US20090321887A1 - Method of fabricating an electromechanical structure including at least one mechanical reinforcing pillar - Google Patents
Method of fabricating an electromechanical structure including at least one mechanical reinforcing pillar Download PDFInfo
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- US20090321887A1 US20090321887A1 US12/488,841 US48884109A US2009321887A1 US 20090321887 A1 US20090321887 A1 US 20090321887A1 US 48884109 A US48884109 A US 48884109A US 2009321887 A1 US2009321887 A1 US 2009321887A1
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Images
Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L29/00—Semiconductor devices specially adapted for rectifying, amplifying, oscillating or switching and having potential barriers; Capacitors or resistors having potential barriers, e.g. a PN-junction depletion layer or carrier concentration layer; Details of semiconductor bodies or of electrodes thereof ; Multistep manufacturing processes therefor
- H01L29/66—Types of semiconductor device ; Multistep manufacturing processes therefor
- H01L29/66007—Multistep manufacturing processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B81—MICROSTRUCTURAL TECHNOLOGY
- B81C—PROCESSES OR APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OR TREATMENT OF MICROSTRUCTURAL DEVICES OR SYSTEMS
- B81C1/00—Manufacture or treatment of devices or systems in or on a substrate
- B81C1/00349—Creating layers of material on a substrate
- B81C1/00357—Creating layers of material on a substrate involving bonding one or several substrates on a non-temporary support, e.g. another substrate
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B81—MICROSTRUCTURAL TECHNOLOGY
- B81C—PROCESSES OR APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OR TREATMENT OF MICROSTRUCTURAL DEVICES OR SYSTEMS
- B81C1/00—Manufacture or treatment of devices or systems in or on a substrate
- B81C1/00642—Manufacture or treatment of devices or systems in or on a substrate for improving the physical properties of a device
- B81C1/0065—Mechanical properties
- B81C1/00682—Treatments for improving mechanical properties, not provided for in B81C1/00658 - B81C1/0065
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B81—MICROSTRUCTURAL TECHNOLOGY
- B81B—MICROSTRUCTURAL DEVICES OR SYSTEMS, e.g. MICROMECHANICAL DEVICES
- B81B2201/00—Specific applications of microelectromechanical systems
- B81B2201/02—Sensors
- B81B2201/0264—Pressure sensors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B81—MICROSTRUCTURAL TECHNOLOGY
- B81C—PROCESSES OR APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OR TREATMENT OF MICROSTRUCTURAL DEVICES OR SYSTEMS
- B81C2201/00—Manufacture or treatment of microstructural devices or systems
- B81C2201/01—Manufacture or treatment of microstructural devices or systems in or on a substrate
- B81C2201/0174—Manufacture or treatment of microstructural devices or systems in or on a substrate for making multi-layered devices, film deposition or growing
- B81C2201/019—Bonding or gluing multiple substrate layers
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L2924/00—Indexing scheme for arrangements or methods for connecting or disconnecting semiconductor or solid-state bodies as covered by H01L24/00
- H01L2924/0001—Technical content checked by a classifier
- H01L2924/0002—Not covered by any one of groups H01L24/00, H01L24/00 and H01L2224/00
Definitions
- the present invention relates to a method of fabricating an electromechanical structure presenting a substrate of the monocrystalline layer type (being made in particular of silicon, germanium, perovskite, or quartz) on a sacrificial layer, in particular for a microsystem or a micro-electromechanical system (MEMS) or a nano-electromechanical system (NEMS), said substrate presenting at least one mechanical reinforcing region (or “pillar”).
- MEMS micro-electromechanical system
- NEMS nano-electromechanical system
- So-called surface technologies enable the size of electromechanical structures (MEMS and/or NEMS) made on silicon to be reduced.
- MEMS and/or NEMS electromechanical structures
- These technologies rely on using a stack of at least three layers: a mechanical layer (typically 0.1 micrometer ( ⁇ m) to 100 ⁇ m thick); a sacrificial layer (typically 0.1 ⁇ m to a few Am thick); and a support (typically 10 ⁇ m to 1000 ⁇ m thick).
- a mechanical layer typically 0.1 micrometer ( ⁇ m) to 100 ⁇ m thick
- a sacrificial layer typically 0.1 ⁇ m to a few Am thick
- a support typically 10 ⁇ m to 1000 ⁇ m thick.
- the non-etched zones of the sacrificial layer enable so-called “anchor” zones or mechanical reinforcement zones (or “pillars”) to be made that serve to connect the mechanical structure to the support.
- a silicon substrate is assembled by molecular bonding to the top of the oxide layer, which oxide layer then acts as the sacrificial layer during final fabrication of the MEMS.
- trenches are formed through the silicon substrate that has been assembled by molecular bonding and the sacrificial layer is removed.
- the pillars serve to support the microsystem.
- the interface zone between the added substrate and the remainder of the structure is subjected to chemical etching (in general with HF acid), thereby leading to shapes that are poorly controlled if the interface is not perfect, since the speed of etching is variable, and there is a risk of revealing the bonding interface.
- chemical etching in general with HF acid
- the pillars are made of thick poly-Si and their lateral size is limited by the technology.
- the pillars are made in the sacrificial layer by filling from a deposit of poly-Si. Filling takes place via the flanks of the cavity so the thickness of the filling is greater than half the width of the pillars.
- the lateral size of the pillar is typically limited to 5 ⁇ m.
- the thickness to be deposited is than about 3 times to 5 times the thickness of the sacrificial layer so as to enable the layer to be planarized.
- FIGS. 27 and 28 show pillars that pass both through the sacrificial layer and through the mechanical layer. In that configuration also, the cavities are filled via the flanks thereby limiting the lateral size of a pillar. Filling with poly-Si may be preceded by depositing a fine nitride layer to insulate the outside of the pillar.
- pillars of width that is limited to the thickness of the poly-Si layer used for filling them.
- the thicknesses used are typically of the order of a few ⁇ m, thereby limiting the lateral dimensions of pillars to a few ⁇ m.
- a known method consists in making a second layer of the second material on the other face of the first substrate with the same thickness as the first layer in order to compensate for the deformations induced by the differences between the said material and silicon, and make it easier to put the two substrates into contact during bonding.
- the first substrate containing as its thick layer at least the sacrificial layer of SiO 2 .
- the material used for filling is thick poly-Si. Since the stress state of polycrystalline Si (at the time of deposition or during heating) is different from that of SiO 2 , limiting the lateral dimensions of the pillars serves to limit non-uniformities in the sacrificial layer.
- the present invention proposes a fabrication method that enables mechanical reinforcing pillars to be fabricated in versatile manner, i.e. without limitation on their width, so their width can be a function of the intended application, and the pillars can be selected to be insulating or conductive at will, in particular in order to enable a contact to be made, while avoiding the drawback of any risk of revealing the bonding interface of a substrate on the sacrificial layer.
- a variant of the method makes it possible to limit the topology that stems from fabricating pillars.
- the invention thus provides a method of fabricating an electromechanical structure presenting a first substrate including at least one layer of monocrystalline material covered in a sacrificial layer that presents a free surface, the structure presenting at least one mechanical reinforcing pillar received in said sacrificial layer, wherein the method comprises:
- b′ depositing a filler layer of a second material different from the first material for terminating the filling of the well region(s), said filler layer covering the first functionalization layer at least in part around the well region(s), and planarizing the filler layer, the pillar(s) being formed by the superposition of at least the first material and the second material in the well region(s);
- the monocrystalline material may be selected in particular from Si, Ge, quartz, or indeed perovskite.
- the substrate may be a thick Si substrate or it may be a substrate of the SOI type in particular, or indeed a substrate having a stop layer (SiGe, porous Si).
- the etching the sacrificial layer to form at least one well may be performed through at least one opening in a mask deposited on the sacrificial layer.
- the planarization of the second layer may be continued until the first functionalization layer is reached, in particular to ensure that the second layer does not remain in the well regions.
- the method may optionally include:
- the second substrate is advantageously of the same kind as the monocrystalline layer of the first substrate.
- the second substrate presents an assembly surface that is covered in a bonding layer, e.g. of silicon oxide.
- the invention may implement depositing a bonding layer on the first and/or second substrate with an interface being formed between these two substrates.
- a bonding layer in the second material may be made on the first substrate prior to bonding.
- the first material may for example be silicon nitride or polycrystalline Si.
- the second material may be silicon oxide, or optionally doped polycrystalline Si, a metal, or a polymer.
- the method may subsequently present a step d) of etching the sacrificial layer through at least one through opening in the first substrate in order to release the electromechanical structure.
- the first substrate is advantageously thinned prior to performing step d) by one or more filling techniques (chemical-mechanical planarization (CMP), rectification, dry etching, wet etching, . . . ).
- the method may include a step b′′) of making at least one well in the first functionalization layer when said layer is an insulating layer and optionally in the filler layer, which well extends at least as far as the sacrificial layer, and depositing a conductive material at least in said well(s) to form at least one electrode.
- steps b′) and b′′) may be advantageous between steps b′) and b′′) to deposit an additional layer of the first material in such a manner as to thicken the insulating first layer, in particular when the planarization of the second layer is continued until the first layer is reached.
- step b′′ provision may be made to deposit a layer including at least one conductive region, e.g. a plane region forming a ground plane.
- the first layer may be made of a conductive material, in particular doped polycrystalline Si, a metal, or a metal and semiconductor alloy.
- the method may include the first functionalization layer and a second functionalization layer, one of the functionalization layers being conducive and the other insulating, and between steps b) and b′), it may include a step b 0 ) of depositing the second functionalization layer, with the functionalization layer that is conductive forming a first interconnection level.
- the second functionalization layer may be made of a third material selected from: silicon nitride; doped or insulating polysilicon Si; and a metal.
- the first functionalization layer may cover a portion only of the well region(s), the other portion of the well regions being covered by the second functionalization layer, thereby enabling the conductive pillars and insulating pillars to be formed.
- the sacrificial layer may be covered by both the first and second functionalization layers together.
- the second functionalization layer may cover the entire surface of the sacrificial layer and of the third functionalization layer.
- the second material of the filler layer may be selected to be identical to the material of the sacrificial layer.
- the method may include, after step b 0 ), a step b′ 1 ) of depositing an insulating layer that forms a third functionalization layer.
- Planarizing the filler layer may then be continued until the third functionalization layer is reached.
- the method may include a step b′ 2 ) of making at least one via in said third functionalization layer and of depositing a conductor at least in said via, said deposit forming a contact on the conductive second functionalization layer so as to form a second interconnection level.
- the method may include successively depositing additional functionalization layers alternatively of conductive material and of insulating material and making vias so as to form additional interconnection levels from the conductive layers.
- the last of said interconnection levels may cover the entire surface so as to form a ground plane.
- the last interconnection level is plane and includes interconnection areas to make it possible, during assembly with the second substrate, to connect elements of the second substrate to the electromechanical structure.
- the invention also provides an electromechanical structure presenting a first substrate presenting at least one monocrystalline layer, a sacrificial layer, and at least one mechanical reinforcing (supporting) pillar received in the sacrificial layer, the structure being suitable for being fabricated by a method as defined above, and wherein at least one mechanical support region is a well region received at least in the entire thickness of the sacrificial layer, at least one said well region being covered in a first layer of a first mechanical support material and being filled with a second layer of a second mechanical support material, the pillar(s) being formed by superposing at least the first and second materials in the well region(s).
- FIGS. 1 a to 1 f show a method of the invention that serves in preferred manner to make two-material reinforcements or pillars, FIG. 1 d ′ showing an advantageous variant of the method;
- FIGS. 2 a to 2 d show a variant of the method of the invention in which there are so-called conductive or insulating pillars, and FIGS. 2 c 1 , 2 c 2 , and 2 d ′ show an implementation having a second level of interconnection;
- FIGS. 3 a to 3 d show a variant of the method of the invention enabling interconnection levels to be made using planar technology, with FIGS. 3 c 1 to 3 c 8 constituting an implementation with a plurality of interconnect levels; and
- FIG. 4 shows, by way of example, a pressure sensor made with the method of FIGS. 1 a to 1 f.
- FIGS. 1 a to 1 f show a preferred implementation of the method of the invention, serving to enable insulating pillars to be made from wide trenches (e.g. several tens of ⁇ m and more precisely 50 ⁇ m for example).
- the method starts with a substrate 1 presenting at least one monocrystalline layer 1 ′ (e.g. of monocrystalline Si), coated in a sacrificial layer 2 (e.g. SiO 2 ).
- the layer 1 ′ may occupy all of the substrate (thick Si substrate) or only a portion thereof (e.g. the top layer of an SOI substrate or some other type of substrate presenting an etching stop layer).
- the initial substrate is a silicon substrate including a monocrystalline SiGe stop layer (not shown in the figure) and a monocrystalline silicon layer 1 ′.
- the layer 2 may be an oxide deposited by low pressure chemical vapor deposition (LPCVD) or by plasma-enhanced CVD (PECVD), or it may be made by thermally oxidizing the layer 1 ′. Its thickness may lie in the range 200 nanometers (nm) to 5 ⁇ m (typically in the range 2 ⁇ m to 3 ⁇ m).
- a layer 3 of photosensitive resin is exposed to enable one or more zones such as 5 1 to be made in the layer 2 ( FIG. 1 a ), these zones providing recesses for making the reinforcing region(s).
- the reinforcing regions may be open zones or they may be closed zones, e.g. annular or polygonal, as applies to a pressure sensor.
- a functionalization layer 4 is deposited on the layer 2 , e.g. a silicon nitride layer having thickness lying for example in the range 10 nm to 500 nm, thereby providing a layer 4 1 on the side walls of the zone(s) 5 1 , and a layer 4 2 on the bare face of the substrate 1 ( FIG. 1 b ) (note: 4 1 and 4 2 can be seen in FIGS. 1 b and 1 e ).
- the nitride may be deposited by chemical vapor deposition, in particular LPCVD or PECVD or by using atomic layer CVD (ALCVD).
- the layer 4 may also be made of optionally doped polysilicon, or of a metal, or of a metal and semiconductor alloy. It needs to present etching selectivity relative to the sacrificial layer. This layer does not necessarily cover the entire surface of the sacrificial layer (it may be etched locally). It enables insulating or conductive pillars to be made depending on the nature of the material constituting the functionalization layer 4 , acting as etching stops for the sacrificial layer and as electrical contacts leading to the mechanical layer 1 ′ when the pillars are conductive.
- the region 4 2 of the layer 4 may be anchored in the layer 1 ′ by using the technique described in French patent application FR 2 859 201. That involves continuing etching the zone 5 1 in the Si so as to be able subsequently to anchor the pillar in a shallow depth (e.g. 100 nm to 500 nm) by means of the region 4 2 , but without the pillar going through said layer 1 ′.
- the etched zones in the sacrificial layer makes it possible to provide functional structures in the mechanical layer that are locally independent of the support.
- the non-etched zones of the sacrificial layer make it possible to make so-called anchor zones or mechanical reinforcement zones (or “pillars”).
- the layer 4 is referred to as the “functionalization” layer since it enables functions to be added to the sacrificial layer: pillars made with etching stops, electrodes under the sacrificial layer, electrical connections between the mechanical layer and said electrodes, or between portions of the mechanical layer that are not interconnected.
- LPCVD LPCVD
- PECVD PECVD
- the filler layer is made of the same material as the sacrificial layer, as in the example shown, then the layer 2 must cover the entire surface.
- the filler layer 6 or 6 ′ is planarized to terminate the mechanical reinforcement zone(s) or pillars 9 constituted by the regions 4 1 , 4 2 , 6 1 ( FIGS. 1 d and 1 d ′).
- the method used for this purpose is chemical mechanical planarization (CMP), for example. This planarization may be carried out so as to remove only a fraction of the thickness of the layer 6 ( FIG. 1 d ′), or as shown in FIG. 1 d, it may be continued and come to an end at the layer 4 of silicon nitride, allowing a substantially plane face to appear at the pillar ( 4 1 , 4 2 , 6 1 ).
- CMP chemical mechanical planarization
- a thin bonding layer 7 is deposited, e.g. an oxide layer (optionally followed by CMP), thereby making it possible subsequently to add on a substrate 8 of monocrystalline Si by molecular bonding (molecular bonding between Si and SiO 2 ), optionally oxidized at its surface that comes into contact with the layer 7 (molecular bonding SiO 2 and SiO 2 ) ( FIG. 1 e ).
- This deposit is optional when only a portion of the thickness of the layer 6 is removed ( FIG. 1 d ′). It may also be omitted from the configuration of FIG. 1 d, but that leads to bonding via a heterogeneous interface, thereby giving rise, other things being equal, to bonding energies that are smaller.
- SiO 2 is its ability to be deposited as a thick layer with little mechanical stress relative to the other materials such as silicon nitride or polysilicon, and also because of its suitability for being planarized with the thoroughly-mastered CMP technique. Furthermore, when the sacrificial layer is also made of SiO 2 , that makes it possible to limit non-uniformities of the sacrificial layer after functionalization; the layer is made for the great majority out of a single material.
- the filler layer is thus preferably made out of the same material as the sacrificial layer.
- a silicon substrate 1 of thickness suitable for making an MEMS e.g. 5 ⁇ m to 50 ⁇ m thick
- Such thinning may be performed by rectification followed by CMP.
- the silicon portion of the initial substrate is rectified to a thickness of about 10 ⁇ m.
- the thickness is determined by the accuracy that is available for this rectification step and also in such a manner that the layer 1 ′ does not include any work-hardened zones, which zones are created during the rectification step. It is thus a function in particular of the desired speed of rectification.
- the thickness of the remaining Si of the initial substrate is subsequently removed by chemical etching, stopping at the SiGe stop layer.
- etching Si and stopping on SiGe Various methods are known for etching Si and stopping on SiGe. Mention can be made of wet etching methods (mixtures of the tetramethylammonium hydroxide (TMAH) or of the KOH type, cf. bibliography on selecting etching) or dry etching (Japanese Journal of Applied Physics, Vol. 43, No. 6B, 2004, pp. 3964-3966, 2004 The Japan Society of Applied Physics).
- TMAH tetramethylammonium hydroxide
- KOH tetramethylammonium hydroxide
- dry etching Japanese Society of Applied Physics
- Depositing the layer 7 is optional, it being possible for the substrate 8 to be added by the technique described in patent application WO 2006/035031. That technique enables molecular bonding to be established between the substrate 8 and the surface made up of two different materials, in particular silicon nitride and SiO 2 .
- the process according to the invention further comprises a step of releasing the electromechanical structure by removing at least partially the sacrificial layer 2 .
- the removal of the sacrificial layer can be done by etching openings 10 , but also by any other means.
- the Si layer 1 ′ is etched to make one or more openings 10 ( FIG. 1 f ). These openings 10 may also serve to define the MEMS structure in the layer 1 ′ and they are used to remove the sacrificial layer 2 by forming one or more cavities 2 1 with the help of hydrofluoric acid in the liquid phase or the vapor phase, when etching a layer of SiO 2 , such that the active structure of FIG. 1 is held by the pillar(s) ( 4 1 , 4 2 , 6 1 ).
- the pillar materials are selected so as to be selective relative to the solution used for etching the sacrificial layer.
- the mechanical structure is thus made in the layer 1 ′ which can be referred to as a mechanical layer.
- the interface zone 8 ′ between the substrate 8 fitted by molecular bonding and the layer 7 is protected from any chemical etching when making the opening(s) 10 and when releasing the MEMS structure by using HF acid to remove the sacrificial layer 2 .
- FIGS. 2 a to 2 d ′ show a variant embodiment in which the pillars include a conductive layer, here made of polycrystalline Si, thus enabling contacts to be made, and indeed multiple interconnection levels by combining conductive pillars and insulating pillars.
- a conductive layer here made of polycrystalline Si
- FIG. 2 a shows wells 35 being made in the sacrificial layer 2 , e.g. made of SiO 2 , on a substrate 1 comprising in particular a layer 1 ′, e.g. made of monocrystalline Si.
- FIG. 2 b shows localized deposition (deposition over the entire surface and then localized etching) of an insulating first functionalization layer 31 made of silicon nitride, in particular on well zones where the insulating pillars are to be made.
- This nitride layer serves to provide insulating pillars and to isolate the polycrystalline Si layer (see description below) chemically from the mechanical layer 1 and the sacrificial layer 2 of the filler layer when made of the same material as the sacrificial layer.
- FIG. 2 c shows the localized deposition (in particular by deposition of the entire surface followed by localized etching) of a conductive second functionalization layer 30 , e.g. of doped polycrystalline Si in well regions 351 where it is desired to make pillars that also perform a conductive function, in particular for making contact with the layer 1 (mechanical layer). Outside well regions, this layer may also serve to make a first interconnection level or electrodes.
- the other wells 35 2 may have no deposit of polycrystalline Si in order to limit capacitive coupling at the insulating pillars. This does not apply if, for reasons of topology, an electrical connection needs to be passed through an insulating pillar as shown in the wells 35 1 .
- the insulating functionalization layer 31 may be deposited after the conductive functionalization layer 30 .
- etching the functionalization layer in the wells needs to be performed in two stages: the functionalization layer is etched in the wells 35 1 , and then after the layer 30 has been made, the functionalization layer is etched in the wells 35 2 .
- FIG. 2 d shows deposition of a filler layer 32 , e.g. of SiO 2 , for filling the wells 35 .
- This deposition is subsequently planarized by using a thinning technique, e.g. the CMP method.
- the pillars thus have either an external conductive layer 31 made of polycrystalline Si, or else an insulating layer 30 at a layer 32 , e.g. of SiO 2 , constituting the core thereof.
- the pillars are therefore made of two materials or of three materials.
- FIGS. 2 c 1 , 2 c 2 , and 2 d ′ show an embodiment including a second level of interconnection layer, here made by polycrystalline Si.
- This second level of interconnection layer enables tracks to be made that electrically interconnect two conductive zones 30 made of polycrystalline Si (conductive pillars or electrodes) that are not interconnected by the first level, for topological reasons.
- FIG. 2 c 1 shows an insulating layer 34 (nitride or oxide) being deposited for the purpose of insulating the interconnection layers. This layer is etched locally with etching stopping at the layer 30 , thereby enabling electrical accesses (aa) to be provided on the zones 30 for connection.
- insulating layer 34 nitride or oxide
- FIG. 2 c 2 shows a second localized conducive layer being made that serves to interconnect the electrical accesses (aa) in application of the interconnection scheme. Vias are thus provided between the first and second interconnection levels.
- a last layer can be made as a layer that covers the entire component, optionally being connected to one or more tracks of the lower layers, and acting as a ground plane for the MEMS system.
- the ground plane may also be made at the same level as the last track, in which case it covers part of the surface only.
- FIG. 2 d ′ shows a filler and bonding layer 40 , e.g. made of silicon oxide, being deposited on the structure obtained in FIG. 2 c 2 .
- FIGS. 3 a to 3 d show another variant of the method enabling the topology due to the various deposited layers to be limited: each localized deposition increases the topology of the final stack initially created by making zones such as 5 1 in the sacrificial layer.
- FIG. 3 a shows the substrate after layers of nitride 31 and of polycrystalline Si 30 have been deposited in succession using a method such as that described with reference to FIGS. 2 a to 2 c.
- the SiN layer 31 is made over the entire substrate apart from the zones of the polycrystalline Si pillars (layer 30 ).
- the polycrystalline Si layer is made over the entire surface of the layer 2 , removing only the zones that serve to insulate those zones that need to be insulated.
- FIG. 3 b shows an additional layer 35 made of SiN being deposited that serves as a reference for rectifying the filler layer.
- FIG. 3 c shows deposition of the filler layer 36 made of SiO 2 after chemical mechanical planarizing (CMP) stopping at the SiN layer 35 .
- CMP chemical mechanical planarizing
- FIG. 3 d shows deposition and planarizing of a second bonding layer 37 , e.g. made of SiO 2 , serving to achieve bonding.
- a second bonding layer 37 e.g. made of SiO 2
- FIG. 3 c 1 an additional oxide layer is made ( FIG. 3 c 1 ) for use as insulation.
- This layer is locally etched to make openings ( FIG. 3 c 2 ) corresponding to electrical connections between interconnection tracks.
- a polycrystalline Si layer is deposited on the entire plate, followed by CMP, stopping at the oxide, thereby leaving polycrystalline Si 39 ′ only in the openings 39 ( FIG. 3 c 3 ).
- FIG. 3 c 4 shows nitride and oxide layers 50 and 51 being deposited in succession. Openings 52 are made by successively etching the oxide 51 (stop on nitride) and then the nitride 50 (stop on oxide) that corresponds to the interconnection tracks ( FIG. 3 c 5 ). The tracks 53 are made ( FIG. 3 d 6 ) by depositing doped polycrystalline Si with CMP and stopping on the oxide constituting the layer 51 .
- an oxide layer 54 is made with Openings 55 being created therein (stop at the polycrystalline Si of the tracks 53 ) for the electrical connections ( FIG. 3 c 7 ). These openings are filled with doped polycrystalline Si 56 by full wafer deposition, followed by CMP stopping at the oxide of the layer 54 . The steps described in FIGS. 3 c 4 to 3 c 6 are repeated.
- the bonding layer of FIG. 3 d is not added since it is the combined oxide and Cu layer that acts as the bonding layer.
- This bonding serves to provide electrical connections between the MEMS substrate and the associated CMOS circuit substrate. Only a fraction of the metal areas needs to serve as electrical connections between the MEMS and the CMOS circuit, with the remainder being made to increase the effective bonding area. Under such circumstances, the electrical connection with the MEMS and CMOS circuit assembly take place via contacts made at the surface of the MEMS.
- the plane of contact areas may be replaced by a continuous metal plane connected to a limited number of MEMS connection tracks and enabling electrical contacts to be established between the support and the MEMS ground.
- FIG. 4 shows a pressure sensor made in accordance with the method of FIGS. 1 a to 1 f .
- An opening 10 is made through the substrate 1 within the perimeter of a pillar 9 ( 4 1 , 4 1 , 6 1 ) of annular shape, and this opening is used for removing the sacrificial layer 2 within this perimeter so as to form a cavity 21 .
- the opening 10 is then recovered in conventional manner, e.g. with polycrystalline silicon phosphosilicate glass (PSG).
- PSG polycrystalline silicon phosphosilicate glass
- the region 22 of the substrate 1 that is situated in the perimeter of the pillar 9 forms the diaphragm of the pressure sensor and it is mechanically supported by the pillar.
- openings 10 for making MEMS of more complicated structure e.g. including one or more fixed-end beams.
- the examples given essentially illustrate making a substrate in which the monocrystalline layer is made of silicon associated with a sacrificial layer made of SiO 2
- the invention enables substrate variants to be made, in particular a substrate with a layer of monocrystalline germanium associated with a sacrificial layer of SiO 2 , or indeed a substrate with a layer of monocrystalline perovskite associated with a sacrificial layer of polycrystalline Si or of SiO 2 .
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Abstract
The invention relates to a method of fabricating an electromechanical structure presenting a first substrate (1) including at least one layer (1′) of monocrystalline material covered in a sacrificial layer (2) that presents a free surface, the structure presenting at least one mechanical reinforcing pillar received in said sacrificial layer, the method being characterized in that it comprises:
-
- a) making at least one well region (51, 52) in the sacrificial layer (2) by etching, at least in the entire thickness of the sacrificial layer (2), the well region defining at least one said mechanical pillar;
- b) depositing a first functionalization layer (4, 31) of a first material, relative to which the sacrificial layer is suitable for being etched selectively, the functionalization layer (4) filling at least one well region (5 1) at least partially and covering the free surface of the sacrificial layer (2) at least around the well region(s); and
- b′) depositing a filler layer (6, 32) of a second material different from the first material for terminating the filling of the well region(s) (5′), said filler layer (6) covering the first functionalization layer (4) at least in part around the well region(s) (5′), and planarizing the filler layer (6, 32), the pillar(s) being formed by the superposition of at least the first material and the second material in the well region(s);
- and releasing the electromechanical structure by removing at least partially the sacrificial layer (2).
The invention also relates to an electromechanical structure obtained by the method.
Description
- The present invention relates to a method of fabricating an electromechanical structure presenting a substrate of the monocrystalline layer type (being made in particular of silicon, germanium, perovskite, or quartz) on a sacrificial layer, in particular for a microsystem or a micro-electromechanical system (MEMS) or a nano-electromechanical system (NEMS), said substrate presenting at least one mechanical reinforcing region (or “pillar”).
- So-called surface technologies (in contrast with bulk technologies) enable the size of electromechanical structures (MEMS and/or NEMS) made on silicon to be reduced. These technologies rely on using a stack of at least three layers: a mechanical layer (typically 0.1 micrometer (μm) to 100 μm thick); a sacrificial layer (typically 0.1 μm to a few Am thick); and a support (typically 10 μm to 1000 μm thick). Selective chemical etching of the sacrificial layer makes it possible to provide functional structures in the mechanical layer that are locally independent of the support.
- The non-etched zones of the sacrificial layer enable so-called “anchor” zones or mechanical reinforcement zones (or “pillars”) to be made that serve to connect the mechanical structure to the support.
- In known methods that enable such pillars to be incorporated, e.g. the method described in application WO 2006/035031, a silicon substrate is assembled by molecular bonding to the top of the oxide layer, which oxide layer then acts as the sacrificial layer during final fabrication of the MEMS. During the final fabrication, trenches are formed through the silicon substrate that has been assembled by molecular bonding and the sacrificial layer is removed. The pillars serve to support the microsystem. During that operation, the interface zone between the added substrate and the remainder of the structure is subjected to chemical etching (in general with HF acid), thereby leading to shapes that are poorly controlled if the interface is not perfect, since the speed of etching is variable, and there is a risk of revealing the bonding interface. After the sacrificial layer has been removed, and the MEMS structure has been released, mechanical integrity is not good.
- Other known methods that reflect that drawback are described in particular in U.S. Pat. No. 6,916,728 (FIGS. 9 and 10;
column 6, lines 20 to 47) and U.S. Pat. No. 6,952,041 (FIGS. 4a to 4f;column 8; line 28 tocolumn 9, line 49). - The article by T. Yamamoto et al. “Capacitive accelerometer with high aspect ratio single crystalline silicon microstructure using the SOI structure with polysilicon-based interconnect technique”, published in MEMS 2000, the thirteenth annual international conference, Jan. 23-27, 2000, Miyazaki, Japan, pp. 514-519 does not present that drawback. Nevertheless, the pillars are made of thick poly-Si and their lateral size is limited by the technology. The pillars are made in the sacrificial layer by filling from a deposit of poly-Si. Filling takes place via the flanks of the cavity so the thickness of the filling is greater than half the width of the pillars. In order to avoid depositing layers of poly-Si that are too thick (typical maximum 3 μm), the lateral size of the pillar is typically limited to 5 μm.
- If filling takes place via the bottom of the cavity, the thickness to be deposited is than about 3 times to 5 times the thickness of the sacrificial layer so as to enable the layer to be planarized.
- The article by G. J. O'Brien and D. J. Monk entitled “MEMS process flow insensitive to timed etch induced anchor perimeter variation on SOI and bulk silicon wafer substrates”, published in IEEE 2000, pp. 481-484, and U.S. Pat. No. 6,913, 941, in particular its FIGS. 27 and 28, show pillars that pass both through the sacrificial layer and through the mechanical layer. In that configuration also, the cavities are filled via the flanks thereby limiting the lateral size of a pillar. Filling with poly-Si may be preceded by depositing a fine nitride layer to insulate the outside of the pillar.
- Known methods are therefore limited to pillars of width that is limited to the thickness of the poly-Si layer used for filling them. For reasons of technology and of expense, the thicknesses used are typically of the order of a few μm, thereby limiting the lateral dimensions of pillars to a few μm.
- There is another reason why known methods limit the lateral dimensions of pillars that are filled using poly-Si when the method contains a step of bonding a second silicon substrate (above-mentioned article by T. Yamamoto).
- In order to make it easier to bond a first silicon substrate containing a thick layer (typically a few μm thick) of a material that is other than silicon (with different stress or expansion coefficients) on a second substrate of silicon, a known method consists in making a second layer of the second material on the other face of the first substrate with the same thickness as the first layer in order to compensate for the deformations induced by the differences between the said material and silicon, and make it easier to put the two substrates into contact during bonding. Such a method is described by Yamamoto, the first substrate containing as its thick layer at least the sacrificial layer of SiO2. In the known methods of making pillars in the sacrificial layer, the material used for filling is thick poly-Si. Since the stress state of polycrystalline Si (at the time of deposition or during heating) is different from that of SiO2, limiting the lateral dimensions of the pillars serves to limit non-uniformities in the sacrificial layer.
- The present invention proposes a fabrication method that enables mechanical reinforcing pillars to be fabricated in versatile manner, i.e. without limitation on their width, so their width can be a function of the intended application, and the pillars can be selected to be insulating or conductive at will, in particular in order to enable a contact to be made, while avoiding the drawback of any risk of revealing the bonding interface of a substrate on the sacrificial layer. A variant of the method makes it possible to limit the topology that stems from fabricating pillars.
- The invention thus provides a method of fabricating an electromechanical structure presenting a first substrate including at least one layer of monocrystalline material covered in a sacrificial layer that presents a free surface, the structure presenting at least one mechanical reinforcing pillar received in said sacrificial layer, wherein the method comprises:
- a) making at least one well region in the sacrificial layer by etching, at least in the entire thickness of the sacrificial layer, the well region defining at least one said mechanical pillar;
- b) depositing a first functionalization layer of a first material, relative to which the sacrificial layer is suitable for being etched selectively, the functionalization layer filling at least one well region at least partially and covering the free surface of the sacrificial layer at least around the well region(s); and
- b′) depositing a filler layer of a second material different from the first material for terminating the filling of the well region(s), said filler layer covering the first functionalization layer at least in part around the well region(s), and planarizing the filler layer, the pillar(s) being formed by the superposition of at least the first material and the second material in the well region(s);
- and releasing the electromechanical structure by removing the sacrificial layer.
- It should be observed that when the pillars pass through the sacrificial layer only, filling with the second material involves only a thickness that is substantially equal to the thickness of the sacrificial layer, and as a result there is no limit on making pillars that are wide (e.g. several tens of μm and more precisely 50 μm, for example).
- The monocrystalline material may be selected in particular from Si, Ge, quartz, or indeed perovskite.
- The substrate may be a thick Si substrate or it may be a substrate of the SOI type in particular, or indeed a substrate having a stop layer (SiGe, porous Si). The etching the sacrificial layer to form at least one well may be performed through at least one opening in a mask deposited on the sacrificial layer.
- The planarization of the second layer may be continued until the first functionalization layer is reached, in particular to ensure that the second layer does not remain in the well regions.
- The method may optionally include:
- c) assembly with a second substrate opposite from the first substrate via an assembly surface of the first substrate. The second substrate is advantageously of the same kind as the monocrystalline layer of the first substrate.
- Advantageously, the second substrate presents an assembly surface that is covered in a bonding layer, e.g. of silicon oxide.
- Prior to step c), the invention may implement depositing a bonding layer on the first and/or second substrate with an interface being formed between these two substrates. A bonding layer in the second material may be made on the first substrate prior to bonding.
- The first material may for example be silicon nitride or polycrystalline Si. The second material may be silicon oxide, or optionally doped polycrystalline Si, a metal, or a polymer.
- The method may subsequently present a step d) of etching the sacrificial layer through at least one through opening in the first substrate in order to release the electromechanical structure. The first substrate is advantageously thinned prior to performing step d) by one or more filling techniques (chemical-mechanical planarization (CMP), rectification, dry etching, wet etching, . . . ).
- Before or after step b′) of depositing a filler layer and of planarizing the filler layer, the method may include a step b″) of making at least one well in the first functionalization layer when said layer is an insulating layer and optionally in the filler layer, which well extends at least as far as the sacrificial layer, and depositing a conductive material at least in said well(s) to form at least one electrode.
- It may be advantageous between steps b′) and b″) to deposit an additional layer of the first material in such a manner as to thicken the insulating first layer, in particular when the planarization of the second layer is continued until the first layer is reached.
- After step b″), provision may be made to deposit a layer including at least one conductive region, e.g. a plane region forming a ground plane.
- In order to make the conductive pillars that enable contact to be made, in particular interconnection to be made, the first layer may be made of a conductive material, in particular doped polycrystalline Si, a metal, or a metal and semiconductor alloy.
- In a first variant, the method may include the first functionalization layer and a second functionalization layer, one of the functionalization layers being conducive and the other insulating, and between steps b) and b′), it may include a step b0) of depositing the second functionalization layer, with the functionalization layer that is conductive forming a first interconnection level.
- The second functionalization layer may be made of a third material selected from: silicon nitride; doped or insulating polysilicon Si; and a metal.
- The first functionalization layer may cover a portion only of the well region(s), the other portion of the well regions being covered by the second functionalization layer, thereby enabling the conductive pillars and insulating pillars to be formed.
- The sacrificial layer may be covered by both the first and second functionalization layers together.
- Alternatively, the second functionalization layer may cover the entire surface of the sacrificial layer and of the third functionalization layer.
- The second material of the filler layer may be selected to be identical to the material of the sacrificial layer.
- In a variant where the first functionalization layer is insulating and thus the second functionalization layer is conductive, the method may include, after step b0), a step b′1) of depositing an insulating layer that forms a third functionalization layer.
- Planarizing the filler layer may then be continued until the third functionalization layer is reached.
- After step b′1), the method may include a step b′2) of making at least one via in said third functionalization layer and of depositing a conductor at least in said via, said deposit forming a contact on the conductive second functionalization layer so as to form a second interconnection level.
- The method may include successively depositing additional functionalization layers alternatively of conductive material and of insulating material and making vias so as to form additional interconnection levels from the conductive layers.
- The last of said interconnection levels may cover the entire surface so as to form a ground plane.
- Alternatively, the last interconnection level is plane and includes interconnection areas to make it possible, during assembly with the second substrate, to connect elements of the second substrate to the electromechanical structure.
- The invention also provides an electromechanical structure presenting a first substrate presenting at least one monocrystalline layer, a sacrificial layer, and at least one mechanical reinforcing (supporting) pillar received in the sacrificial layer, the structure being suitable for being fabricated by a method as defined above, and wherein at least one mechanical support region is a well region received at least in the entire thickness of the sacrificial layer, at least one said well region being covered in a first layer of a first mechanical support material and being filled with a second layer of a second mechanical support material, the pillar(s) being formed by superposing at least the first and second materials in the well region(s).
- The invention can be better understood on reading the following description with reference to the accompanying drawings, in which:
-
FIGS. 1 a to 1 f show a method of the invention that serves in preferred manner to make two-material reinforcements or pillars,FIG. 1 d′ showing an advantageous variant of the method; -
FIGS. 2 a to 2 d show a variant of the method of the invention in which there are so-called conductive or insulating pillars, andFIGS. 2 c 1, 2c -
FIGS. 3 a to 3 d show a variant of the method of the invention enabling interconnection levels to be made using planar technology, withFIGS. 3 c 1 to 3c 8 constituting an implementation with a plurality of interconnect levels; and -
FIG. 4 shows, by way of example, a pressure sensor made with the method ofFIGS. 1 a to 1 f. -
FIGS. 1 a to 1 f show a preferred implementation of the method of the invention, serving to enable insulating pillars to be made from wide trenches (e.g. several tens of μm and more precisely 50 μm for example). The method starts with asubstrate 1 presenting at least onemonocrystalline layer 1′ (e.g. of monocrystalline Si), coated in a sacrificial layer 2 (e.g. SiO2). Thelayer 1′ may occupy all of the substrate (thick Si substrate) or only a portion thereof (e.g. the top layer of an SOI substrate or some other type of substrate presenting an etching stop layer). Preferably, the initial substrate is a silicon substrate including a monocrystalline SiGe stop layer (not shown in the figure) and amonocrystalline silicon layer 1′. Thelayer 2 may be an oxide deposited by low pressure chemical vapor deposition (LPCVD) or by plasma-enhanced CVD (PECVD), or it may be made by thermally oxidizing thelayer 1′. Its thickness may lie in the range 200 nanometers (nm) to 5 μm (typically in therange 2 μm to 3 μm). - A
layer 3 of photosensitive resin is exposed to enable one or more zones such as 5 1 to be made in the layer 2 (FIG. 1 a), these zones providing recesses for making the reinforcing region(s). The reinforcing regions may be open zones or they may be closed zones, e.g. annular or polygonal, as applies to a pressure sensor. - After removing the
resin 3, afunctionalization layer 4 is deposited on thelayer 2, e.g. a silicon nitride layer having thickness lying for example in therange 10 nm to 500 nm, thereby providing alayer 4 1 on the side walls of the zone(s) 5 1, and alayer 4 2 on the bare face of the substrate 1 (FIG. 1 b) (note: 4 1 and 4 2 can be seen inFIGS. 1 b and 1 e). The nitride may be deposited by chemical vapor deposition, in particular LPCVD or PECVD or by using atomic layer CVD (ALCVD). Thelayer 4 may also be made of optionally doped polysilicon, or of a metal, or of a metal and semiconductor alloy. It needs to present etching selectivity relative to the sacrificial layer. This layer does not necessarily cover the entire surface of the sacrificial layer (it may be etched locally). It enables insulating or conductive pillars to be made depending on the nature of the material constituting thefunctionalization layer 4, acting as etching stops for the sacrificial layer and as electrical contacts leading to themechanical layer 1′ when the pillars are conductive. - Alternatively, the
region 4 2 of thelayer 4 may be anchored in thelayer 1′ by using the technique described in Frenchpatent application FR 2 859 201. That involves continuing etching the zone 5 1 in the Si so as to be able subsequently to anchor the pillar in a shallow depth (e.g. 100 nm to 500 nm) by means of theregion 4 2, but without the pillar going through saidlayer 1′. The etched zones in the sacrificial layer makes it possible to provide functional structures in the mechanical layer that are locally independent of the support. - The non-etched zones of the sacrificial layer make it possible to make so-called anchor zones or mechanical reinforcement zones (or “pillars”). The
layer 4 is referred to as the “functionalization” layer since it enables functions to be added to the sacrificial layer: pillars made with etching stops, electrodes under the sacrificial layer, electrical connections between the mechanical layer and said electrodes, or between portions of the mechanical layer that are not interconnected. - Another insulating or
non-insulating layer 6 referred to as a filler layer and made of a material that is different from thelayer 4, e.g. of SiO2, is then made (e.g. by LPCVD or by PECVD) so as to fill the zone(s) 5 1 and so as to cover all or part of thelayer 4 covering the layer 2 (FIG. 1 c). In particular, after providing total coverage as shown inFIG. 1 c, it is possible to etch thelayer 6 locally so that only aportion 6′ remains surrounding the region(s) 5 1 (see Schiltz and Pons “Two-layer planarization process”, J. Electrochem. Soc. 133: 178-181 (1986)). If the filler layer is made of the same material as the sacrificial layer, as in the example shown, then thelayer 2 must cover the entire surface. - Thereafter, starting from the configuration of
FIG. 1 c, thefiller layer pillars 9 constituted by theregions FIGS. 1 d and 1 d′). The method used for this purpose is chemical mechanical planarization (CMP), for example. This planarization may be carried out so as to remove only a fraction of the thickness of the layer 6 (FIG. 1 d′), or as shown inFIG. 1 d, it may be continued and come to an end at thelayer 4 of silicon nitride, allowing a substantially plane face to appear at the pillar (4 1, 4 2, 6 1). Thereafter, athin bonding layer 7 is deposited, e.g. an oxide layer (optionally followed by CMP), thereby making it possible subsequently to add on asubstrate 8 of monocrystalline Si by molecular bonding (molecular bonding between Si and SiO2), optionally oxidized at its surface that comes into contact with the layer 7 (molecular bonding SiO2 and SiO2) (FIG. 1 e). This deposit is optional when only a portion of the thickness of thelayer 6 is removed (FIG. 1 d′). It may also be omitted from the configuration ofFIG. 1 d, but that leads to bonding via a heterogeneous interface, thereby giving rise, other things being equal, to bonding energies that are smaller. - An important reason for selecting SiO2 as a filler is its ability to be deposited as a thick layer with little mechanical stress relative to the other materials such as silicon nitride or polysilicon, and also because of its suitability for being planarized with the thoroughly-mastered CMP technique. Furthermore, when the sacrificial layer is also made of SiO2, that makes it possible to limit non-uniformities of the sacrificial layer after functionalization; the layer is made for the great majority out of a single material. The filler layer is thus preferably made out of the same material as the sacrificial layer.
- In order to obtain a
silicon substrate 1 of thickness suitable for making an MEMS (e.g. 5 μm to 50 μm thick), it is general practice to begin with a starting substrate that is thicker than thesingle layer 1′, with this substrate subsequently being thinned to the desired thickness after thesubstrate 8 has been molecular bonded thereto. Such thinning may be performed by rectification followed by CMP. - When the
layer 1′ is made of monocrystalline silicon grown on the SiGe stop layer, the silicon portion of the initial substrate is rectified to a thickness of about 10 μm. The thickness is determined by the accuracy that is available for this rectification step and also in such a manner that thelayer 1′ does not include any work-hardened zones, which zones are created during the rectification step. It is thus a function in particular of the desired speed of rectification. - The thickness of the remaining Si of the initial substrate is subsequently removed by chemical etching, stopping at the SiGe stop layer. Various methods are known for etching Si and stopping on SiGe. Mention can be made of wet etching methods (mixtures of the tetramethylammonium hydroxide (TMAH) or of the KOH type, cf. bibliography on selecting etching) or dry etching (Japanese Journal of Applied Physics, Vol. 43, No. 6B, 2004, pp. 3964-3966, 2004 The Japan Society of Applied Physics). The stop layer is subsequently removed by chemical etching stopping at the Si of the
layer 1. - Various known methods exist for etching SiGe and stopping on Si. Mention can be made of high temperature HCl etching methods (“Selective chemical vapor etching of Si1-xGex versus Si with gaseous HCl”, by Y. Bogumilowicz, H. M. Hartmann, J. M. Fabri, and T. Bilon, in Semicond. Sci. Technol. 21, No. 12 (December 2006), pp. 1668-1674, chemical etching methods based on mixtures of the hydrofluoric acid, nitric acid, and acetic acid (HNA) type, and dry etching methods (see above-mentioned article in Japanese Journal of Applied Physics). This use of a starting substrate made up of a layer of SiGe on thick silicon provides better control over the final thickness of the
layer 1. - Depositing the
layer 7 is optional, it being possible for thesubstrate 8 to be added by the technique described in patent application WO 2006/035031. That technique enables molecular bonding to be established between thesubstrate 8 and the surface made up of two different materials, in particular silicon nitride and SiO2. - The method continues (
FIG. 1 e) in the upside-down position, as in the prior art method described in the introduction to the present description. - Then, the process according to the invention further comprises a step of releasing the electromechanical structure by removing at least partially the
sacrificial layer 2. The removal of the sacrificial layer can be done by etchingopenings 10, but also by any other means. - The
Si layer 1′ is etched to make one or more openings 10 (FIG. 1 f). Theseopenings 10 may also serve to define the MEMS structure in thelayer 1′ and they are used to remove thesacrificial layer 2 by forming one ormore cavities 2 1 with the help of hydrofluoric acid in the liquid phase or the vapor phase, when etching a layer of SiO2, such that the active structure ofFIG. 1 is held by the pillar(s) (4 1, 4 2, 6 1). The pillar materials are selected so as to be selective relative to the solution used for etching the sacrificial layer. The mechanical structure is thus made in thelayer 1′ which can be referred to as a mechanical layer. - It can be seen that the
interface zone 8′ between thesubstrate 8 fitted by molecular bonding and thelayer 7 is protected from any chemical etching when making the opening(s) 10 and when releasing the MEMS structure by using HF acid to remove thesacrificial layer 2. -
FIGS. 2 a to 2 d′ show a variant embodiment in which the pillars include a conductive layer, here made of polycrystalline Si, thus enabling contacts to be made, and indeed multiple interconnection levels by combining conductive pillars and insulating pillars. - As in
FIG. 1 a,FIG. 2 ashows wells 35 being made in thesacrificial layer 2, e.g. made of SiO2, on asubstrate 1 comprising in particular alayer 1′, e.g. made of monocrystalline Si. -
FIG. 2 b shows localized deposition (deposition over the entire surface and then localized etching) of an insulatingfirst functionalization layer 31 made of silicon nitride, in particular on well zones where the insulating pillars are to be made. This nitride layer serves to provide insulating pillars and to isolate the polycrystalline Si layer (see description below) chemically from themechanical layer 1 and thesacrificial layer 2 of the filler layer when made of the same material as the sacrificial layer. -
FIG. 2 c shows the localized deposition (in particular by deposition of the entire surface followed by localized etching) of a conductivesecond functionalization layer 30, e.g. of doped polycrystalline Si inwell regions 351 where it is desired to make pillars that also perform a conductive function, in particular for making contact with the layer 1 (mechanical layer). Outside well regions, this layer may also serve to make a first interconnection level or electrodes. Theother wells 35 2 may have no deposit of polycrystalline Si in order to limit capacitive coupling at the insulating pillars. This does not apply if, for reasons of topology, an electrical connection needs to be passed through an insulating pillar as shown in thewells 35 1. It should be observed that the insulatingfunctionalization layer 31 may be deposited after theconductive functionalization layer 30. However if the materials of thelayers wells 35 1, and then after thelayer 30 has been made, the functionalization layer is etched in thewells 35 2. -
FIG. 2 d shows deposition of afiller layer 32, e.g. of SiO2, for filling thewells 35. This deposition is subsequently planarized by using a thinning technique, e.g. the CMP method. - The pillars thus have either an external
conductive layer 31 made of polycrystalline Si, or else an insulatinglayer 30 at alayer 32, e.g. of SiO2, constituting the core thereof. Depending on circumstances, the pillars are therefore made of two materials or of three materials. -
FIGS. 2 c 1, 2c - This second level of interconnection layer enables tracks to be made that electrically interconnect two
conductive zones 30 made of polycrystalline Si (conductive pillars or electrodes) that are not interconnected by the first level, for topological reasons. -
FIG. 2 c 1 shows an insulating layer 34 (nitride or oxide) being deposited for the purpose of insulating the interconnection layers. This layer is etched locally with etching stopping at thelayer 30, thereby enabling electrical accesses (aa) to be provided on thezones 30 for connection. -
FIG. 2 c 2 shows a second localized conducive layer being made that serves to interconnect the electrical accesses (aa) in application of the interconnection scheme. Vias are thus provided between the first and second interconnection levels. - These operations (depositing the insulating layer with openings, localized deposition of polycrystalline Si) can be repeated so as to make multiple interconnection levels using additional conductive and insulating functionalization layers.
- In particular, a last layer can be made as a layer that covers the entire component, optionally being connected to one or more tracks of the lower layers, and acting as a ground plane for the MEMS system.
- Depending on circumstances, the ground plane may also be made at the same level as the last track, in which case it covers part of the surface only.
- Finally,
FIG. 2 d′ shows a filler andbonding layer 40, e.g. made of silicon oxide, being deposited on the structure obtained inFIG. 2 c 2. -
FIGS. 3 a to 3 d show another variant of the method enabling the topology due to the various deposited layers to be limited: each localized deposition increases the topology of the final stack initially created by making zones such as 5 1 in the sacrificial layer. -
FIG. 3 a shows the substrate after layers ofnitride 31 and ofpolycrystalline Si 30 have been deposited in succession using a method such as that described with reference toFIGS. 2 a to 2 c. To obtain a plane reference surface, theSiN layer 31 is made over the entire substrate apart from the zones of the polycrystalline Si pillars (layer 30). In the same manner, the polycrystalline Si layer is made over the entire surface of thelayer 2, removing only the zones that serve to insulate those zones that need to be insulated. -
FIG. 3 b shows anadditional layer 35 made of SiN being deposited that serves as a reference for rectifying the filler layer. -
FIG. 3 c shows deposition of thefiller layer 36 made of SiO2 after chemical mechanical planarizing (CMP) stopping at theSiN layer 35. -
FIG. 3 d shows deposition and planarizing of asecond bonding layer 37, e.g. made of SiO2, serving to achieve bonding. - It is also possible to make multiple interconnection levels using the so-called “double damascene” principle. After the steps of
FIG. 3 c, an additional oxide layer is made (FIG. 3 c 1) for use as insulation. This layer is locally etched to make openings (FIG. 3 c 2) corresponding to electrical connections between interconnection tracks. A polycrystalline Si layer is deposited on the entire plate, followed by CMP, stopping at the oxide, thereby leavingpolycrystalline Si 39′ only in the openings 39 (FIG. 3 c 3). -
FIG. 3 c 4 shows nitride andoxide layers FIG. 3 c 5). Thetracks 53 are made (FIG. 3 d 6) by depositing doped polycrystalline Si with CMP and stopping on the oxide constituting thelayer 51. - If an additional interconnection level is needed, the same principle can be repeated: an
oxide layer 54 is made withOpenings 55 being created therein (stop at the polycrystalline Si of the tracks 53) for the electrical connections (FIG. 3 c 7). These openings are filled with dopedpolycrystalline Si 56 by full wafer deposition, followed by CMP stopping at the oxide of thelayer 54. The steps described inFIGS. 3 c 4 to 3c 6 are repeated. - Starting from the steps of
FIG. 3 c 3, it is possible to replace the polycrystalline Si with a metal, such as copper, for example. - Under such circumstances, it is possible to replace the
substrate 8 with a substrate having CMOS circuits and terminated by a layer of Cu areas in a matrix of SiO2. In this variant, the bonding layer ofFIG. 3 d is not added since it is the combined oxide and Cu layer that acts as the bonding layer. This bonding serves to provide electrical connections between the MEMS substrate and the associated CMOS circuit substrate. Only a fraction of the metal areas needs to serve as electrical connections between the MEMS and the CMOS circuit, with the remainder being made to increase the effective bonding area. Under such circumstances, the electrical connection with the MEMS and CMOS circuit assembly take place via contacts made at the surface of the MEMS. - It should be observed that the principle of bonding a CMOS circuit from an array of metal areas can be implemented even if the method used for making interconnections it not planar. For example, starting from the substrate of
FIG. 2 d′, it is possible to make a plane of contact areas by adding a nitride layer and an oxide layer and then by making the array of areas using the method described Starting fromFIGS. 3 c 4. - The plane of contact areas may be replaced by a continuous metal plane connected to a limited number of MEMS connection tracks and enabling electrical contacts to be established between the support and the MEMS ground.
- By way of example,
FIG. 4 shows a pressure sensor made in accordance with the method ofFIGS. 1 a to 1 f. Anopening 10 is made through thesubstrate 1 within the perimeter of a pillar 9 (4 1, 4 1, 6 1) of annular shape, and this opening is used for removing thesacrificial layer 2 within this perimeter so as to form acavity 21. Theopening 10 is then recovered in conventional manner, e.g. with polycrystalline silicon phosphosilicate glass (PSG). Theregion 22 of thesubstrate 1 that is situated in the perimeter of thepillar 9 forms the diaphragm of the pressure sensor and it is mechanically supported by the pillar. - It is naturally possible to define one or
more openings 10 for making MEMS of more complicated structure, e.g. including one or more fixed-end beams. - Although the examples given essentially illustrate making a substrate in which the monocrystalline layer is made of silicon associated with a sacrificial layer made of SiO2, the invention enables substrate variants to be made, in particular a substrate with a layer of monocrystalline germanium associated with a sacrificial layer of SiO2, or indeed a substrate with a layer of monocrystalline perovskite associated with a sacrificial layer of polycrystalline Si or of SiO2.
Claims (24)
1. A method of fabricating an electromechanical structure presenting a first substrate including at least one layer of monocrystalline material covered in a sacrificial layer that presents a free surface, the structure presenting at least one mechanical reinforcing pillar received in said sacrificial layer, wherein the method comprises:
a) making at least one well region (51, 52) in the sacrificial layer (2) by etching, at least in the entire thickness of the sacrificial layer (2), the well region defining at least one said mechanical pillar;
b) depositing a first functionalization layer (4, 31) of a first material, relative to which the sacrificial layer is suitable for being etched selectively, the functionalization layer (4) filling at least one well region (51) at least partially and covering the free surface of the sacrificial layer (2) at least around the well region(s); and
b′) depositing a filler layer (6, 32) of a second material different from the first material for terminating the filling of the well region(s) (5 1), said filler layer (6) covering the first functionalization layer (4) at least in part around the well region(s) (5 1), and planarizing the filler layer (6, 32), the pillar(s) being formed by the superposition of at least the first material and the second material in the well region(s);
and releasing the electromechanical structure by removing at least partially the sacrificial layer (2).
2. A method according to claim 1 , wherein the monocrystalline material is selected from Si, Ge, quartz, or a perovskite.
3. A method according to claim 1 , wherein the filler layer is planarized until the first functionalization layer is reached.
4. A method according to claim 1 , also including:
c) assembly with a second substrate opposite from the first substrate via an assembly surface of the first substrate.
5. A method according to claim 4 , wherein the second substrate presents an assembly surface covered in a bonding layer.
6. A method according to claim 1 , wherein prior to step c) it implements depositing a bonding layer on said assembly surface of the first substrate and/or on the second substrate, said layer forming an interface between the two substrates.
7. A method according to claim 6 , wherein the filler layer is planarized until the first functionalization layer is reached, and wherein a bonding layer of the second material is made on the first substrate prior to bonding.
8. A method according to claim 1 , wherein the first material is selected from: silicon nitride; doped or insulating polycrystalline Si; a metal; and a polymer.
9. A method according to claim 1 , wherein the second material is selected from: silicon oxide; doped or insulating polycrystalline Si; and a polymer.
10. A method according to claim 1 , including a step d) of etching the sacrificial layer through at least one through opening formed in the first substrate, in order to release the electromechanical structure.
11. A method according to claim 1 , wherein before or after step b′), it includes a step b″) of making at least one well in the first insulating layer, which well extends at least as far as the sacrificial layer, and depositing a conductive material at least in said well(s) in order to form at least one electrode.
12. A method according to claim 1 , including the first functionalization layer and a second functionalization layer, one of the functionalization layers being conducive and the other insulating, and in that between steps b) and b′), it includes a step b0) of depositing the second functionalization layer, with the functionalization layer that is conductive forming a first interconnection level.
13. A method according to claim 12 , wherein the second functionalization layer is made of a third material selected from: silicon nitride; doped or insulating polysilicon Si; and a metal.
14. A method according to claim 13 , wherein the first functionalization layer covers a portion only of the well region(s), the other portion of the well regions being covered by the second functionalization layer, thereby enabling the conductive pillars and insulating pillars to be formed.
15. A method according to claim 12 , wherein the sacrificial layer is covered by both the first functionalization layer and the second functionalization layer, together.
16. A method according to claim 12 , wherein the second functionalization layer covers the entire surface of the sacrificial layer and of the third functionalization layer.
17. A method according to claim 1 , wherein the second material of the filler layer is selected to be identical to the material of the sacrificial layer.
18. A method according to claim 12 , wherein the first functionalization layer is insulating, the second functionalization layer is conductive, and in that after step b0) it includes a step b′1) of depositing an insulating layer constituting a third functionalization layer.
19. A method according to claim 18 , wherein planarizing the filler layer continues until the third functionalization layer is reached.
20. A method according to claim 18 , wherein after step b′1), it includes a step b′2) of making at least one via in said third functionalization layer and of depositing a conductor at least in said via, said deposit forming a contact on the conductive second functionalization layer so as to form a second interconnection level.
21. A method according to claim 19 , including successively depositing additional functionalization layers alternatively of conductive material and of insulating material and making vias so as to form additional interconnection levels from the conductive layers.
22. A method according to claim 20 , wherein the last interconnection level covers the entire surface so as to make a ground plane.
23. A method according to claim 19 , wherein the last interconnection level is plane and includes interconnection areas to make it possible, during assembly with the second substrate, to connect elements of the second substrate to the electromechanical structure.
24. An electromechanical structure presenting a first substrate presenting at least one monocrystalline layer, a sacrificial layer, and at least one mechanical reinforcing pillar received in the sacrificial layer, the structure being suitable for being fabricated by a method according to claim 1 , and wherein at least one mechanical support region is a well region received at least in the entire thickness of the sacrificial layer, at least one said well region being covered in a first layer of a first mechanical support material and being filled with a second layer of a second mechanical support material, the pillar(s) being formed by superposing at least the first and second materials in the well region(s).
Priority Applications (1)
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US13/912,307 US10290721B2 (en) | 2008-06-23 | 2013-06-07 | Method of fabricating an electromechanical structure including at least one mechanical reinforcing pillar |
Applications Claiming Priority (2)
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FR0803495A FR2932789B1 (en) | 2008-06-23 | 2008-06-23 | METHOD FOR MANUFACTURING AN ELECTROMECHANICAL STRUCTURE COMPRISING AT LEAST ONE MECHANICAL REINFORCING PILLAR |
FR0803495 | 2008-06-23 |
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US13/912,307 Division US10290721B2 (en) | 2008-06-23 | 2013-06-07 | Method of fabricating an electromechanical structure including at least one mechanical reinforcing pillar |
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US20090321887A1 true US20090321887A1 (en) | 2009-12-31 |
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US12/488,841 Abandoned US20090321887A1 (en) | 2008-06-23 | 2009-06-22 | Method of fabricating an electromechanical structure including at least one mechanical reinforcing pillar |
US13/912,307 Active 2031-02-01 US10290721B2 (en) | 2008-06-23 | 2013-06-07 | Method of fabricating an electromechanical structure including at least one mechanical reinforcing pillar |
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US13/912,307 Active 2031-02-01 US10290721B2 (en) | 2008-06-23 | 2013-06-07 | Method of fabricating an electromechanical structure including at least one mechanical reinforcing pillar |
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US (2) | US20090321887A1 (en) |
EP (1) | EP2138453B1 (en) |
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US20140077317A1 (en) * | 2012-09-14 | 2014-03-20 | Solid State System Co., Ltd. | Microelectromechanical system (mems) device and fabrication method thereof |
US8692337B2 (en) | 2011-07-12 | 2014-04-08 | Commissariat A L'energie Atomique Et Aux Energies Alternatives | Structure with a moving portion and a buried electrode for movement detection included in a multi-substrate configuration |
US9783407B2 (en) | 2011-07-12 | 2017-10-10 | Commissariat à l'énergie atomique et aux énergies alternatives | Method for making a suspended membrane structure with buried electrode |
CN113039635A (en) * | 2018-09-14 | 2021-06-25 | 索泰克公司 | Method of manufacturing advanced substrate for hybrid integration |
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Also Published As
Publication number | Publication date |
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FR2932789A1 (en) | 2009-12-25 |
EP2138453A1 (en) | 2009-12-30 |
US10290721B2 (en) | 2019-05-14 |
FR2932789B1 (en) | 2011-04-15 |
JP2010005784A (en) | 2010-01-14 |
JP5511235B2 (en) | 2014-06-04 |
US20130273683A1 (en) | 2013-10-17 |
EP2138453B1 (en) | 2012-11-21 |
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