ATE187200T1 - METHOD FOR PRODUCING SURFACTANT GRANULES - Google Patents
METHOD FOR PRODUCING SURFACTANT GRANULESInfo
- Publication number
- ATE187200T1 ATE187200T1 AT93920800T AT93920800T ATE187200T1 AT E187200 T1 ATE187200 T1 AT E187200T1 AT 93920800 T AT93920800 T AT 93920800T AT 93920800 T AT93920800 T AT 93920800T AT E187200 T1 ATE187200 T1 AT E187200T1
- Authority
- AT
- Austria
- Prior art keywords
- neutralization
- anionic surfactant
- granulation
- simultaneous
- drying
- Prior art date
Links
- 239000008187 granular material Substances 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 239000004094 surface-active agent Substances 0.000 title 1
- 239000003945 anionic surfactant Substances 0.000 abstract 4
- 239000002253 acid Substances 0.000 abstract 3
- -1 fatty alcohol sulfonic acids Chemical class 0.000 abstract 3
- 238000005469 granulation Methods 0.000 abstract 3
- 230000003179 granulation Effects 0.000 abstract 3
- 238000006386 neutralization reaction Methods 0.000 abstract 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 abstract 2
- 238000001035 drying Methods 0.000 abstract 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract 1
- 229910021536 Zeolite Inorganic materials 0.000 abstract 1
- 239000003599 detergent Substances 0.000 abstract 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 229910000029 sodium carbonate Inorganic materials 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
- 239000010457 zeolite Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
- C11D17/065—High-density particulate detergent compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Compounds Of Unknown Constitution (AREA)
Abstract
Detergent anionic surfactant granules of high anionic surfactant content can be produced by neutralization of anionic surfactants in their acid form using a powdered neutralizer, with simultaneous granulation and, as needed, simultaneous drying. Preferably this involves the neutralization of fatty alcohol sulfonic acids, alkyl benzene-sulfonic acids and/or (alpha)-alkylsulfonic acid methyl ester acids with an excess of sodium carbonate, and the simultaneous granulation with other liquid components, in particular with anionic surfactant pastes, aqueous hydrogen peroxide solution and/or a zeolite suspension. This production can be effected in any apparatus in which neutralization can be carried out simultaneously with granulation and drying. Preferably this preparation takes place in a continuous fluidized bed system.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4232874A DE4232874A1 (en) | 1992-09-30 | 1992-09-30 | Process for the preparation of surfactant granules |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE187200T1 true ATE187200T1 (en) | 1999-12-15 |
Family
ID=6469291
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT93920800T ATE187200T1 (en) | 1992-09-30 | 1993-09-22 | METHOD FOR PRODUCING SURFACTANT GRANULES |
Country Status (6)
Country | Link |
---|---|
EP (1) | EP0663005B1 (en) |
CN (1) | CN1087945A (en) |
AT (1) | ATE187200T1 (en) |
DE (2) | DE4232874A1 (en) |
ES (1) | ES2140467T3 (en) |
WO (1) | WO1994007990A1 (en) |
Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4304015A1 (en) * | 1993-02-11 | 1994-08-18 | Henkel Kgaa | Process for the production of granules |
DE4314885A1 (en) * | 1993-05-05 | 1994-11-10 | Sued Chemie Ag | Process for neutralizing the acid form of anionic surfactants, agglomerates and detergents obtained thereafter |
GB9313878D0 (en) * | 1993-07-05 | 1993-08-18 | Unilever Plc | Detergent composition or component containing anionic surfactant and process for its preparation |
GB9415904D0 (en) * | 1994-08-05 | 1994-09-28 | Unilever Plc | Process for the production of detergent composition |
TW397862B (en) * | 1996-09-06 | 2000-07-11 | Kao Corp | Detergent granules and method for producing the same, and high-bulk density detergent composition |
GB9712583D0 (en) | 1997-06-16 | 1997-08-20 | Unilever Plc | Production of detergent granulates |
GB9712580D0 (en) * | 1997-06-16 | 1997-08-20 | Unilever Plc | Production of detergent granulates |
GB9713748D0 (en) * | 1997-06-27 | 1997-09-03 | Unilever Plc | Production of detergent granulates |
DE19822943A1 (en) * | 1998-05-22 | 1999-11-25 | Henkel Kgaa | Preparation of high bulk density detergents or washing compositions without need for spray drying |
DE19844523A1 (en) | 1998-09-29 | 2000-03-30 | Henkel Kgaa | Granulation process |
DE19851454B4 (en) * | 1998-11-09 | 2010-11-04 | Henkel Ag & Co. Kgaa | Surfactant granules by fluidized bed granulation |
GB9825563D0 (en) | 1998-11-20 | 1999-01-13 | Unilever Plc | Particulate laundry detergent compositions containing anionic surfactant granules |
DE10163603B4 (en) * | 2001-12-21 | 2006-05-04 | Henkel Kgaa | Process for the preparation of builder-containing surfactant granules |
DE10258011A1 (en) * | 2002-12-12 | 2004-07-08 | Henkel Kgaa | Dry neutralization process |
DE102005005499A1 (en) * | 2005-02-04 | 2006-08-17 | Henkel Kgaa | Process for the preparation of detergents or cleaners |
WO2011061045A1 (en) | 2009-11-20 | 2011-05-26 | Unilever Nv | Detergent granule and its manufacture |
CN103820253B (en) * | 2014-02-12 | 2016-06-01 | 浙江赞宇科技股份有限公司 | Technique and the device of powdery MES particle is prepared in a kind of serialization |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ZA72295B (en) * | 1971-02-01 | 1973-09-26 | Colgate Palmolive Co | Method for neutralization of detergent acid |
JPS6187657A (en) * | 1984-10-05 | 1986-05-06 | Kao Corp | Preparation of alpha-sulfo-fatty acid ester salt |
US4734224A (en) * | 1986-09-15 | 1988-03-29 | The Dial Corporation | Dry neutralization process for detergent slurries |
GB2209172A (en) * | 1987-08-28 | 1989-05-04 | Unilever Plc | Preparation of solid particulate components for detergents |
IN170991B (en) * | 1988-07-21 | 1992-06-27 | Lever Hindustan Ltd | |
GB8818613D0 (en) * | 1988-08-05 | 1988-09-07 | Paterson Zochonis Uk Ltd | Detergents |
-
1992
- 1992-09-30 DE DE4232874A patent/DE4232874A1/en not_active Ceased
-
1993
- 1993-09-22 WO PCT/EP1993/002567 patent/WO1994007990A1/en active IP Right Grant
- 1993-09-22 AT AT93920800T patent/ATE187200T1/en not_active IP Right Cessation
- 1993-09-22 ES ES93920800T patent/ES2140467T3/en not_active Expired - Lifetime
- 1993-09-22 EP EP93920800A patent/EP0663005B1/en not_active Expired - Lifetime
- 1993-09-22 DE DE59309891T patent/DE59309891D1/en not_active Expired - Lifetime
- 1993-09-29 CN CN93118176A patent/CN1087945A/en active Pending
Also Published As
Publication number | Publication date |
---|---|
ES2140467T3 (en) | 2000-03-01 |
DE59309891D1 (en) | 2000-01-05 |
CN1087945A (en) | 1994-06-15 |
EP0663005A1 (en) | 1995-07-19 |
DE4232874A1 (en) | 1994-03-31 |
WO1994007990A1 (en) | 1994-04-14 |
EP0663005B1 (en) | 1999-12-01 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
REN | Ceased due to non-payment of the annual fee |