) 1966-02-28 1968-12-24 Halcon International Inc Water extractive distillation of an ethylene oxide stream containing formaldehyde
BE755247R (en) 1969-09-30 1971-02-25 Halcon International Inc OXIDE RECOVERY PROCESS
US3745092A (en) 1971-01-11 1973-07-10 Shell Oil Co Recovery and purification of ethylene oxide by distillation and absorption
US4012425A (en) 1972-01-07 1977-03-15 Shell Oil Company Ethylene oxide process
US4356312A (en) 1972-01-07 1982-10-26 Shell Oil Company Ethylene oxide process
IT972793B (en) 1972-12-22 1974-05-31 Sir Soc Italiana Resine Spa IMPROVEMENTS IN PROCEDURES FOR THE PREPARATION OF ETHYLENE OXIDE
US3964980A (en) 1975-03-24 1976-06-22 Halcon International, Inc. Process for the recovery of ethylene oxide
US4233221A (en) 1979-10-24 1980-11-11 The Dow Chemical Company Ethylene carbonate process
US4221727A (en) 1979-08-17 1980-09-09 The Dow Chemical Company Ethylene oxide recovery
US4437939A (en) 1981-07-17 1984-03-20 The Halcon Sd Group, Inc. Process for separating ethylene oxide from aqueous solutions
US4437938A (en) 1981-07-17 1984-03-20 The Halcon Sd Group, Inc. Process for recovering ethylene oxide from aqueous solutions
US4950773A (en) 1988-01-28 1990-08-21 Eastman Kodak Company Selective epoxidation of olefins
US4897498A (en) 1988-01-28 1990-01-30 Eastman Kodak Company Selective monoepoxidation of olefins
US5081096A (en) 1990-07-25 1992-01-14 Eastman Kodak Company Epoxidation catalyst
US5117012A (en) * 1991-10-07 1992-05-26 Eastman Kodak Company Recovery of 3,4-epoxy-1-butene from 1,3-butadiene oxidation effluents
DE4241942A1 (en) 1992-12-11 1994-06-16 Basf Ag Process for the preparation of 3,4-epoxy-1-butene
US5312931A (en) * 1993-10-04 1994-05-17 Eastman Chemical Company Recovery of 3,4-epoxy-1-butene from 1,3,-butadiene oxidation effluents
US5559255A (en) 1994-09-08 1996-09-24 Mitsubishi Chemical Corporation Method of recovering ethylene oxide
US5529667A (en) 1994-12-01 1996-06-25 Hoechst Celanese Corporation Process for recovering ethylene oxide
US5756779A (en) * 1997-09-29 1998-05-26 Eastman Chemical Company Recovery of 3,4-epoxy-1-butene from 1,3-butadiene oxidation effluents
US6018061A (en) 1999-05-05 2000-01-25 Eastman Chemical Company Process for recovering 3,4-epoxy-1-butene

Also Published As

Publication number Publication date
EP1409469B1 (en) 2004-11-10
CN1533383A (en) 2004-09-29
US6395913B1 (en) 2002-05-28
TW574217B (en) 2004-02-01
WO2003008400A1 (en) 2003-01-30
DE60201916D1 (en) 2004-12-16
DE60201916T2 (en) 2005-03-31
EP1409469A1 (en) 2004-04-21

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