US20120047945A1 - Bellows Valve for Use in Cryogenics - Google Patents

Bellows Valve for Use in Cryogenics Download PDF

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Publication number
US20120047945A1
US20120047945A1 US13/318,882 US201013318882A US2012047945A1 US 20120047945 A1 US20120047945 A1 US 20120047945A1 US 201013318882 A US201013318882 A US 201013318882A US 2012047945 A1 US2012047945 A1 US 2012047945A1
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US
United States
Prior art keywords
valve
vent
circuit
gas
tube
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
US13/318,882
Inventor
Alain Briglia
Francine Chommy
Emmanuel Garnier
Thierry Gesbert
Natacha Haik-Beraud
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LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
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Application filed by LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Assigned to L'AIR LIQUIDE, SOCIETE ANONYME POUR L'ETUDE ET L'EXPLOITATION DES PROCEDES GEORGES CLAUDE reassignment L'AIR LIQUIDE, SOCIETE ANONYME POUR L'ETUDE ET L'EXPLOITATION DES PROCEDES GEORGES CLAUDE ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: CHOMMY, FRANCINE, HAIK-BERAUD, NATACHA, BRIGLIA, ALAIN, GARNIER, EMMANUEL, GESBERT, THIERRY
Publication of US20120047945A1 publication Critical patent/US20120047945A1/en
Abandoned legal-status Critical Current

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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16KVALVES; TAPS; COCKS; ACTUATING-FLOATS; DEVICES FOR VENTING OR AERATING
    • F16K41/00Spindle sealings
    • F16K41/10Spindle sealings with diaphragm, e.g. shaped as bellows or tube
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T137/00Fluid handling
    • Y10T137/0318Processes

Definitions

  • the present invention relates to bellows safety valves used on cryogenic fluids.
  • a bellows valve comprises a circuit for fluid conveyed through a valve body, a sealing member that can move between a rest position and an active position, taken from an open position and a closed position of said circuit, and a resilient annular bellows system for connection between said sealing member and said body, sealing off said circuit.
  • Bellows valves are safety devices which, by their design, make it possible to accommodate a high back-pressure at exhaust thereof. To do so, it is essential for the body of the valve, called the bonnet, to be in pressure balance with the outside.
  • the balancing function is provided by the vent of the bonnet, and therefore it is essential for this vent not to be obstructed, as indicated in the API 520 standard.
  • the presence of ice 9 ( FIG. 2 ) in the bellows 5 results from the conjunction of two events: the presence of water and a low temperature in the bellows, equal to or below 0° C.
  • the low temperature may be due to various causes:
  • the solution consists in permanently having an atmosphere free of any moisture in the cavity formed by the bonnet of the valve (which cavity is in contact via orifices with the inside of the bellows).
  • a valve of the type comprising a circuit for fluid conveyed through a valve body, a sealing member that can move between a rest position and an active position, taken from an open position and a closed position of said circuit, and a resilient annular bellows system for connection between said sealing member and said body sealing off said circuit, the fluid circuit being open to the outside of the valve through a vent formed in the body, and the vent being provided with means preventing the ingress of wet gas into the body, characterized in that a tube is connected to the vent, this tube being connected to a source of pressurized dry gas.
  • the valve comprises:
  • a gas separation unit operating by distillation at a temperature below 0° C. in an enclosure, the walls of which are scavenged by a dry gas, the unit including a valve as described above, the fluid being a gas intended for or coming from the distillation and the tube being connected to a wall of the enclosure so that the dry scavenging gas penetrates the tube.
  • the unit is optionally provided with bellows rupture detection means.
  • the unit may be a gas separation unit operating by distillation at a temperature below 0° C. that includes a valve as described above, the fluid being a gas intended for or coming from the distillation.
  • FIG. 3 a simple tube 15 is connected to the vent 3 of the bonnet 1 of the valve 2 , to which a permanent scavenging stream of dry gas (instrument air, service nitrogen, etc.) passing through the tubes 11 , 17 is connected.
  • a permanent scavenging stream of dry gas instrument air, service nitrogen, etc.
  • the flow rate of scavenging gas is controlled by a valve 13 .
  • a small device connected to the vent 3 of the bonnet 1 of the valve 2 , minimizes the effect of respiration by a nonreturn valve system 19 .
  • This valve is connected to the vent 3 via the tube 23 .
  • a cartridge of a dessicant 21 is inserted into the tube 21 upstream of the valve 19 .
  • a small device connected to the vent 3 of the bonnet 1 of the valve 2 , via a tube 25 , obstructs the vent in a controlled manner, either by a flexible membrane 24 or by a rupture disk calibrated to a few millibars, the principle being that this closure is broken in the event of a large overpressure due to the bellows 5 rupturing.
  • a simple tube 27 is connected between the vent 3 of the bonnet 1 of the valve 2 and the enclosure 31 of the cold box of a cryogenic separation unit.
  • the bonnet 1 is thus in permanent contact with a dry atmosphere, owing to the permanent scavenging of the enclosure of the cold box with a dry gas, thus preventing any accumulation of water due either to natural respiration or to cryopumping.
  • a filter element 33 will be installed on the end of the dip tube 35 so as to prevent any entry of perlite.
  • a T-piece 35 equipped with a plug 29 may also be installed so as to carry out measurements for detecting any rupture of the bellows 5 .

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  • Engineering & Computer Science (AREA)
  • General Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Safety Valves (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Drying Of Gases (AREA)

Abstract

The invention relates to a valve including a circuit for a fluid conveyed into a valve body, a stopper that is movable between a rest position and an operative position from among an open position and a closed position of said circuit, and a resilient annular bellows system connecting said stopper and said body and sealingly closing said circuit in relation to a chamber, wherein the chamber is open towards the outside of the valve via a vent formed in the body, the vent being provided with means for preventing the ingress of wet gas into the body.

Description

  • The present invention relates to bellows safety valves used on cryogenic fluids.
  • A bellows valve comprises a circuit for fluid conveyed through a valve body, a sealing member that can move between a rest position and an active position, taken from an open position and a closed position of said circuit, and a resilient annular bellows system for connection between said sealing member and said body, sealing off said circuit.
  • Bellows valves are safety devices which, by their design, make it possible to accommodate a high back-pressure at exhaust thereof. To do so, it is essential for the body of the valve, called the bonnet, to be in pressure balance with the outside. The balancing function is provided by the vent of the bonnet, and therefore it is essential for this vent not to be obstructed, as indicated in the API 520 standard.
  • Because of the abovementioned constraints, the use of bellows safety valves in cryogenics is not recommended, or even sometimes prohibited because of the risk of the valve being blocked by the accidental presence of ice 9 in the bellows 5 (FIG. 2), preventing the upward movement of the sealing member or poppet 7 (FIG. 1) of the valve 2. The risk incurred in the event of such an incident may lead to the failure of equipment, causing major damage on a unit, or even fatalities.
  • The presence of ice 9 (FIG. 2) in the bellows 5 results from the conjunction of two events: the presence of water and a low temperature in the bellows, equal to or below 0° C.
  • The presence of water may occur through two effects:
      • condensation of the moisture contained in the ambient air because of natural respiration of the cavity formed by the bonnet 1 of the valve (FIG. 1) via the vent 3 present, owing to day/night temperature variations; and
      • condensation of the moisture contained in the ambient air because of the cryopumping (capture of moisture on a cold surface) that occurs if there is slight leakage on the valve, which cools the latter below the temperature at which the wet air condenses.
  • The low temperature may be due to various causes:
      • ambient temperature;
      • valve (seat/poppet 7) leakage;
      • very short distance between the process and the valve, the latter being cooled by conduction or convection.
  • To overcome the aforementioned problems, it is possible to make use of another valve technology, namely control valves, but the cost of these is substantially higher.
  • The invention described below makes it possible at very low cost to use the technology of bellows valves in cryogenics by overcoming the aforementioned drawbacks.
  • As described above, it is the conjunction of two events that make it dangerous to use bellows valves in cryogenics, namely:
      • the presence of water; and
      • a cold temperature.
  • Since the temperature is a parameter on which they may be little influence, the solution consists in permanently having an atmosphere free of any moisture in the cavity formed by the bonnet of the valve (which cavity is in contact via orifices with the inside of the bellows).
  • According to one subject of the invention, what is provided is a valve of the type comprising a circuit for fluid conveyed through a valve body, a sealing member that can move between a rest position and an active position, taken from an open position and a closed position of said circuit, and a resilient annular bellows system for connection between said sealing member and said body sealing off said circuit, the fluid circuit being open to the outside of the valve through a vent formed in the body, and the vent being provided with means preventing the ingress of wet gas into the body, characterized in that a tube is connected to the vent, this tube being connected to a source of pressurized dry gas.
  • According to other optional aspects, the valve comprises:
      • a tube connected to the vent, this tube being connected to a drying means;
      • a nonreturn valve closing off the tube; and
      • a tube connected to the vent and provided with a membrane or with a rupture disk.
  • According to another aspect of the invention, what is provided is the use of a valve as described above at a temperature below 0° C., or even below −50° C.
  • According to another aspect of the invention, what is provided is a gas separation unit operating by distillation at a temperature below 0° C. in an enclosure, the walls of which are scavenged by a dry gas, the unit including a valve as described above, the fluid being a gas intended for or coming from the distillation and the tube being connected to a wall of the enclosure so that the dry scavenging gas penetrates the tube.
  • The unit is optionally provided with bellows rupture detection means.
  • The unit may be a gas separation unit operating by distillation at a temperature below 0° C. that includes a valve as described above, the fluid being a gas intended for or coming from the distillation.
  • The invention will be described in greater detail with reference to the figures that illustrate the four families of solutions according to the invention:
      • 1. scavenging by a dry gas, illustrated in FIG. 3;
      • 2. dessicator, illustrated in FIG. 4;
      • 3. closure of the vent by a membrane, in FIGS. 5; and
      • 4. collecting of the vent, in FIG. 6.
  • For all the figures, the basic structure of the bellows valve, illustrated in FIG. 1, is maintained. In FIG. 3, a simple tube 15 is connected to the vent 3 of the bonnet 1 of the valve 2, to which a permanent scavenging stream of dry gas (instrument air, service nitrogen, etc.) passing through the tubes 11, 17 is connected. This thus creates a barrier to the ambient air that could enter the cavity formed by the bonnet of the valve. The flow rate of scavenging gas is controlled by a valve 13.
  • In FIG. 4, a small device, connected to the vent 3 of the bonnet 1 of the valve 2, minimizes the effect of respiration by a nonreturn valve system 19. This valve is connected to the vent 3 via the tube 23. In addition, given that the system may not be perfectly sealed, a cartridge of a dessicant 21 is inserted into the tube 21 upstream of the valve 19.
  • In FIG. 5, a small device, connected to the vent 3 of the bonnet 1 of the valve 2, via a tube 25, obstructs the vent in a controlled manner, either by a flexible membrane 24 or by a rupture disk calibrated to a few millibars, the principle being that this closure is broken in the event of a large overpressure due to the bellows 5 rupturing.
  • In FIG. 6, a simple tube 27 is connected between the vent 3 of the bonnet 1 of the valve 2 and the enclosure 31 of the cold box of a cryogenic separation unit. The bonnet 1 is thus in permanent contact with a dry atmosphere, owing to the permanent scavenging of the enclosure of the cold box with a dry gas, thus preventing any accumulation of water due either to natural respiration or to cryopumping.
  • A filter element 33 will be installed on the end of the dip tube 35 so as to prevent any entry of perlite.
  • A T-piece 35 equipped with a plug 29 may also be installed so as to carry out measurements for detecting any rupture of the bellows 5.

Claims (8)

1-6. (canceled)
7. A valve of the type comprising a circuit for fluid conveyed through a valve body, a sealing member that can move between a rest position and an active position, taken from an open position and a closed position of said circuit, and a resilient annular bellows system for connection between said sealing member and said body sealing off said circuit, the chamber being open to the outside of the valve through a vent formed in the body, and the vent is provided with means preventing the ingress of wet gas into the body, wherein said valve includes a tube connected to the vent, this tube being connected to a source of pressurized dry gas.
8. A flow control method comprising:
a) conveying a fluid through a circuit through a valve body,
b) moving a sealing member that can move between a rest position and an active position, resulting in the movement from an open position and a closed position of said circuit,
c) connecting between said sealing member and said body sealing off said circuit a resilient annular bellows system,
d) allowing the chamber to open to the outside of the valve through a vent formed in the body, and the vent being provided with means preventing the ingress of wet gas into the body, wherein said valve includes a tube connected to the vent, and
e) connecting this tube to a source of pressurized dry gas.
9. The flow control method of claim 8, wherein said fluid is at a temperature below 0° C.
10. The flow control method of claim 8, wherein said fluid is at temperature below −50° C.
11. A gas separation unit operating by distillation at a temperature below 0° C. that includes the valve in claim 8, the fluid being a gas intended for or coming from the distillation
12. A gas separation unit operating by distillation at a temperature below 0° C. in an enclosure, the walls of which are scavenged by a dry gas, the unit comprising the valve in claim 7, the fluid being a gas intended for or coming from the distillation and the tube being connected to a wall of the enclosure so that the dry scavenging gas penetrates the tube.
13. The unit in claim 12, provided with bellows rupture detection means.
US13/318,882 2009-05-05 2010-04-29 Bellows Valve for Use in Cryogenics Abandoned US20120047945A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0952977 2009-05-05
FR0952977A FR2945333B1 (en) 2009-05-05 2009-05-05 VALVE WITH BELLOW SUITABLE FOR USE IN CRYOGENIC
PCT/FR2010/050816 WO2010130912A1 (en) 2009-05-05 2010-04-29 Bellows valve for use in cryogenics

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US20120047945A1 true US20120047945A1 (en) 2012-03-01

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US13/318,882 Abandoned US20120047945A1 (en) 2009-05-05 2010-04-29 Bellows Valve for Use in Cryogenics

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US (1) US20120047945A1 (en)
EP (1) EP2427680B1 (en)
CN (1) CN102414495A (en)
FR (1) FR2945333B1 (en)
WO (1) WO2010130912A1 (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014105788A (en) * 2012-11-28 2014-06-09 Fukui Seisakusho:Kk Safety valve
CN104662052A (en) * 2012-09-24 2015-05-27 埃克森美孚化学专利公司 Functionalized resins obtained via olefin metathesis
US20180074581A1 (en) * 2015-03-23 2018-03-15 Haim Melman Eye Tracking System
US10268213B1 (en) 2017-10-20 2019-04-23 The United States Of America As Represented By The Administrator Of Nasa Check valve with pilot tube pressure sensing
US20210341078A1 (en) * 2020-04-30 2021-11-04 Emerson Automation Solutions Final Control US LP Systems and Methods for Determining Failure in a Back Pressure Balanced Relief Valve
US12000505B2 (en) * 2021-04-30 2024-06-04 Emerson Automation Solutions Final Control US LP Systems and methods for determining failure in a back pressure balanced relief valve

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US4131129A (en) * 1977-04-06 1978-12-26 Firestone Raymond A Device for controlling gas flow into vessels
US4884410A (en) * 1988-08-22 1989-12-05 Helix Technology Corporation Purge/charge manifold and method for cryogenic systems
US5363879A (en) * 1994-02-15 1994-11-15 Liquid Carbonic Corporation Cryogenic coupling
US5417072A (en) * 1993-11-08 1995-05-23 Trw Inc. Controlling the temperature in a cryogenic vessel
US5597009A (en) * 1994-03-17 1997-01-28 Societe Europeenne De Propulsion Vacuum-enclosed integral cryogenic valve
US5644855A (en) * 1995-04-06 1997-07-08 Air Products And Chemicals, Inc. Cryogenically purged mini environment
US6182715B1 (en) * 2000-01-18 2001-02-06 Alex R. Ziegler Liquid nitrogen injection system with flexible dosing arm for pressurization and inerting containers on production lines
US20040016240A1 (en) * 2002-04-02 2004-01-29 Brook Thomas Currie Method for transferring cryogenic liquids and associated cryogenic fill nozzle insulating boot
US6978799B2 (en) * 2003-10-22 2005-12-27 S.P.M. Flow Control, Inc. Emergency pressure relief valve with enhanced reset
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US20100251887A1 (en) * 2009-04-07 2010-10-07 Innosepra Llc Carbon Dioxide Recovery
US20110056571A1 (en) * 2009-09-08 2011-03-10 Questar Gas Company Methods and systems for reducing pressure of natural gas and methods and systems of delivering natural gas
US8011380B2 (en) * 2009-10-01 2011-09-06 Vision Tech International Llp Single component two-stage regulator
US8051812B2 (en) * 2007-04-16 2011-11-08 Scuderi Group, Llc Variable valve actuator with a pneumatic booster

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US4131129A (en) * 1977-04-06 1978-12-26 Firestone Raymond A Device for controlling gas flow into vessels
US4884410A (en) * 1988-08-22 1989-12-05 Helix Technology Corporation Purge/charge manifold and method for cryogenic systems
US5417072A (en) * 1993-11-08 1995-05-23 Trw Inc. Controlling the temperature in a cryogenic vessel
US5363879A (en) * 1994-02-15 1994-11-15 Liquid Carbonic Corporation Cryogenic coupling
US5597009A (en) * 1994-03-17 1997-01-28 Societe Europeenne De Propulsion Vacuum-enclosed integral cryogenic valve
US5644855A (en) * 1995-04-06 1997-07-08 Air Products And Chemicals, Inc. Cryogenically purged mini environment
US6182715B1 (en) * 2000-01-18 2001-02-06 Alex R. Ziegler Liquid nitrogen injection system with flexible dosing arm for pressurization and inerting containers on production lines
US20040016240A1 (en) * 2002-04-02 2004-01-29 Brook Thomas Currie Method for transferring cryogenic liquids and associated cryogenic fill nozzle insulating boot
US7281550B2 (en) * 2003-07-14 2007-10-16 Cryotech International, Inc. Liquid delivery system with horizontally displaced dispensing point
US6978799B2 (en) * 2003-10-22 2005-12-27 S.P.M. Flow Control, Inc. Emergency pressure relief valve with enhanced reset
US20060086101A1 (en) * 2004-05-07 2006-04-27 Kabushiki Kaisha Kobe Seiko Sho. Cryogenic system
US20060010886A1 (en) * 2004-07-14 2006-01-19 Clamage Eric D Liquid cryogen dosing system with nozzle for pressurizing and inerting containers
US8051812B2 (en) * 2007-04-16 2011-11-08 Scuderi Group, Llc Variable valve actuator with a pneumatic booster
US20100064891A1 (en) * 2008-09-17 2010-03-18 Airgard, Inc. Reactive gas control
US20100251887A1 (en) * 2009-04-07 2010-10-07 Innosepra Llc Carbon Dioxide Recovery
US20110056571A1 (en) * 2009-09-08 2011-03-10 Questar Gas Company Methods and systems for reducing pressure of natural gas and methods and systems of delivering natural gas
US8011380B2 (en) * 2009-10-01 2011-09-06 Vision Tech International Llp Single component two-stage regulator

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104662052A (en) * 2012-09-24 2015-05-27 埃克森美孚化学专利公司 Functionalized resins obtained via olefin metathesis
JP2014105788A (en) * 2012-11-28 2014-06-09 Fukui Seisakusho:Kk Safety valve
US20180074581A1 (en) * 2015-03-23 2018-03-15 Haim Melman Eye Tracking System
US10268213B1 (en) 2017-10-20 2019-04-23 The United States Of America As Represented By The Administrator Of Nasa Check valve with pilot tube pressure sensing
US20210341078A1 (en) * 2020-04-30 2021-11-04 Emerson Automation Solutions Final Control US LP Systems and Methods for Determining Failure in a Back Pressure Balanced Relief Valve
US12000505B2 (en) * 2021-04-30 2024-06-04 Emerson Automation Solutions Final Control US LP Systems and methods for determining failure in a back pressure balanced relief valve

Also Published As

Publication number Publication date
CN102414495A (en) 2012-04-11
EP2427680A1 (en) 2012-03-14
FR2945333B1 (en) 2015-08-07
WO2010130912A1 (en) 2010-11-18
FR2945333A1 (en) 2010-11-12
EP2427680B1 (en) 2013-08-21

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