US20120160329A1 - Method and apparatus for monitoring fluids - Google Patents
Method and apparatus for monitoring fluids Download PDFInfo
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- US20120160329A1 US20120160329A1 US13/379,087 US201013379087A US2012160329A1 US 20120160329 A1 US20120160329 A1 US 20120160329A1 US 201013379087 A US201013379087 A US 201013379087A US 2012160329 A1 US2012160329 A1 US 2012160329A1
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Images
Classifications
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- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B21/00—Methods or apparatus for flushing boreholes, e.g. by use of exhaust air from motor
- E21B21/08—Controlling or monitoring pressure or flow of drilling fluid, e.g. automatic filling of boreholes, automatic control of bottom pressure
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B43/00—Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
- E21B43/01—Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells specially adapted for obtaining from underwater installations
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B47/00—Survey of boreholes or wells
- E21B47/001—Survey of boreholes or wells for underwater installation
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B47/00—Survey of boreholes or wells
- E21B47/10—Locating fluid leaks, intrusions or movements
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
- Y10T137/0318—Processes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
- Y10T137/7722—Line condition change responsive valves
- Y10T137/7837—Direct response valves [i.e., check valve type]
Definitions
- the present invention relates to a method and apparatus for use in the hydrocarbon exploration and production industry and in particular to a method and apparatus for monitoring a fluid that is to be transported through a fluid conduit.
- the monitoring of a fluid to be transported through a fluid conduit provides a dynamic indication of the occurrence of detrimental effects for the fluid flow within the conduit.
- the described method and apparatus have particular application for preventing blockages within fluid umbilicals, although the methods and apparatus may also be adapted for monitoring fluids for the occurrence of detrimental effects within pipelines, wellbores and risers.
- a fluid umbilical is a bundled collection of steel and/or thermoplastic tubing and electrical cabling. Typically they are employed to transmit chemicals, hydraulic fluids, electric power, and two-way data communication and control signals between surface production facilities and subsea production equipment. Umbilicals typically range up to 10 inches (254 mm) in diameter, with internal tubes ranging from 0.5 inch to 1 inch (12.7 mm to 25.4 mm) in diameter.
- a dynamic umbilical is the portion of the umbilical that is suspended from a semi-submersible vessel to the seabed, where it is coupled to a static section of the umbilical. In a typical umbilical, the multiple internal conduits are twisted together into a helical rope-like structure in order to increase the tensile strength. This is a particularly important consideration for the dynamic umbilical section since it must withstand stresses due to its own weight and the dynamic loading from currents.
- Examples of some of the most frequently transmitted chemicals through umbilicals within the hydrocarbon exploration and production industry include: scale inhibitors; corrosion inhibitors; methanol, ethanol, ethylene glycol, mono ethylene glycol, MEG (examples of hydrate inhibitors); industrial methylated spirits; wax inhibitors and pour point depressants (PPD); low dosage hydrate inhibitors (LDHIs); asphaltene inhibitors and dispersants; flow improvers and surfactants; biocides; H 2 S scavengers; and demulsifiers.
- the relatively small diameters of the internal tubes within the subsea umbilical in combination with the fact that their helical path arrangement significantly increases the frictional drag experienced by objects inserted into the internal tubes, means that umbilicals are particularly prone to blockages. Such blockages completely prevent fluid transmission through the umbilical and so can cause considerable disruption to production activities.
- the helical path arrangement of the internal conduits means that conventional cleaning equipment is often prohibited from being inserted to attempt to clear a blockage. If a blockage cannot be removed then this results in obvious time and cost implications for the operator. It is estimated that the costs incurred in replacing a typical subsea fluid umbilical run into several millions of pounds.
- a further detrimental effect that occurs within fluid conduits is the onset of corrosion.
- the effects of corrosion can be exacerbated by the chemical nature of the fluid supply being transported through the conduit. Corrosion can ultimately lead to structural failures within a fluid conduit and therefore it is obviously beneficial to be able to monitor the detrimental effects of corrosion within a fluid conduit.
- a yet further object of an aspect of the present invention to provide a method and apparatus for monitoring the level of corrosion within a fluid conduit system.
- the described method and apparatus is applicable to a wide range of fluid conduit systems used in the hydrocarbon exploration and production industry, and in particular to fluid umbilicals.
- a method for monitoring a fluid supply to be transported through a fluid conduit located within a hydrocarbon exploration and production installation comprising the steps of:
- the step of monitoring the fluid supply within the monitoring zone comprises the step of detecting solids or solidification within the fluid supply.
- the method further comprises the step of shutting off the fluid supply to the fluid conduit when solidification is detected.
- Shutting off the fluid supply to the fluid conduit allows an operator to check the installation to see if a non-compatible chemical supply has been introduced to the fluid supply.
- the step of detecting solids or solidification within the fluid supply comprises monitoring a pressure differential across a filter located within the monitoring zone.
- a change in the pressure differential across the filter is indicative of a change in the viscosity within the fluid supply and hence a possible contamination of the fluid supply.
- the step of shutting off the fluid supply to the fluid conduit occurs when the pressure differential across the filter is outside of a predetermined tolerance value for the fluid supply.
- the step of monitoring the pressure differential across the filter further comprises the step of correlating the monitored pressure differential with a temperature of the fluid supply.
- the step of detecting solids or solidification within the fluid supply comprises the step of monitoring the water content of the fluid supply.
- the step of shutting off the fluid supply to the fluid conduit occurs when the water content of the fluid supply is outside a predetermined tolerance value for the fluid supply.
- the step of detecting solids or solidification within the fluid supply comprises the step of monitoring a particulate or debris content of the fluid supply.
- the step of shutting off the fluid supply to the fluid conduit occurs when a density or mass of the particulate or debris content within the fluid supply is outside a predetermined tolerance value for the fluid supply.
- an alarm may be activated to notify an operator of the shut down event.
- an automated electronic notification may also be sent to an appropriate preselected person notifying them of the shut down event.
- the step of monitoring the fluid supply within the monitoring zone further comprises the step of analysing the quality or purity of the chemical composition of the fluid supply.
- the step of monitoring the fluid supply within the monitoring zone further comprises the step of monitoring the rate of flow of the fluid supply.
- the method further comprises the step of notifying an operator of the risk of a blockage occurring within the fluid conduit when the quality or purity of the chemical composition of the fluid supply is outside a predetermined tolerance value.
- the method further comprises the step of recording information relating to one or more of the monitored parameters. Recording information regarding fluid cleanliness, viscosity, water content, differential pressure, absolute pressure, temperature and fluid flow rates allows for historical data reviews to be generated.
- a method for monitoring a fluid supply to be transported through a fluid umbilical comprising the steps of:
- Embodiments of the second aspect of the invention may comprise preferred and optional features of the first aspect of the invention and vice versa.
- a fluid monitoring unit for monitoring a fluid supply to a fluid conduit, the fluid monitoring unit comprising a monitoring zone and a sensor, the sensor providing a means for detecting the occurrence of one or more events within the monitoring zone detrimental to the flow of the fluid supply through the fluid conduit, wherein the monitoring zone is configured to provide upstream fluid cooperation with an entrance of the fluid conduit.
- the fluid monitoring unit By having the monitoring zone configured to provide upstream fluid cooperation with an entrance to the fluid conduit allows the fluid monitoring unit to dynamically monitor the fluid supply prior to entering the fluid conduit. This allows for the early detection of potential blockage forming scenarios and so significantly reduces the risk of costly blockages occurring within the fluid conduit.
- the senor comprises a filter located within the monitoring zone and a pressure detector arranged to monitor the pressure differential of the fluid supply across the filter.
- the senor further comprises a thermometer arranged to provide a means for the fluid monitoring unit to correlate changes in the monitored pressure differential across the filter with temperature changes of the fluid supply.
- the senor comprises a hygrometer arranged to monitor the water content of the fluid supply.
- the senor comprises a particulate sensor arranged to monitor the fluid supply transmitted through the monitoring zone for the presence of particulate or debris.
- the particulate sensor may comprise an optical particulate sensor.
- the particulate sensor may comprise a passive-induction particulate sensor.
- the senor comprises a UV spectrometer arranged to monitor the chemical composition of the fluid supply transmitted through the monitoring zone.
- the senor comprises a flow meter arranged to monitor the rate of flow of the fluid supply.
- the fluid monitoring unit comprises a computer processing unit that provides a means for controlling the sensor.
- the computer processing unit also provides a means for the fluid monitoring unit to transmit and receive data.
- the computer processing unit Preferably the computer processing unit generates an output signal if the pressure differential of the fluid supply across the filter is outside of a predetermined tolerance value.
- the computer processing unit may also generate an output signal if the water content within the fluid supply is outside of a predetermined tolerance value.
- the computer processing unit may also generate an output signal if a density or mass of the particulate or debris content within the fluid supply is outside a predetermined tolerance value.
- the computer processing unit may also generate an output signal if the quality or purity of the chemical composition of the fluid supply is outside a predetermined tolerance value.
- a fluid monitoring unit for monitoring a fluid supply to a fluid umbilical
- the fluid monitoring unit comprising a monitoring zone and a sensor, the sensor providing a means for detecting the occurrence of one or more events within the monitoring zone detrimental to the flow of the fluid supply through the fluid umbilical, wherein the monitoring zone is configured to provide upstream fluid cooperation with an entrance of the fluid umbilical.
- Embodiments of the fourth aspect of the invention may comprise preferred and optional features of the third aspect of the invention and vice versa.
- a hydrocarbon exploration and production installation comprising at least one supply conduit that provides a means for fluid communication between a fluid source and a fluid conduit, and a fluid monitoring unit in accordance with the third aspect of the present invention, wherein the fluid monitoring unit is located within the supply conduit upstream of the fluid conduit.
- the installation further comprises a pump located between the fluid source and the fluid monitoring unit.
- the installation further comprises a shut off valve located between the fluid monitoring unit and the fluid conduit.
- an output signal from the fluid monitoring unit is employed as a feedback signal to activate a shut down of the pump.
- the output signal may also be employed as a feedback signal to activate closure of the shut off valve.
- the installation further comprises an operations control module connected to the fluid monitoring unit so as to provide a means for monitoring and recording output data from the fluid monitoring unit.
- a hydrocarbon exploration and production installation comprising at least one supply conduit that provides a means for fluid communication between a fluid source and a fluid umbilical, and a fluid monitoring unit in accordance with the fourth aspect of the present invention, wherein the fluid monitoring unit is located within the supply conduit upstream of the fluid umbilical.
- Embodiments of the sixth aspect of the invention may comprise preferred and optional features of the third fourth and fifth aspects of the invention and vice versa.
- FIG. 1 presents a schematic diagram of a surface production facility, that provides fluid communication with an umbilical, and which incorporates fluid monitoring units in accordance with an embodiment of the present invention
- FIG. 2 presents a schematic diagram of the fluid monitoring units of FIG. 1 .
- FIG. 1 a schematic diagram of a surface production facility, generally depicted by the reference numeral 1 , is presented in FIG. 1
- FIG. 2 presents a schematic diagram of a fluid monitoring unit 2 employed with the surface production facility 1 .
- the surface production facility 1 can be seen to comprise four supply conduits 3 that provide a means for fluid communication between a corresponding fluid source 4 and an umbilical 5 via a topside umbilical termination unit (TUTU) 6 .
- the fluid sources comprise a corrosion inhibitor 4 a (one such suitable corrosion inhibitor being that sold by Champion Technologies under the trade mark Scortron® G10000), a scale inhibitor 4 b (one such suitable scale inhibitor being that sold by Champion Technologies under the trade mark Gyptron® SA110N), methanol 4 c and a wax inhibitor 4 d (one such suitable wax inhibitor being that sold by Champion Technologies under the trade mark Flexoil® WM1840).
- each supply conduit 3 is located a metering pump 7 , a fluid monitoring unit 2 and a shut-off valve 8 .
- Each metering pump 7 is employed to regulate the pressure flow of the fluid within its respective supply conduit 3 and hence into an internal tube of the umbilical 5 .
- the fluid monitoring units 2 are located between the metering pumps 7 and the TUTU 6 and are employed to monitor one or more parameters associated with the transported fluid before it is pumped into the umbilical 5 .
- a feedback connection 9 provides a means for the fluid monitoring unit 2 to stop its respective metering pump 7 and/or to close the respective shut-off valve 8 when the occurrence of a detrimental effect for the fluid flow within the umbilical 5 is detected e.g. a potential blockage forming scenario is detected or significant levels of corrosion are detected, further details of which are provided below.
- An electricity supply 10 provides a dedicated power source for each of the fluid monitoring units 2 .
- Each fluid monitoring unit 2 is also connected to an operations control module 11 which may be located within the surface production facility 1 .
- the operations control module 11 is connected to a remote operations control module 12 that provides a means for remotely monitoring and controlling the fluid supplies into the umbilical 5 .
- Communication to and from the facility and within the facility itself may be by RS232, Ethernet or wireless means.
- each fluid monitoring unit 2 can be seen to comprise a monitoring zone in the form of a conduit 13 through which the fluid supply is transmitted such that the monitoring zone provides a means for upstream fluid cooperation with an entrance of an internal tubing of the umbilical 5 .
- a filter 14 Located within the monitoring zone 13 is a filter 14 which provides an initial means for preventing particulates and other debris from entering the internal tubing of the umbilical 5 .
- the fluid monitoring unit 2 further comprises a pressure sensor 15 that provides a means for measuring the pressure differential of the fluid supply across the filter 14 or the absolute pressure of the fluid supply within the monitoring zone 13 (an Able Instrumentation Differential Pressure Gauge Model 126 being one such suitable pressure sensor), a thermometer 16 that provides a means for measuring the temperature of the fluid supply (an Able Instruments eight wire, one series temperature switch being one such suitable thermometer), and a hygrometer 17 that provides a means for measuring the water content within the fluid supply (an Able Instruments HTF dewpoint sensor being one such suitable hygrometer).
- a pressure sensor 15 that provides a means for measuring the pressure differential of the fluid supply across the filter 14 or the absolute pressure of the fluid supply within the monitoring zone 13
- an Able Instrumentation Differential Pressure Gauge Model 126 being one such suitable pressure sensor
- a thermometer 16 that provides a means for measuring the temperature of the fluid supply
- an Able Instruments eight wire, one series temperature switch being one such suitable thermometer
- the fluid monitoring unit 2 further comprises a particulate or flocculation sensor 18 (an Able Instruments Model 980 series dual beam Photometer being one such suitable particulate sensor); a UV spectrometer 19 (an Able Instruments Model 960 UV-Analyzer being one such suitable UV spectrometer); and a flow meter 20 that provides a means for accurately monitoring the rate of flow of the fluid before it enters the internal tubing of the umbilical 5 .
- the flow meter may be a positive displacement flow meter, for example a helical screw flow meter or a rotary piston flow meter since both meter types provide accurate readings at relatively low flow rates.
- Each of the sensors 15 , 16 , 17 , 18 , 19 and 20 are connected to a CPU 21 which provides a means for controlling the sensors 15 , 16 , 17 , 18 , 19 and 20 , processing the measured data and relaying the data on to the control modules 11 and/or 12 .
- the filter 14 comprises a two micron absolute filter, however the filter size may be changed depending on expected flow rates within the system.
- the fluid supply flow rates range from a minimum flow rate of 40 ml/min to a maximum flow rate of 1000 ml/min.
- Corresponding pressures through the system range from 0 to 5000 psi.
- the distance between the fluid monitoring unit 2 and the shut-off valve 8 is preferable for the distance between the fluid monitoring unit 2 and the shut-off valve 8 to be sufficient that on the fluid monitoring unit 2 detecting the occurrence of a detrimental effect for the fluid flow within the umbilical the shut-off valve 8 can be closed before the fluid supply passes its physical location.
- the above described fluid monitoring units 2 allow for various ways to detect the occurrence of solidification within supplied fluids and for analysing the quality of supplied fluids.
- the onset of solidification within the fluid supply can be indicative of coagulation or flocculation caused by chemical reactions between different fluids or the use of low quality or purity fluids, and/or the formation of solid particulates or debris as a result of corrosion within the umbilical itself.
- the first method employs the pressure sensor 15 to monitor a pressure differential across the filter 14 .
- the pressure differential is correlated with the temperature of the fluid, as measured by the thermometer 16 . This correlation may take place directly within the pressure sensor 15 , the CPU 21 or more preferably within the control modules 11 or 12 .
- a change in the viscosity within the fluid supply is detected as a corresponding change in the pressure differential across the filter 14 . If the change in pressure differential is outside of a predetermined tolerance value for that particular fluid, and does not correlate with a corresponding temperature change, as detected by the thermometer 16 , then this is indicative of a chemical reaction causing coagulation or flocculation, for example the inadvertent mixing of a scale inhibitor and methanol.
- Coagulation or flocculation can lead to the onset of a blockage within the umbilical 5 and so in such circumstances the fluid monitoring unit 2 would activate an alarm within the control module 11 and/or 12 and preferably provide for the automatic shut down of the metering pump 7 in conjunction with the closing of the corresponding shut-off valve 8 . This would allow the operator to check the facility 1 to see if a non-compatible chemical combination had been set up in error sufficiently early in the process so as to avoid the occurrence of a costly blockage.
- the second method for detecting potential on set of a blockage is achieved via the employment of the hygrometer 17 .
- the hygrometer 17 is set to detect the presence of water within the fluid supply between 0% and 100% using a small electrical current.
- a predetermined value, with acceptable tolerance levels, is provided for a particular fluid supply. Activation of the alarms and/or the shutting down of the fluid supply, as previously described, again results if the detected water level moves out with the predetermined tolerance levels.
- the water content for a water-based fluid supply e.g. a biocide may be of the order of 80% with an accepted tolerance level of ⁇ 0.5%.
- the water content may fall to around 78% thus triggering the alarms and/or the shutting down of the supply line.
- the water content for a solvent-based fluid supply e.g. an ashphaltene inhibitor may be of the order of 0% with an accepted tolerance level of +0.5%. If a water based fluid, for example an H 2 S scavenger or even simply rain water were to be introduced to the solvent-based fluid supply then the water content may rise to above 0.5% thus triggering the alarms and/or the shutting down of the supply line.
- What is important for the operation of the above solidification diagnostic is the establishment of a base water level content for a fluid supply and an appropriate tolerance level.
- the hygrometer 17 then allows for changes in the water content of the fluid supply to be monitored and appropriate action taken if this exceeds the predetermined tolerance value.
- the fluid monitoring unit 2 it is preferable for the fluid monitoring unit 2 to also be capable of measuring and recording the absolute pressure, temperature and rate of fluid flow of the fluid supply.
- the pressure sensor 15 , the thermometer 16 and the flow meter 20 in conjunction with the control modules 11 and/or 12 can facilitate all of these diagnostics.
- the employment of the particulate sensor 18 provides a means for detecting the presence of particulates or debris with the fluid supply.
- the particulates or debris may be of a type that is transmitted directly into the monitoring zone 13 or are formed as a result of a chemical reaction within the monitoring zone 13 e.g. via corrosion.
- the particulate sensor 18 preferably comprises an optical sensor whereby one or more light sources and a photodetector are arranged to provide sensing points within the monitoring zone 13 e.g. an Able Instruments Model 980 series dual beam Photometer. Particulates or debris passing through sensing points then acts to scatter the light from the light source onto the photodetector which is thereafter transformed into a pulsed signal. The number of pulses per unit time is proportional to the density of particulates or debris presents. The pulse signal is then converted into a voltage output for relaying to the control modules 11 and/or 12 .
- an optical sensor whereby one or more light sources and a photodetector are arranged to provide sensing points within the monitoring zone 13 e.g. an Able Instruments Model 980 series dual beam Photometer. Particulates or debris passing through sensing points then acts to scatter the light from the light source onto the photodetector which is thereafter transformed into a pulsed signal. The number of pulses per unit time is proportional to the density of particulates or debris
- the particulate sensor 18 may comprise a type that employs a combination of passive-induction and protected-probe technologies (a Baumer Process Instrumentation conductivity sensor ISL05x being one such suitable sensor). As particles or debris flow near and around the probe, minute currents are dynamically induced within the probe. These currents can then be processed to provide an absolute output that is substantially linear to the mass of the particulates or debris present.
- a Baumer Process Instrumentation conductivity sensor ISL05x being one such suitable sensor.
- Optical particulate sensors are preferable for use with oil based fluids or solvents e.g. wax inhibitor while they are less effective when used with water based fluids e.g. biocides. In such fluids it is preferable to employ the passive induction type of sensors.
- a predetermined particulate or debris level is defined for a particular fluid supply. If the mass of the particulate or debris exceeds this predetermined value then the fluid monitoring unit 2 activates the corresponding alarms and/or shuts down the fluid supply.
- control modules 11 or 12 may also be configured to automatically e-mail an appropriate preselected person about the potential problem within the facility 1 .
- This facility has particular application in the following circumstances.
- the employment of the UV spectrometer 19 provides a means for analysing the chemical composition of a fluid within the monitoring zone 13 and thus provide an indication if it falls below a predefined quality or purity level. In such circumstances the fluid monitoring unit 2 notifies the control modules 11 and/or 12 that the fluid should not be allowed to remain static within the umbilical 5 .
- shut down event of the surface production facility 1 occurs during this period then subsequent periodic reminders may be sent to the operator of the surface production facility 1 notifying them that unless pumping of the fluid is re started then they are heading for the occurrence of a blockage within the umbilical 5 .
- the above described method and apparatus provide a means for protecting the integrity of a fluid conduit and in particular a fluid umbilical.
- the method and apparatus allow for a reduction in the vulnerability of these expensive assets due to human error by providing a means for continuous dynamic monitoring of the injected fluid supplies and providing for automated pump shut down when potential detrimental effects for the fluid flow within the fluid umbilical are detected e.g. blockage forming circumstances.
- the fluid monitoring units provide a proactive method that prevents the formation of blockages rather than allowing for a reactive method to be employed in response to the detection of a blockage, as is the case for known prior art systems.
- the adapted facility also allows for periodic integrity reviews to be carried out wherein information regarding fluid cleanliness (NAS rating), viscosity, water content, differential pressure, absolute pressure, temperature and flow rates can be displayed in real time or downloaded for historical data reviews.
- NAS rating fluid cleanliness
- viscosity viscosity
- water content differential pressure
- absolute pressure absolute pressure
- temperature flow rates
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Abstract
Description
- The present invention relates to a method and apparatus for use in the hydrocarbon exploration and production industry and in particular to a method and apparatus for monitoring a fluid that is to be transported through a fluid conduit. The monitoring of a fluid to be transported through a fluid conduit provides a dynamic indication of the occurrence of detrimental effects for the fluid flow within the conduit. The described method and apparatus have particular application for preventing blockages within fluid umbilicals, although the methods and apparatus may also be adapted for monitoring fluids for the occurrence of detrimental effects within pipelines, wellbores and risers.
- During the production and transportation of hydrocarbons, it is common for the interiors of fluid conduits, including pipelines, wellbores, risers and umbilicals, to become fouled. This fouling can lead to the build up of layers of debris or particulate matter on the inside of conduits, which reduces the effective inner diameter (ID) of the conduit and thus reduces the flow rate. Fouling can also produce blockages in the fluid conduits which completely prevent fluid flow.
- A fluid umbilical is a bundled collection of steel and/or thermoplastic tubing and electrical cabling. Typically they are employed to transmit chemicals, hydraulic fluids, electric power, and two-way data communication and control signals between surface production facilities and subsea production equipment. Umbilicals typically range up to 10 inches (254 mm) in diameter, with internal tubes ranging from 0.5 inch to 1 inch (12.7 mm to 25.4 mm) in diameter. A dynamic umbilical is the portion of the umbilical that is suspended from a semi-submersible vessel to the seabed, where it is coupled to a static section of the umbilical. In a typical umbilical, the multiple internal conduits are twisted together into a helical rope-like structure in order to increase the tensile strength. This is a particularly important consideration for the dynamic umbilical section since it must withstand stresses due to its own weight and the dynamic loading from currents.
- Examples of some of the most frequently transmitted chemicals through umbilicals within the hydrocarbon exploration and production industry include: scale inhibitors; corrosion inhibitors; methanol, ethanol, ethylene glycol, mono ethylene glycol, MEG (examples of hydrate inhibitors); industrial methylated spirits; wax inhibitors and pour point depressants (PPD); low dosage hydrate inhibitors (LDHIs); asphaltene inhibitors and dispersants; flow improvers and surfactants; biocides; H2S scavengers; and demulsifiers.
- The relatively small diameters of the internal tubes within the subsea umbilical, in combination with the fact that their helical path arrangement significantly increases the frictional drag experienced by objects inserted into the internal tubes, means that umbilicals are particularly prone to blockages. Such blockages completely prevent fluid transmission through the umbilical and so can cause considerable disruption to production activities. Furthermore, the helical path arrangement of the internal conduits means that conventional cleaning equipment is often prohibited from being inserted to attempt to clear a blockage. If a blockage cannot be removed then this results in obvious time and cost implications for the operator. It is estimated that the costs incurred in replacing a typical subsea fluid umbilical run into several millions of pounds.
- In order to mitigate the risk of blockages forming within umbilicals it is known in the art to provide the internal tubes with a filter at its entrance. Such filters do help prevent certain particulates and other debris from entering the internal tubing. However, in practice it is found that the major contributing factor to the formation of blockages within a fluid umbilical is human error, either through the poor design of the chemical bunkering systems, unsuitable methodologies being employed in offshore environments or even faulty chemical compatibility testing being carried out. For example, if an operator accidentally allows incompatible fluids to be transmitted down the same internal tube then coagulation or flocculation may take place so resulting in blockages within the umbilical. Some examples of known incompatible fluid combinations include:
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- 1) Scale inhibitors and methanol or glycols. If the scale inhibitor is water based (as is normally the case) then methanol or a glycol will precipitate the inhibitor;
- 2) Pour point depressants and methanol or glycols. When the level of methanol or glycol is above a certain level then precipitation of some polymer PPDs occurs;
- 3) Asphaltene inhibitors and methanol;
- 4) Asphaltene dispersants and polar solvents (e.g. alcohols, glycols or water);
- 5) Flow improvers for water and polar solvents;
- 6) Flow improvers for oil and any of the other above listed transmitted chemicals;
- 7) H2S scavengers and methanol or organic solvents; and
- 8) Biocides and methanol.
- A further detrimental effect that occurs within fluid conduits is the onset of corrosion. The effects of corrosion can be exacerbated by the chemical nature of the fluid supply being transported through the conduit. Corrosion can ultimately lead to structural failures within a fluid conduit and therefore it is obviously beneficial to be able to monitor the detrimental effects of corrosion within a fluid conduit.
- It is therefore an object of an aspect of the present invention to provide a method and apparatus for monitoring a fluid that is to be transported through a fluid conduit so as to provide a dynamic indication of the occurrence of detrimental effects for the fluid flow within the conduit.
- It is a further object of an aspect of the present invention to provide a method and apparatus for monitoring the formation of a blockage within a fluid conduit system.
- A yet further object of an aspect of the present invention to provide a method and apparatus for monitoring the level of corrosion within a fluid conduit system.
- The described method and apparatus is applicable to a wide range of fluid conduit systems used in the hydrocarbon exploration and production industry, and in particular to fluid umbilicals.
- According to a first aspect of the present invention there is provided a method for monitoring a fluid supply to be transported through a fluid conduit located within a hydrocarbon exploration and production installation, the method comprising the steps of:
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- providing a monitoring zone upstream of the fluid conduit;
- introducing the fluid supply to the fluid conduit via the monitoring zone; and
- monitoring the fluid supply within the monitoring zone so as to detect the occurrence of one or more events detrimental to the flow of the fluid supply through the fluid conduit.
- It is advantageous to monitor the fluid supply prior to entering the fluid conduit as this allows for the early detection of an event detrimental to the flow of the fluid supply e.g. a chemical reaction indicative of corrosion of the fluid conduit or the formation of a potential blockage within the fluid conduit. In this way the risk of costly blockages or structural failure occurring within the fluid conduit is significantly reduced.
- Most preferably the step of monitoring the fluid supply within the monitoring zone comprises the step of detecting solids or solidification within the fluid supply.
- Preferably the method further comprises the step of shutting off the fluid supply to the fluid conduit when solidification is detected. Shutting off the fluid supply to the fluid conduit allows an operator to check the installation to see if a non-compatible chemical supply has been introduced to the fluid supply.
- Optionally the step of detecting solids or solidification within the fluid supply comprises monitoring a pressure differential across a filter located within the monitoring zone. A change in the pressure differential across the filter is indicative of a change in the viscosity within the fluid supply and hence a possible contamination of the fluid supply.
- Preferably the step of shutting off the fluid supply to the fluid conduit occurs when the pressure differential across the filter is outside of a predetermined tolerance value for the fluid supply.
- Most preferably the step of monitoring the pressure differential across the filter further comprises the step of correlating the monitored pressure differential with a temperature of the fluid supply. By correlating the pressure differential across the filter with the temperature of the fluid supply reduces the risk of erroneous contamination events being detected.
- Optionally, the step of detecting solids or solidification within the fluid supply comprises the step of monitoring the water content of the fluid supply.
- Preferably the step of shutting off the fluid supply to the fluid conduit occurs when the water content of the fluid supply is outside a predetermined tolerance value for the fluid supply.
- Optionally, the step of detecting solids or solidification within the fluid supply comprises the step of monitoring a particulate or debris content of the fluid supply.
- Preferably the step of shutting off the fluid supply to the fluid conduit occurs when a density or mass of the particulate or debris content within the fluid supply is outside a predetermined tolerance value for the fluid supply.
- If the fluid supply to the fluid conduit is shut down then an alarm may be activated to notify an operator of the shut down event. Optionally an automated electronic notification may also be sent to an appropriate preselected person notifying them of the shut down event.
- Preferably the step of monitoring the fluid supply within the monitoring zone further comprises the step of analysing the quality or purity of the chemical composition of the fluid supply.
- Optionally the step of monitoring the fluid supply within the monitoring zone further comprises the step of monitoring the rate of flow of the fluid supply.
- Preferably the method further comprises the step of notifying an operator of the risk of a blockage occurring within the fluid conduit when the quality or purity of the chemical composition of the fluid supply is outside a predetermined tolerance value.
- Optionally the method further comprises the step of recording information relating to one or more of the monitored parameters. Recording information regarding fluid cleanliness, viscosity, water content, differential pressure, absolute pressure, temperature and fluid flow rates allows for historical data reviews to be generated.
- According to a second aspect of the present invention there is provided a method for monitoring a fluid supply to be transported through a fluid umbilical, the method comprising the steps of:
-
- providing a monitoring zone upstream of the fluid umbilical;
- introducing the fluid supply to the fluid umbilical via the monitoring zone; and
- monitoring the fluid supply within the monitoring zone so as to detect the occurrence of one or more events detrimental to the flow of the fluid supply through the fluid umbilical.
- Embodiments of the second aspect of the invention may comprise preferred and optional features of the first aspect of the invention and vice versa.
- According to a third aspect of the present invention there is provided a fluid monitoring unit for monitoring a fluid supply to a fluid conduit, the fluid monitoring unit comprising a monitoring zone and a sensor, the sensor providing a means for detecting the occurrence of one or more events within the monitoring zone detrimental to the flow of the fluid supply through the fluid conduit, wherein the monitoring zone is configured to provide upstream fluid cooperation with an entrance of the fluid conduit.
- By having the monitoring zone configured to provide upstream fluid cooperation with an entrance to the fluid conduit allows the fluid monitoring unit to dynamically monitor the fluid supply prior to entering the fluid conduit. This allows for the early detection of potential blockage forming scenarios and so significantly reduces the risk of costly blockages occurring within the fluid conduit.
- Most preferably the sensor comprises a filter located within the monitoring zone and a pressure detector arranged to monitor the pressure differential of the fluid supply across the filter.
- Preferably the sensor further comprises a thermometer arranged to provide a means for the fluid monitoring unit to correlate changes in the monitored pressure differential across the filter with temperature changes of the fluid supply.
- Alternatively, or in addition, the sensor comprises a hygrometer arranged to monitor the water content of the fluid supply.
- Alternatively, or in addition, the sensor comprises a particulate sensor arranged to monitor the fluid supply transmitted through the monitoring zone for the presence of particulate or debris.
- The particulate sensor may comprise an optical particulate sensor. The particulate sensor may comprise a passive-induction particulate sensor.
- Alternatively, or in addition, the sensor comprises a UV spectrometer arranged to monitor the chemical composition of the fluid supply transmitted through the monitoring zone.
- Alternatively, or in addition, the sensor comprises a flow meter arranged to monitor the rate of flow of the fluid supply.
- Most preferably the fluid monitoring unit comprises a computer processing unit that provides a means for controlling the sensor. The computer processing unit also provides a means for the fluid monitoring unit to transmit and receive data.
- Preferably the computer processing unit generates an output signal if the pressure differential of the fluid supply across the filter is outside of a predetermined tolerance value.
- The computer processing unit may also generate an output signal if the water content within the fluid supply is outside of a predetermined tolerance value.
- The computer processing unit may also generate an output signal if a density or mass of the particulate or debris content within the fluid supply is outside a predetermined tolerance value.
- The computer processing unit may also generate an output signal if the quality or purity of the chemical composition of the fluid supply is outside a predetermined tolerance value.
- According to a fourth aspect of the present invention there is provided a fluid monitoring unit for monitoring a fluid supply to a fluid umbilical, the fluid monitoring unit comprising a monitoring zone and a sensor, the sensor providing a means for detecting the occurrence of one or more events within the monitoring zone detrimental to the flow of the fluid supply through the fluid umbilical, wherein the monitoring zone is configured to provide upstream fluid cooperation with an entrance of the fluid umbilical.
- Embodiments of the fourth aspect of the invention may comprise preferred and optional features of the third aspect of the invention and vice versa.
- According to a fifth aspect of the present invention there is provided a hydrocarbon exploration and production installation, the installation comprising at least one supply conduit that provides a means for fluid communication between a fluid source and a fluid conduit, and a fluid monitoring unit in accordance with the third aspect of the present invention, wherein the fluid monitoring unit is located within the supply conduit upstream of the fluid conduit.
- Preferably the installation further comprises a pump located between the fluid source and the fluid monitoring unit.
- Optionally the installation further comprises a shut off valve located between the fluid monitoring unit and the fluid conduit.
- Preferably an output signal from the fluid monitoring unit is employed as a feedback signal to activate a shut down of the pump. The output signal may also be employed as a feedback signal to activate closure of the shut off valve.
- Preferably the installation further comprises an operations control module connected to the fluid monitoring unit so as to provide a means for monitoring and recording output data from the fluid monitoring unit.
- According to a sixth aspect of the present invention there is provided a hydrocarbon exploration and production installation, the installation comprising at least one supply conduit that provides a means for fluid communication between a fluid source and a fluid umbilical, and a fluid monitoring unit in accordance with the fourth aspect of the present invention, wherein the fluid monitoring unit is located within the supply conduit upstream of the fluid umbilical.
- Embodiments of the sixth aspect of the invention may comprise preferred and optional features of the third fourth and fifth aspects of the invention and vice versa.
- Aspects and advantages of the present invention will become apparent upon reading the following detailed description of example embodiments and upon reference to the following drawings in which:
-
FIG. 1 presents a schematic diagram of a surface production facility, that provides fluid communication with an umbilical, and which incorporates fluid monitoring units in accordance with an embodiment of the present invention; and -
FIG. 2 presents a schematic diagram of the fluid monitoring units ofFIG. 1 . - In the description which follows, like parts are marked throughout the specification and drawings with the same reference numerals. The drawings are not necessarily to scale and the proportions of certain parts have been exaggerated to better illustrate details and features of embodiments of the invention.
- In order to provide understanding of the various aspects of the present invention a schematic diagram of a surface production facility, generally depicted by the
reference numeral 1, is presented inFIG. 1 , whileFIG. 2 presents a schematic diagram of afluid monitoring unit 2 employed with thesurface production facility 1. - The
surface production facility 1 can be seen to comprise foursupply conduits 3 that provide a means for fluid communication between a correspondingfluid source 4 and an umbilical 5 via a topside umbilical termination unit (TUTU) 6. In the presently described embodiment the fluid sources comprise acorrosion inhibitor 4 a (one such suitable corrosion inhibitor being that sold by Champion Technologies under the trade mark Scortron® G10000), ascale inhibitor 4 b (one such suitable scale inhibitor being that sold by Champion Technologies under the trade mark Gyptron® SA110N),methanol 4 c and awax inhibitor 4 d (one such suitable wax inhibitor being that sold by Champion Technologies under the trade mark Flexoil® WM1840). - Within each
supply conduit 3 is located ametering pump 7, afluid monitoring unit 2 and a shut-offvalve 8. Eachmetering pump 7 is employed to regulate the pressure flow of the fluid within itsrespective supply conduit 3 and hence into an internal tube of the umbilical 5. Thefluid monitoring units 2 are located between the metering pumps 7 and theTUTU 6 and are employed to monitor one or more parameters associated with the transported fluid before it is pumped into the umbilical 5. Afeedback connection 9 provides a means for thefluid monitoring unit 2 to stop itsrespective metering pump 7 and/or to close the respective shut-offvalve 8 when the occurrence of a detrimental effect for the fluid flow within the umbilical 5 is detected e.g. a potential blockage forming scenario is detected or significant levels of corrosion are detected, further details of which are provided below. - An
electricity supply 10 provides a dedicated power source for each of thefluid monitoring units 2. Eachfluid monitoring unit 2 is also connected to anoperations control module 11 which may be located within thesurface production facility 1. Optionally, theoperations control module 11 is connected to a remote operations controlmodule 12 that provides a means for remotely monitoring and controlling the fluid supplies into the umbilical 5. Communication to and from the facility and within the facility itself may be by RS232, Ethernet or wireless means. - From
FIG. 2 eachfluid monitoring unit 2 can be seen to comprise a monitoring zone in the form of a conduit 13 through which the fluid supply is transmitted such that the monitoring zone provides a means for upstream fluid cooperation with an entrance of an internal tubing of the umbilical 5. Located within the monitoring zone 13 is a filter 14 which provides an initial means for preventing particulates and other debris from entering the internal tubing of the umbilical 5. Thefluid monitoring unit 2 further comprises a pressure sensor 15 that provides a means for measuring the pressure differential of the fluid supply across the filter 14 or the absolute pressure of the fluid supply within the monitoring zone 13 (an Able Instrumentation Differential Pressure Gauge Model 126 being one such suitable pressure sensor), athermometer 16 that provides a means for measuring the temperature of the fluid supply (an Able Instruments eight wire, one series temperature switch being one such suitable thermometer), and ahygrometer 17 that provides a means for measuring the water content within the fluid supply (an Able Instruments HTF dewpoint sensor being one such suitable hygrometer). Optionally, thefluid monitoring unit 2 further comprises a particulate or flocculation sensor 18 (an Able Instruments Model 980 series dual beam Photometer being one such suitable particulate sensor); a UV spectrometer 19 (an Able Instruments Model 960 UV-Analyzer being one such suitable UV spectrometer); and aflow meter 20 that provides a means for accurately monitoring the rate of flow of the fluid before it enters the internal tubing of the umbilical 5. The flow meter may be a positive displacement flow meter, for example a helical screw flow meter or a rotary piston flow meter since both meter types provide accurate readings at relatively low flow rates. - Each of the
sensors CPU 21 which provides a means for controlling thesensors control modules 11 and/or 12. - In the presently described embodiment the filter 14 comprises a two micron absolute filter, however the filter size may be changed depending on expected flow rates within the system. For the presently described
surface production facility 1 the fluid supply flow rates range from a minimum flow rate of 40 ml/min to a maximum flow rate of 1000 ml/min. Corresponding pressures through the system range from 0 to 5000 psi. - It is preferable for the distance between the
fluid monitoring unit 2 and the shut-offvalve 8 to be sufficient that on thefluid monitoring unit 2 detecting the occurrence of a detrimental effect for the fluid flow within the umbilical the shut-offvalve 8 can be closed before the fluid supply passes its physical location. - The above described
fluid monitoring units 2 allow for various ways to detect the occurrence of solidification within supplied fluids and for analysing the quality of supplied fluids. The onset of solidification within the fluid supply can be indicative of coagulation or flocculation caused by chemical reactions between different fluids or the use of low quality or purity fluids, and/or the formation of solid particulates or debris as a result of corrosion within the umbilical itself. The various techniques will now be described in further detail. - The first method employs the pressure sensor 15 to monitor a pressure differential across the filter 14. The pressure differential is correlated with the temperature of the fluid, as measured by the
thermometer 16. This correlation may take place directly within the pressure sensor 15, theCPU 21 or more preferably within thecontrol modules thermometer 16, then this is indicative of a chemical reaction causing coagulation or flocculation, for example the inadvertent mixing of a scale inhibitor and methanol. Coagulation or flocculation can lead to the onset of a blockage within the umbilical 5 and so in such circumstances thefluid monitoring unit 2 would activate an alarm within thecontrol module 11 and/or 12 and preferably provide for the automatic shut down of themetering pump 7 in conjunction with the closing of the corresponding shut-offvalve 8. This would allow the operator to check thefacility 1 to see if a non-compatible chemical combination had been set up in error sufficiently early in the process so as to avoid the occurrence of a costly blockage. - The second method for detecting potential on set of a blockage is achieved via the employment of the
hygrometer 17. Thehygrometer 17 is set to detect the presence of water within the fluid supply between 0% and 100% using a small electrical current. A predetermined value, with acceptable tolerance levels, is provided for a particular fluid supply. Activation of the alarms and/or the shutting down of the fluid supply, as previously described, again results if the detected water level moves out with the predetermined tolerance levels. For example, the water content for a water-based fluid supply e.g. a biocide may be of the order of 80% with an accepted tolerance level of ±0.5%. If a solvent, for example a wax inhibitor, were to be introduced to the water-based fluid supply then the water content may fall to around 78% thus triggering the alarms and/or the shutting down of the supply line. Alternatively, the water content for a solvent-based fluid supply e.g. an ashphaltene inhibitor may be of the order of 0% with an accepted tolerance level of +0.5%. If a water based fluid, for example an H2S scavenger or even simply rain water were to be introduced to the solvent-based fluid supply then the water content may rise to above 0.5% thus triggering the alarms and/or the shutting down of the supply line. - What is important for the operation of the above solidification diagnostic is the establishment of a base water level content for a fluid supply and an appropriate tolerance level. The
hygrometer 17 then allows for changes in the water content of the fluid supply to be monitored and appropriate action taken if this exceeds the predetermined tolerance value. - It is preferable for the
fluid monitoring unit 2 to also be capable of measuring and recording the absolute pressure, temperature and rate of fluid flow of the fluid supply. The pressure sensor 15, thethermometer 16 and theflow meter 20 in conjunction with thecontrol modules 11 and/or 12 can facilitate all of these diagnostics. - The employment of the particulate sensor 18 provides a means for detecting the presence of particulates or debris with the fluid supply. The particulates or debris may be of a type that is transmitted directly into the monitoring zone 13 or are formed as a result of a chemical reaction within the monitoring zone 13 e.g. via corrosion.
- The particulate sensor 18 preferably comprises an optical sensor whereby one or more light sources and a photodetector are arranged to provide sensing points within the monitoring zone 13 e.g. an Able Instruments Model 980 series dual beam Photometer. Particulates or debris passing through sensing points then acts to scatter the light from the light source onto the photodetector which is thereafter transformed into a pulsed signal. The number of pulses per unit time is proportional to the density of particulates or debris presents. The pulse signal is then converted into a voltage output for relaying to the
control modules 11 and/or 12. - Alternatively, or in addition to the optical particulate sensor, the particulate sensor 18 may comprise a type that employs a combination of passive-induction and protected-probe technologies (a Baumer Process Instrumentation conductivity sensor ISL05x being one such suitable sensor). As particles or debris flow near and around the probe, minute currents are dynamically induced within the probe. These currents can then be processed to provide an absolute output that is substantially linear to the mass of the particulates or debris present.
- Optical particulate sensors are preferable for use with oil based fluids or solvents e.g. wax inhibitor while they are less effective when used with water based fluids e.g. biocides. In such fluids it is preferable to employ the passive induction type of sensors.
- In a similar manner to that described above a predetermined particulate or debris level is defined for a particular fluid supply. If the mass of the particulate or debris exceeds this predetermined value then the
fluid monitoring unit 2 activates the corresponding alarms and/or shuts down the fluid supply. - As well as the
fluid monitoring units 2 being configured to operate or trigger an alarm and/or shut down the fluid supply upon exceeding one or more predetermined parameters, thecontrol modules facility 1. This facility has particular application in the following circumstances. - During the operation of the
surface production facility 1 there are times when it is required to be shut down. On occasion this shut down period may last several weeks. On restarting thesurface production facility 1 it can be found to have developed a blockage even although no obvious contamination of the fluid has occurred. - It has been recognised by the inventors that the source of the formation of such blockages lie within the inherent quality or purity of the fluid being transported i.e. if the fluid quality or purity is below a predetermined value and then the fluid is allowed to remain static within the umbilical then a blockage may form.
- The employment of the
UV spectrometer 19 provides a means for analysing the chemical composition of a fluid within the monitoring zone 13 and thus provide an indication if it falls below a predefined quality or purity level. In such circumstances thefluid monitoring unit 2 notifies thecontrol modules 11 and/or 12 that the fluid should not be allowed to remain static within the umbilical 5. - If a shut down event of the
surface production facility 1 occurs during this period then subsequent periodic reminders may be sent to the operator of thesurface production facility 1 notifying them that unless pumping of the fluid is re started then they are heading for the occurrence of a blockage within the umbilical 5. - The above described method and apparatus provide a means for protecting the integrity of a fluid conduit and in particular a fluid umbilical. The method and apparatus allow for a reduction in the vulnerability of these expensive assets due to human error by providing a means for continuous dynamic monitoring of the injected fluid supplies and providing for automated pump shut down when potential detrimental effects for the fluid flow within the fluid umbilical are detected e.g. blockage forming circumstances. Significantly, the fluid monitoring units provide a proactive method that prevents the formation of blockages rather than allowing for a reactive method to be employed in response to the detection of a blockage, as is the case for known prior art systems.
- By performing real time particle analysis and monitoring chemical compatibilities, via pressure, temperature, water and particle content measurements, and UV spectroscopy round the clock analysis can be performed. This allows for trends within the facility to be built up for individual umbilicals, or other fluid conduits, and so enables the activation of alarms or automated shut downs, as and when appropriate.
- The adapted facility also allows for periodic integrity reviews to be carried out wherein information regarding fluid cleanliness (NAS rating), viscosity, water content, differential pressure, absolute pressure, temperature and flow rates can be displayed in real time or downloaded for historical data reviews.
- The foregoing description of the invention has been presented for purposes of illustration and description and is not intended to be exhaustive or to limit the invention to the precise form disclosed. The described embodiments were chosen and described in order to best explain the principles of the invention and its practical application to thereby enable others skilled in the art to best utilise the invention in various embodiments and with various modifications as are suited to the particular use contemplated. Therefore, further modifications or improvements may be incorporated without departing from the scope of the invention as defined by the appended claims.
Claims (37)
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- 2010-06-18 WO PCT/GB2010/051014 patent/WO2010150000A2/en active Application Filing
- 2010-06-18 EP EP20100742528 patent/EP2446110A2/en not_active Withdrawn
- 2010-06-18 CN CN2010800282417A patent/CN102459807A/en active Pending
- 2010-06-18 BR BRPI1014842A patent/BRPI1014842A2/en not_active IP Right Cessation
- 2010-06-18 AU AU2010264270A patent/AU2010264270A1/en not_active Abandoned
- 2010-06-18 IN IN700DEN2012 patent/IN2012DN00700A/en unknown
- 2010-06-18 GB GB1010265.5A patent/GB2471549B/en active Active
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Also Published As
Publication number | Publication date |
---|---|
GB201010265D0 (en) | 2010-08-04 |
GB0910978D0 (en) | 2009-08-05 |
GB2471549B (en) | 2012-03-28 |
EP2446110A2 (en) | 2012-05-02 |
BRPI1014842A2 (en) | 2016-05-03 |
WO2010150000A2 (en) | 2010-12-29 |
GB2471549A (en) | 2011-01-05 |
CN102459807A (en) | 2012-05-16 |
AU2010264270A1 (en) | 2012-01-12 |
IN2012DN00700A (en) | 2015-06-19 |
WO2010150000A3 (en) | 2011-08-11 |
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