ATE247631T1 - METHOD FOR PRODUCING ACETONE CYANHYDRIN - Google Patents
METHOD FOR PRODUCING ACETONE CYANHYDRINInfo
- Publication number
- ATE247631T1 ATE247631T1 AT00926732T AT00926732T ATE247631T1 AT E247631 T1 ATE247631 T1 AT E247631T1 AT 00926732 T AT00926732 T AT 00926732T AT 00926732 T AT00926732 T AT 00926732T AT E247631 T1 ATE247631 T1 AT E247631T1
- Authority
- AT
- Austria
- Prior art keywords
- acetone
- gas
- cyanhydrin
- reactor
- hydrogen cyanide
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Acetone-cyanhydrin can be produced in a gas-liquid reactor from a hydrogen cyanide-containing gas, especially the crude gas originating from a methane-ammonia (BMA) or Andrussow process, and acetone in the presence of a base. The aim of the invention is to overcome the disadvantages of the methods for producing acetone-cyanhydrin known from the art. To this end, the gaseous phase removed from the reactor is liberated from the unreacted acetone and hydrogen cyanide in a gas purifier that is operated with a high-boiling solvent, especially with stabilized acetone-cyanhydrin, and the washed phase is fed to the gas-liquid reactor.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19918246A DE19918246A1 (en) | 1999-04-22 | 1999-04-22 | Continuous production of acetone cyanhydrin, used e.g. for production of methacrylate, involves reacting hydrogen cyanide with acetone, scrubbing off-gas with pure acetone cyanhydrin and recycling the wash |
PCT/EP2000/002014 WO2000064861A2 (en) | 1999-04-22 | 2000-03-08 | Method of producing acetone-cyanhydrin |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE247631T1 true ATE247631T1 (en) | 2003-09-15 |
Family
ID=7905469
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT00926732T ATE247631T1 (en) | 1999-04-22 | 2000-03-08 | METHOD FOR PRODUCING ACETONE CYANHYDRIN |
Country Status (7)
Country | Link |
---|---|
US (1) | US6417385B1 (en) |
EP (1) | EP1171420B1 (en) |
JP (1) | JP2002543056A (en) |
AT (1) | ATE247631T1 (en) |
AU (1) | AU4538500A (en) |
DE (2) | DE19918246A1 (en) |
WO (1) | WO2000064861A2 (en) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1371632A1 (en) * | 2002-06-14 | 2003-12-17 | Rohm And Haas Company | Process for producing acetone cyanohydrin |
DE102006058250A1 (en) * | 2006-12-08 | 2008-06-12 | Evonik Röhm Gmbh | Integrated process and apparatus for producing methacrylic acid esters from acetone and hydrocyanic acid |
DE102006058249A1 (en) * | 2006-12-08 | 2008-06-12 | Evonik Röhm Gmbh | Process for the preparation of cyanohydrins and their use in the preparation of methacrylic acid alkyl esters |
DE102006059512A1 (en) * | 2006-12-14 | 2008-06-19 | Evonik Röhm Gmbh | Distillative work-up of acetone cyanohydrin and process for the preparation of methacrylic acid esters and subsequent products |
FR2931477B1 (en) * | 2008-05-21 | 2012-08-17 | Arkema France | CYANHYDRIC ACID DERIVED FROM RENEWABLE RAW MATERIAL |
FR2931822B1 (en) * | 2008-05-30 | 2012-11-02 | Arkema France | BIOMASS - DERIVED METHYL METHACRYLATE, PROCESS FOR PRODUCING THE SAME, USES AND CORRESPONDING POLYMERS. |
ES2526165T3 (en) * | 2011-02-23 | 2015-01-07 | Evonik Degussa Gmbh | Storage stable 2-hydroxy-4- (methylthio) butyric acid nitrile |
DE102011076642A1 (en) | 2011-05-27 | 2012-11-29 | Evonik Röhm Gmbh | Process for the preparation of methacrylic acid |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1257765B (en) | 1960-10-29 | 1968-01-04 | Degussa | Process for the production of acetone cyanohydrin |
US3700718A (en) | 1969-11-24 | 1972-10-24 | Sumitomo Chemical Co | Method for continuous production of pure acetone cyanohydrin |
DE3933207A1 (en) | 1989-10-05 | 1991-04-18 | Degussa | PROCESS FOR CLEANING ROH CYANHYDRINES WITH 3 TO 6 CARBON ATOMES |
-
1999
- 1999-04-22 DE DE19918246A patent/DE19918246A1/en not_active Withdrawn
-
2000
- 2000-03-08 JP JP2000613814A patent/JP2002543056A/en active Pending
- 2000-03-08 US US09/959,271 patent/US6417385B1/en not_active Expired - Lifetime
- 2000-03-08 WO PCT/EP2000/002014 patent/WO2000064861A2/en active IP Right Grant
- 2000-03-08 AT AT00926732T patent/ATE247631T1/en not_active IP Right Cessation
- 2000-03-08 AU AU45385/00A patent/AU4538500A/en not_active Abandoned
- 2000-03-08 DE DE50003363T patent/DE50003363D1/en not_active Expired - Lifetime
- 2000-03-08 EP EP00926732A patent/EP1171420B1/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
WO2000064861A3 (en) | 2001-05-03 |
WO2000064861A2 (en) | 2000-11-02 |
DE19918246A1 (en) | 2000-10-26 |
JP2002543056A (en) | 2002-12-17 |
EP1171420A2 (en) | 2002-01-16 |
DE50003363D1 (en) | 2003-09-25 |
EP1171420B1 (en) | 2003-08-20 |
AU4538500A (en) | 2000-11-10 |
US6417385B1 (en) | 2002-07-09 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
REN | Ceased due to non-payment of the annual fee |