US819751A - Process of charging silk. - Google Patents
Process of charging silk. Download PDFInfo
- Publication number
- US819751A US819751A US23965405A US1905239654A US819751A US 819751 A US819751 A US 819751A US 23965405 A US23965405 A US 23965405A US 1905239654 A US1905239654 A US 1905239654A US 819751 A US819751 A US 819751A
- Authority
- US
- United States
- Prior art keywords
- silk
- charging
- acid
- sulfo
- charged
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 238000004043 dyeing Methods 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 239000002253 acid Substances 0.000 description 3
- GVCGWXSZNUOTDW-UHFFFAOYSA-N sulfo cyanate Chemical compound OS(=O)(=O)OC#N GVCGWXSZNUOTDW-UHFFFAOYSA-N 0.000 description 3
- ZMZDMBWJUHKJPS-UHFFFAOYSA-N thiocyanic acid Chemical compound SC#N ZMZDMBWJUHKJPS-UHFFFAOYSA-N 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 230000004075 alteration Effects 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- FESBVLZDDCQLFY-UHFFFAOYSA-N sete Chemical compound [Te]=[Se] FESBVLZDDCQLFY-UHFFFAOYSA-N 0.000 description 1
- BZWKPZBXAMTXNQ-UHFFFAOYSA-N sulfurocyanidic acid Chemical compound OS(=O)(=O)C#N BZWKPZBXAMTXNQ-UHFFFAOYSA-N 0.000 description 1
- 150000003606 tin compounds Chemical class 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/20—Halides of elements of Groups 4 or 14 of the Periodic Table, e.g. zirconyl chloride
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S8/00—Bleaching and dyeing; fluid treatment and chemical modification of textiles and fibers
- Y10S8/916—Natural fiber dyeing
- Y10S8/917—Wool or silk
Definitions
- the application of the sulfo-cyanic acid and of its salts is effected during the operations of charging, dyeing, or clearing by means of a diluted solution, (varying from 0,5 to three per cent. and more.) Having exposed to the action of light for ten days some small skeins of silk (organzin) charged with thirty per cent. in excess of its original weight, a portion of which had been subjected after dyeing to clearing by the aid of one per cent. of sulfo-cyanate of ammonia rendered acid by means of sulfuric acid, whilethe other portion had been cleared or brightened by the ordinary method in an acid bath by means of 1:1,000 (one per thousand) of sulfuric acid, the following results were obtained:
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Coloring (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Description
GIUSEPPE GIANOLI, OF MILAN, ITALY.
PROCESS OF CHARGING SILK.
Specification of Letters Patent.
Patented May 8, 1906.
Application filed January 4,1905. Serial No. 239.654.
To all whmn it may concern:
Be it known that I, GrUsEPPE GIANoLI, a subject of the King of Italy, residing at Milan, in the Kingdom of Italy, have invented certain new and useful Improvements in Processes for Dyeing or Charging Silks with Tin Compounds, of which the following is a specification.
It is well known and has even been the cause of complaint that silks charged with salts of tinwhich is the material usually em loyed for this purpose-are subject to suc alteration in their physical and mechanical properties that after a very short space of time they will tear even upon a slight pull. More especially is this the case when such silks are exposed to light. The importance of this loss of resistive power has been demonstrated by the researches made in the laboratory of the Socita Anonima Cooperativa per la stagionatura e lassaggio delle Sete ed affini in connection with silk (see Ammo/ire of the S ocitd Chimica of Milan, sitting of the December 4, 1897) and by the researches of Professor Gnehm and Dr. Banziger. (See Fc'irber Zeitung of 1897.) As it was the intention to study the causes of these alterations produced insilk charged with the abovementioned compounds, various forms of tin combinations were tested, and it is found that by using sulfo-cyanic acid and its salts and derivatives the silk fiber retains its dynamometric qualities almost unchanged.
The application of the sulfo-cyanic acid and of its salts is effected during the operations of charging, dyeing, or clearing by means of a diluted solution, (varying from 0,5 to three per cent. and more.) Having exposed to the action of light for ten days some small skeins of silk (organzin) charged with thirty per cent. in excess of its original weight, a portion of which had been subjected after dyeing to clearing by the aid of one per cent. of sulfo-cyanate of ammonia rendered acid by means of sulfuric acid, whilethe other portion had been cleared or brightened by the ordinary method in an acid bath by means of 1:1,000 (one per thousand) of sulfuric acid, the following results were obtained:
Tenacity. Elasticity.
G'rams. Millimeters. Skein charged without the addition 43,32 57 of sulfo-cyanate. Skein charged with the addition of 63,88 135 sulfo-cyanate.
It will be understood that either the sulfocyanic acid, its salts, or its derivatives may be used.
Having now particularly described and as certained the nature of the said invention and in what manner the same is to be performed, I declare that what I claim is In the process of mordanting or dyeing silk, acting on the silk with an alkaline sulfocyanid and an acid in solution of approximately one to three per cent, substantially as described.
In witness whereof I have hereunto set my hand in presence of two witnesses.
GIUSEPPE GIANOLI.
Witnesses GOFFREDO R1001, MIOHELEO DIAGO.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US23965405A US819751A (en) | 1905-01-04 | 1905-01-04 | Process of charging silk. |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US23965405A US819751A (en) | 1905-01-04 | 1905-01-04 | Process of charging silk. |
Publications (1)
Publication Number | Publication Date |
---|---|
US819751A true US819751A (en) | 1906-05-08 |
Family
ID=2888233
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US23965405A Expired - Lifetime US819751A (en) | 1905-01-04 | 1905-01-04 | Process of charging silk. |
Country Status (1)
Country | Link |
---|---|
US (1) | US819751A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20060191035A1 (en) * | 1997-06-12 | 2006-08-24 | North Carolina State University | Methods and compositions for protein production in tobacco plants with reduced nicotine |
-
1905
- 1905-01-04 US US23965405A patent/US819751A/en not_active Expired - Lifetime
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20060191035A1 (en) * | 1997-06-12 | 2006-08-24 | North Carolina State University | Methods and compositions for protein production in tobacco plants with reduced nicotine |
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