AR092298A1 - PROCESS TO OBTAIN CONCENTRATED PROTEINS OF SOYBEAN FROM THE POROTO BY EXTRACTION WITH ALCOHOL, OBTAINING A HIGH PROTEIN FLOUR WITHOUT ANTI-NUTRITIONAL FACTORS AND A HIGH QUALITY OIL - Google Patents

PROCESS TO OBTAIN CONCENTRATED PROTEINS OF SOYBEAN FROM THE POROTO BY EXTRACTION WITH ALCOHOL, OBTAINING A HIGH PROTEIN FLOUR WITHOUT ANTI-NUTRITIONAL FACTORS AND A HIGH QUALITY OIL

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Publication number
AR092298A1
AR092298A1 ARP130100199A ARP130100199A AR092298A1 AR 092298 A1 AR092298 A1 AR 092298A1 AR P130100199 A ARP130100199 A AR P130100199A AR P130100199 A ARP130100199 A AR P130100199A AR 092298 A1 AR092298 A1 AR 092298A1
Authority
AR
Argentina
Prior art keywords
ethanol
oil
carbohydrates
water
separation
Prior art date
Application number
ARP130100199A
Other languages
Spanish (es)
Original Assignee
Palacios Luis Eduardo
Allocco Mario Domingo
Allocco Mariana Carla
Guala Mirta Bernarda
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Palacios Luis Eduardo, Allocco Mario Domingo, Allocco Mariana Carla, Guala Mirta Bernarda filed Critical Palacios Luis Eduardo
Priority to ARP130100199A priority Critical patent/AR092298A1/en
Priority to PCT/IB2014/058325 priority patent/WO2014115067A1/en
Publication of AR092298A1 publication Critical patent/AR092298A1/en

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23JPROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J1/00Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
    • A23J1/14Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds
    • A23J1/142Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds by extracting with organic solvents
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23JPROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J3/00Working-up of proteins for foodstuffs
    • A23J3/14Vegetable proteins
    • A23J3/16Vegetable proteins from soybean
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23JPROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J7/00Phosphatide compositions for foodstuffs, e.g. lecithin
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L11/00Pulses, i.e. fruits of leguminous plants, for production of food; Products from legumes; Preparation or treatment thereof
    • A23L11/05Mashed or comminuted pulses or legumes; Products made therefrom
    • A23L11/07Soya beans, e.g. oil-extracted soya bean flakes
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L11/00Pulses, i.e. fruits of leguminous plants, for production of food; Products from legumes; Preparation or treatment thereof
    • A23L11/30Removing undesirable substances, e.g. bitter substances
    • A23L11/32Removing undesirable substances, e.g. bitter substances by extraction with solvents
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/10Production of fats or fatty oils from raw materials by extracting

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Nutrition Science (AREA)
  • Organic Chemistry (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Agronomy & Crop Science (AREA)
  • Botany (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Fats And Perfumes (AREA)
  • Beans For Foods Or Fodder (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

Proceso para producir una harina de soja de proteína, baja cantidad de carbohidratos solubles y reducida cantidad de aceite donde se utiliza etanol como único solvente y diluciones acuosas del mismo, no requiere destilación para la separación del aceite, donde la harina de soja de proteína concentrada se obtiene con un solo tratamiento térmico de desolventización y que comprende las siguientes etapas: A) preparación del poroto de soja para su tratamiento mediante limpieza; quebrado y descascarado de porotos de soja, separación de la cáscara y laminado de los porotos de soja descascarados, obteniéndose un material laminado de poroto de soja; B) embebido y expansión del material de soja obtenido en la etapa A con una solución de etanol y aceite, con aproximadamente 20% aceite; C) extracción con etanol de aceites y fosfolípidos del material de soja obtenido en la etapa B por percolación del etanol y las mezclas (miscellas) de etanol-aceite de concentraciones decrecientes en contracorriente a través del material de soja; D) embebido y expansión del material sólido de soja obtenido en la etapa C con una mezcla de etanol-agua y carbohidratos, que contiene hasta 5% de carbohidratos; E) extracción con etanol-agua de los carbohidratos del material de soja desgrasado obtenido en la etapa C por percolación de etanol-agua y las mezclas de etanol-agua-carbohidratos de concentración decreciente en contracorriente a través de dicho material de soja desgrasado; F) separación del aceite de soja del etanol en la solución etanol-aceite obtenida en la etapa C mediante un método no destilativo; G) acondicionamiento del etanol obtenido en la etapa F para su reutilización en ciclo cerrado; H) separación de fosfolípidos y otras impurezas del aceite obtenido en la etapa F; I) separación de los carbohidratos del etanol-agua de la solución carbohidratos-etanol-agua obtenida en la etapa E obteniéndose melazas y etanol que vuelve al proceso; J) separación, concentración y fermentación de las melazas formadas por los hidratos de carbono obtenidos en la etapa I para producir etanol; K) opcionalmente en la etapa J se pueden separar las isoflavonas de las melazas previo a su fermentación; L) obtención de harina de soja de proteína concentrada libre de factores antinutricionales, apta para consumo humano y animal y la producción de aislados de soja, donde en dicho proceso se utiliza como único solvente etanol puro y diluciones en agua, y donde dicho proceso se realiza sin una etapa intermedia de desolventización.Process to produce a protein soybean meal, low amount of soluble carbohydrates and reduced amount of oil where ethanol is used as the sole solvent and aqueous dilutions thereof, does not require distillation for oil separation, where the concentrated protein soybean meal it is obtained with a single heat treatment of desolventization and that includes the following stages: A) preparation of the soy bean for treatment by cleaning; cracking and shelling of soybeans, peel separation and rolling of peeled soybeans, obtaining a soy bean laminate material; B) embedding and expanding the soy material obtained in step A with a solution of ethanol and oil, with approximately 20% oil; C) extraction with ethanol of oils and phospholipids of the soy material obtained in stage B by percolation of the ethanol and the mixtures (miscelles) of ethanol-oil of decreasing concentrations in countercurrent through the soy material; D) embedding and expanding the solid soy material obtained in step C with a mixture of ethanol-water and carbohydrates, which contains up to 5% carbohydrates; E) extraction with ethanol-water of the carbohydrates of the defatted soy material obtained in step C by percolation of ethanol-water and the ethanol-water-carbohydrate mixtures of decreasing concentration in countercurrent through said defatted soy material; F) separation of soybean oil from ethanol in the ethanol-oil solution obtained in step C by a non-distillative method; G) conditioning of the ethanol obtained in step F for reuse in a closed cycle; H) separation of phospholipids and other impurities from the oil obtained in step F; I) separation of the carbohydrates from the ethanol-water from the carbohydrates-ethanol-water solution obtained in step E obtaining molasses and ethanol that returns to the process; J) separation, concentration and fermentation of molasses formed by the carbohydrates obtained in stage I to produce ethanol; K) optionally in step J the isoflavones can be separated from the molasses prior to fermentation; L) obtaining concentrated protein soybean meal free of antinutritional factors, suitable for human and animal consumption and the production of soy isolates, where in this process pure ethanol and water dilutions are used as the sole solvent, and where said process is performed without an intermediate stage of desolventization.

ARP130100199A 2013-01-23 2013-01-23 PROCESS TO OBTAIN CONCENTRATED PROTEINS OF SOYBEAN FROM THE POROTO BY EXTRACTION WITH ALCOHOL, OBTAINING A HIGH PROTEIN FLOUR WITHOUT ANTI-NUTRITIONAL FACTORS AND A HIGH QUALITY OIL AR092298A1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
ARP130100199A AR092298A1 (en) 2013-01-23 2013-01-23 PROCESS TO OBTAIN CONCENTRATED PROTEINS OF SOYBEAN FROM THE POROTO BY EXTRACTION WITH ALCOHOL, OBTAINING A HIGH PROTEIN FLOUR WITHOUT ANTI-NUTRITIONAL FACTORS AND A HIGH QUALITY OIL
PCT/IB2014/058325 WO2014115067A1 (en) 2013-01-23 2014-01-16 Method for obtaining soybean protein concentrate from soy meal by means of extraction with alcohol, obtaining a high-protein flour without antinutritional factors and a high-quality oil

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ARP130100199A AR092298A1 (en) 2013-01-23 2013-01-23 PROCESS TO OBTAIN CONCENTRATED PROTEINS OF SOYBEAN FROM THE POROTO BY EXTRACTION WITH ALCOHOL, OBTAINING A HIGH PROTEIN FLOUR WITHOUT ANTI-NUTRITIONAL FACTORS AND A HIGH QUALITY OIL

Publications (1)

Publication Number Publication Date
AR092298A1 true AR092298A1 (en) 2015-04-15

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
ARP130100199A AR092298A1 (en) 2013-01-23 2013-01-23 PROCESS TO OBTAIN CONCENTRATED PROTEINS OF SOYBEAN FROM THE POROTO BY EXTRACTION WITH ALCOHOL, OBTAINING A HIGH PROTEIN FLOUR WITHOUT ANTI-NUTRITIONAL FACTORS AND A HIGH QUALITY OIL

Country Status (2)

Country Link
AR (1) AR092298A1 (en)
WO (1) WO2014115067A1 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10264805B2 (en) 2015-04-23 2019-04-23 Nutriati, Inc. Dry fractionation for plant based protein extraction
BR102015031383B8 (en) * 2015-12-15 2023-04-25 Fernandes De Siqueira Machado Paula INDUSTRIAL PROCESS FOR PHOSPHOLIPID RECOVERY AND LECITIN PRODUCTION FROM A WASTE FROM THE PRODUCTION OF SOY PROTEIN CONCENTRATE (SPC)
BR102017021876B1 (en) * 2017-10-10 2022-12-20 Rio Pardo Bioenergia S.A SOYBEAN MEAL PRODUCTION PROCESS WITH HIGH CONTENT OF SOLUBLE PROTEINS
CN110951817A (en) * 2019-12-20 2020-04-03 青岛海科生物技术有限公司 Production method of concentrated protein special for efficient fermentation

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1583991A (en) * 1978-05-26 1981-02-04 Unilever Ltd Proteinaceous foodstuffs
US4219470A (en) * 1978-10-23 1980-08-26 Dravo Corporation Process for preparing a protein concentrate and the product obtained thereby
EP1320299B1 (en) * 2001-08-22 2005-06-08 Solae L.L.C. Soybean meal with a reduced fat and soluble sugar content, and methods of making and using the same

Also Published As

Publication number Publication date
WO2014115067A1 (en) 2014-07-31

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