KR20160103756A

KR20160103756A - Cosmetic composition comprising extract of plant

Info

Publication number: KR20160103756A
Application number: KR1020150026519A
Authority: KR
Inventors: 함동곤; 한승호
Original assignee: 울산과학대학교 산학협력단
Priority date: 2015-02-25
Filing date: 2015-02-25
Publication date: 2016-09-02

Abstract

The present invention relates to a cosmetic composition comprising chrysanthemum, green tea, lemon or cinnamon extract, and more particularly to a cosmetic composition comprising extracts from one or more plants selected from the group consisting of chrysanthemum, green tea, lemon and cinnamon, ethanol, purified water, glycerin and essential The cosmetic composition according to the present invention can be effectively used as a cosmetic for deodorant because it has few chemical components, does not clog pores, less irritation to skin, and has anti-mosquito effect and antibacterial effect.

Description

[0001] Cosmetic composition comprising extract of plant [

The present invention relates to a composition for external use containing a tannin-containing plant extract, and more particularly to a cosmetic composition containing a tannin-containing chrysanthemum, green tea, lemon or cinnamon extract.

People develop various body odor depending on their race or societies, and mainly produce odorous substances in specific areas such as head, armpits, palms and soles, which have many fine lines and sebaceous glands. The human body has a line of eczrine and an apocrine, and the sweat secreted from the apocrine contains milk, protein, lipid, fatty acid, cholesterol, glucose, ammonia and iron.

The secreted sweat itself does not produce a strong odor, but the various skin microbes living in the stratum corneum exhibit abnormal proliferation while decomposing the keratin. In this process, the proteins contained in the sweat are decomposed to form isovaleric acid acid, which is known as the cause of odor.

Therefore, cosmetic products for suppressing the generation of odor causing substances, restricting the secretion of perspiration, or suppressing the growth of skin flora have attracted attention.

The deodorant, one of the cosmetics for the disposal, was first developed in 1888 as a wax-like cream with the trademark "Mum", and zinc chloride was used as a major desiccant. This product inhibited the growth of bacteria that occurred when the axilla was moistened and suppressed the cancer. In the early 20th century, powdered sodium hydrogencarbonate mixed with common deodorant and talc was used. In the late 1940s solid aluminum chloride-based deodorant was developed, but there was a side effect of hair loss.

At present, deodorant is a typical ingredient that prevents perspiration as a main ingredient. Aluminum Chlorohydrate (ACH) and triclosan are used as a representative component for killing microorganisms.

However, in Science Daily, when aluminum is used as a sunscreen, it has been reported that not only skin cancer but also oxidation promoting action of aluminum can cause skin damage. In addition, there is a problem that the ACH is accumulated in the human body when the ACH is used over a long period of time.

The above-mentioned triclosan is used as an antibiotic substance and a disinfectant, but it does not show an antibacterial effect and affects a hormone. It transforms a bacterium into a form difficult to cure, causes infertility, sexual maturity and cancer induction, Thereby increasing the possibility of mass production.

Therefore, in order to solve the above-mentioned problems such as safety and side effects, it is necessary to study a substitute material. In particular, studies on cosmetic compositions containing natural substances derived from natural products in association with environmentally friendly hot air are required.

1. Korean Patent No. 10-0785974.

In order to solve the above problems, it is an object of the present invention to provide a cosmetic composition comprising a plant ingredient.

In order to achieve the above object, the present invention provides a plant containing a plant ingredient, which comprises an extract extracted from at least one plant selected from the group consisting of chrysanthemum, green tea, lemon and cinnamon, ethanol, purified water, glycerin and essential oil Thereby providing a cosmetic composition for taking.

The cosmetic composition for ointment containing the extract, ethanol, purified water, glycerin and essential oil extracted from at least one plant selected from the group consisting of chrysanthemum, green tea, lemon and cinnamon of the present invention has few chemical components, (Mosquito repellent) effect and anti-bacterial effect. Therefore, it can be effectively used as a cosmetic product for deodorant.

1 is an image of a chrysanthemum, green tea, lemon or cinnamon extract contained as an active ingredient of the present invention,
FIG. 2 shows the result of confirming the color reaction,
FIG. 3 is a result of evaluating the coloring after spraying a deodorant containing chrysanthemum extract or lemon extract.

The inventors of the present invention have studied the functionality of a natural material extract derived from a natural substance in which no problem of tolerance or safety has been raised. A deodorant composition containing a plant extract obtained from chrysanthemum, green tea, lemon or cinnamon was prepared, As a result of comparison with deodorant, it was confirmed that excellent deodorizing effect was exhibited and the present invention was completed.

Hereinafter, the present invention will be described in more detail.

The present invention relates to a cosmetic composition comprising a botanical ingredient, characterized in that it comprises an extract extracted from at least one plant selected from the group consisting of chrysanthemum, green tea, lemon and cinnamon, ethanol, purified water, glycerin and essential oil.

As used herein, the term deodorant refers to a cosmetic composition for removing or suppressing the odor of a specific region of a human body by suppressing the secretion of sweat, which is an antioxidant, It is a concept to include.

In the present specification, deodorization refers to suppressing or controlling discomfort or odor of the body.

Adding the anhydrous ethanol to at least one plant selected from the group consisting of chrysanthemum, green tea, lemon and cinnamon, mixing, aging and refrigeration; Heating the aged mixture in a hydrothermal distiller; Quenching the distilled extract through the heating; And filtering the rapidly cooled extract.

In addition, the extract includes 0.5 to 10 parts by weight of tannin per 100 parts by weight of the extract.

The tannins are special phenolic compounds that are extensively present in the plant system and are named for their ability to bind to other polymers such as proteins or polysaccharides (Damodaran et al., 2008). Tannins are found in the bark of oak trees and in various fruits, and a paper on the physiological activity of tannin fractions from different fruits is being published. The color range of tannin corresponds to yellowish-white to light brown and is involved in the bitter taste of food. The structure of tannins is very complex and is generally divided into two groups: hydrolysable tannins and condensed tannins. Hydrolyzable tannins include ellagitannin consisting of gallotannin or ellagic acid and saccharide-bonded hexahydroxydiphenic acid, which is formed by a combination of gallic acid and sugar. have.

The essential oil may be at least one selected from the group consisting of tea tree, citronella, rose geranium and orange, but is not limited thereto.

The chrysanthemum is preferably, but not limited to, a bug bug.

The bug kingdom means chrysanthemum which can kill insects, and it contains insecticidal component called pyrethrins with chemical structure of pyrethroid.

The pyrethrin content of the insect pest is deeply correlated with the area and the flowering season, and it is known that the content difference and composition change are large depending on the variety, climate, soil environment, harvesting and drying, extraction and use methods.

In addition, pyrethrins are intensively contained in flower parts, and are contained in flower buds, leaves, and stems.

Therefore, in the present invention, the full flower portion of the bug bug was used.

Therefore, the cosmetic composition according to the present invention has an effect of mosquito repellency and antibacterial action.

The cosmetic composition of the present invention can be used for the external ointment for skin, basic cosmetics, makeup cosmetics, body cosmetics or shaving cosmetics. Examples of the basic cosmetics include essences, lotions, creams, gels, lotions, Cream, emulsion, etc. Examples of the makeup cosmetics may include foundation, lipstick, eye shadow, eyeliner, mascara, eyebrow pencil, makeup base, etc. Body cosmetics include soap, liquid cleanser, Sunscreen cream, sun oil, etc., and shaving cosmetics include aftershave lotion and shaving cream.

In addition to the extract as the active ingredient, a functional material having a deodorizing effect, an excipient for improving physical properties, and a diluent may be included.

For example, the cosmetic composition may further contain a perfume, a pigment, a bactericide, an antioxidant, an antiseptic, a moisturizer, a thickening agent, an inorganic salt, or a synthetic polymer material to improve physical properties. An organic pigment, an organic pigment, an ultraviolet absorber, a pH adjuster, an alcohol, a blood circulation accelerator, a cold agent, a limiting agent, or purified water may be used as a blending component that may be added.

The cosmetic composition may further comprise at least one member selected from the group consisting of collagen, vitamin B, vitamin C, olive liquid, and water solubil.

The compounding ingredient to be added other than the above-mentioned effective ingredient is not limited, and any of the above-mentioned ingredients can be compounded within a range that does not impair the purpose and effect of the present invention.

The cosmetic composition may take the form of a solution, an emulsion, a viscous mixture or the like, and may be in the form of a spray, an emulsion, a cream, a lotion, a pack, a foundation, a lotion, a serum, Or the like.

More particularly, the cosmetic composition of the present invention can be used as a cosmetic composition in the form of a spray, a soap, a cleansing foam, a cleansing lotion, a cleansing cream, a body lotion, a body cleanser, a skin lotion, a skin softener, a skin toner, an astigmant, a lotion, , Massage cream, nutritional cream, moisturizing cream, hand cream, foundation, essence, nutritional essence and pack.

For example, when the formulation of the present invention is spray or powder, lactose, talc, silica, aluminum hydroxide, calcium silicate or polyamide powder may be used as a carrier component, particularly when the formulation of the present invention is a spray In addition, propellants such as chlorofluorohydrocarbons, propane / butane or dimethyl ether may be included.

When the formulation of the present invention is a paste, cream or gel, animal fiber, plant fiber, wax, paraffin, starch, tracant, cellulose derivative, polyethylene glycol, silicone, bentonite, silica, talc or zinc oxide may be used as the carrier component .

When the formulation of the present invention is a solution or an emulsion, a solvent, a solvent or an emulsifier is used as a carrier component, and examples thereof include water, ethanol, isopropanol, ethyl carbonate, ethyl acetate, benzyl alcohol, benzyl benzoate, -Butyl glycol oil, glycerol aliphatic esters, polyethylene glycols or fatty acid esters of sorbitan.

When the formulation of the present invention is a suspension, a carrier such as water, a liquid diluent such as ethanol or propylene glycol, a suspending agent such as ethoxylated isostearyl alcohol, polyoxyethylene sorbitol ester and polyoxyethylene sorbitan ester, Cellulose, aluminum metahydroxide, bentonite, agar or tracant, etc. may be used.

When the formulation of the present invention is an interfacial active agent-containing cleansing, the carrier component may include aliphatic alcohol sulfate, aliphatic alcohol ether sulfate, sulfosuccinic acid monoester, isethionate, imidazolinium derivative, methyltaurate, sarcosinate, fatty acid amide Ether sulfates, alkylamidobetaines, aliphatic alcohols, fatty acid glycerides, fatty acid diethanolamides, vegetable oils, linolenic derivatives or ethoxylated glycerol fatty acid esters.

Hereinafter, the present invention will be described in more detail with reference to the following examples. However, the scope of the present invention is not limited to the following examples.

< Example 1> Plant extract preparation

Chrysanthemums, green tea, lemon or cinnamon extracts as an active ingredient of the present invention were prepared.

For this purpose, 50 g of chrysanthemum, 50 g of green tea, 50 g of lemon or 50 g of cinnamon and anhydrous ethanol were mixed at a volume ratio of 1: 5, respectively, and aged for 2 weeks and refrigerated. The aged mixture was then placed in a reflux condenser and heated for 2 hours, distilled and quenched. The quenched extract was filtered for 7 hours to prepare each extract as shown in Fig.

< Example 2> of the plant extract Tannin Confirmation of content

Tannin shows a color reaction by the reagents shown in Table 1 below.

FeCl ₃ (1 to 2% alcohol solution) blue Ammonia nitric acid black FeCl ₃ - Periancan Cali blue Gibbs reagent Green purple Calcium iodide aqueous solution Developed in pink (unique properties of water-decomposable tannins)

To confirm whether tannin was contained in the chrysanthemum or green tea extract prepared in Example 1, FeCl ₃ was added to confirm the color reaction. As a control, blueberry extract was prepared according to the method of Example 1, and developed by paper chromatography to confirm the red color reaction. At this time, BAW (n-Butanol: Acetic acid: Water) mixed with 2 to 6% of acetic acid, n-butanol, acetic acid and water in a volume ratio of 4: Respectively.

As a result, as shown in Fig. 2, the chrysanthemum and green tea extracts were discolored to blue by FeCl ₃ , but the blueberry extract showed no change. Therefore, it was confirmed that chrysanthemum and green tea extract contain tannin.

< Example 3> Plant extract Tannin Content measurement

To determine the amount of tannin contained in the plant extract prepared in Example 1, the amount of KMnO4 (potassium permanganate) required to oxidize the oxides in the sample was first determined. Then, the amount of tannin in the sample was removed by reacting with the gelatin, and the amount of KMnO4 reacting with the peroxide other than tannin was determined.

1. Required reagents and preparation thereof

1) KMnO4 (potassium permanganate): To 1.33 g of potassium permanganate was added 998.67 g of water to make 1 L of potassium permanganate.

2) Indigocamin aqueous solution: 6 g of indigocammin and 50 ml of concentrated sulfuric acid were added to a 1-liter beaker, and water (distilled water) was poured until the volume became 1 L.

3) Acid saline: 25ml of concentrated sulfuric acid was added to 975ml of saturated salt water to make 1L of final.

4) Gelatin solution: 25 g of gelatin was immersed in saturated saline solution for 1 hour, gently cooled, and diluted in saline solution.

5) Powdered kaolin

2. Analysis

To 10 ml of the reagent, 20 ml of an aqueous solution of indigocamine and 750 ml of water were placed in a 1-L beaker, and potassium permanganate (KMnO 4) was added thereto and titrated. At this time, the amount of potassium permanganate (KMnO4) was measured until the yellow or pale green color became a red color (A ml).

50 ml of gelatin and 100 ml of acidic saline were added to 100 ml of extract, 10 g of kaolin was added and mixed, and the resulting mixture was filtered through a filter paper in an Erlenmeyer flask. Thereafter, 25 ml of the solution, 20 ml of indigocammin and 750 ml of water were added to a 1 L beaker and titrated with potassium permanganate. At this time, it was determined how much potassium permanganate was introduced (B ml) until yellow or pale green became red.

Tannin was measured according to the following equation (1).

[Equation 1]

Amount of tannin = (A-B) * 0.042

As a result, it was confirmed that 0.02 g of chrysanthemum extract, 0.756 g of green tea extract, 0.042 g of cinnamon extract and 0.02 g of lemon extract were contained.

< Example 4> Deodorant For the composition Tannin Ratio measurement

Since the tannin has a yellowish brown color, there was a risk of discoloration in using the deodorant composition containing the tannin, and a suitable ratio of tannin was measured.

Previously launched products usually add 1 to 10% of tannin.

Based on this, tannin was dissolved in distilled water and sprayed on a white cloth as shown in Table 2 to confirm discoloration. At this time, tannin (company product number) was used.

Distilled water Tannin ratio

100ml
1g One% 3g 3% 5g 5% 9g 9%

20ml
0.2 g One% 0.6 g 3% 1g 5% 1.8 g 9%

As a result, it was confirmed that 20 ml of distilled water + 0.2 g (1%) of tannin had no discoloration.

< Example 5 > Deodorant Manufacturing ratio

The production ratio of the deodorant composition was confirmed based on the ratio of tannin determined in Example 4 above.

Deodorant was prepared in various compositions as shown in the following Table 3, and the volatility, viscosity, texture, antibacterial and insect resistance were evaluated and shown in Table 4 below.

In addition, discoloration was also observed when sprayed onto a white cloth.

material One 2 3 4 5 6 7 8 Cinnamon extract 75% - - - - - - - Green tea extract - 75% - - - - - - Lemon extract - - 75% - - - - - Chrysanthemum extract - - - 75% - - - - ethanol - - - - 75% 75% 75% 75% glycerin 10% 10% 10% 10% 10% 10% 10% 10% Purified water 15% 15% 15% 15% 15% 15% 15% 15% Essential oil - - - - Tea tree Eucalyptus geranium Sheet

material One 2 3 4 5 6 7 8 volatility medium medium medium Prize medium medium Ha Ha Viscosity medium Prize Prize Ha Ha Ha Ha Ha Texture medium Ha Ha Prize medium medium Ha medium Antibiotic - - U U - - - - Insect U - - U U U U U

As a result, it was confirmed that No. 4 containing chrysanthemum extract had excellent volatility and texture, and had antimicrobial and insecticidal effect.

In addition, the results of spraying No. 3 containing lemon extract and No. 4 containing chrysanthemum extract on a white cloth showed that no discoloration was observed as shown in Fig.

< Example 6> Sensory evaluation

Sensory tests were carried out on 30 adult women for the deodorant composition of composition No. 4 identified through Example 5 above. Five points were scored as 'very good', 4 points as 'good', 3 points as 'normal', 2 points as 'bad' and 1 point as 'very bad'. The results of the sensory evaluation of the cosmetic composition of the present invention and the comparative example are shown in Table 5 below. At this time, as a comparative example, a deodorant developed by NIVEA, which is commercially available, was used.

Evaluation items Example (No. 4) Comparative Example incense 4.7 4.7 Texture 4.8 4.5 Sweating effect 4.6 4.4 vitality 4.5 4.5 pepper 4.8 4.3 Overall likelihood 4.8 4.6

As a result, as shown in Table 5, the deodorant composition according to the present invention had similar or better flavor, texture, perspiration inhibitory effect, sustained action, irritation and overall acceptability compared to the comparative examples. Especially, Deodorant 's intense texture is not felt and the irritability is remarkably low.

While the present invention has been particularly shown and described with reference to exemplary embodiments thereof, it will be understood by those skilled in the art that various changes and modifications may be made without departing from the spirit and scope of the invention as defined in the appended claims. will be. Accordingly, the actual scope of the present invention will be defined by the appended claims and their equivalents.

Claims

Wherein the cosmetic composition comprises an extract of at least one plant selected from the group consisting of chrysanthemum, green tea, lemon and cinnamon, ethanol, purified water, glycerin and essential oils.

The method according to claim 1,
Adding the anhydrous ethanol to at least one plant selected from the group consisting of chrysanthemum, green tea, lemon and cinnamon, mixing, aging and refrigeration; Heating the aged mixture in a hydrothermal distiller; Quenching the distilled extract through the heating; And extracting the rapidly cooled extract through a step of filtering the cosmetic composition.

3. The method of claim 2,
Wherein the extract comprises a tannin.

The method according to claim 1,
Wherein the essential oil is at least one selected from the group consisting of tea tree, citronella, rose geranium and orange.

The method according to claim 1,
Wherein the chrysanthemum is a bug bug.