KR20040071087A - Nano-sized particle Vermiculite manufacturing, and thereof its cosmetic pack manufacturing with using its functional property - Google Patents

Nano-sized particle Vermiculite manufacturing, and thereof its cosmetic pack manufacturing with using its functional property Download PDF

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KR20040071087A
KR20040071087A KR1020040046335A KR20040046335A KR20040071087A KR 20040071087 A KR20040071087 A KR 20040071087A KR 1020040046335 A KR1020040046335 A KR 1020040046335A KR 20040046335 A KR20040046335 A KR 20040046335A KR 20040071087 A KR20040071087 A KR 20040071087A
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vermiculite
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cosmetic pack
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김만수
김완태
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김만수
김완태
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0216—Solid or semisolid forms
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y5/00—Nanobiotechnology or nanomedicine, e.g. protein engineering or drug delivery
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41—Particular ingredients further characterized by their size
    • A61K2800/413—Nanosized, i.e. having sizes below 100 nm

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  • General Health & Medical Sciences (AREA)
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  • General Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Biophysics (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

PURPOSE: A method of making a functional cosmetic pack using nano-sized vermiculite obtained by micronizing vermiculite with a ball mill at high temperature is provided. The cosmetic pack imparts nutrients, moisturizing and skin whitening effect on the skin and has improved adhesion to the skin and washability during washing while being eliminated in the problems of storage. CONSTITUTION: Vermiculite having a specific gravity of about 0.2 to 0.4g/cc is aged 3.5 times by weight with pure water and then micronized with a ball mill for 360hr to give a vermiculite solution with a particle size of 200 to 300nm, which is heated with hot air at 450deg.C and micronized to give a particle with a size of 0.05 to 0.1nm. The nano-sized vermiculite is mixed with collagen peptide, retinol, titanium dioxide and aroma such as lemon, peppermint, rosemary or the like.

Description

나노 입자의 Vermiculite의 제조와 이의 특성을 이용한 기능성 미용 팩의 제조방법{Nano-sized particle Vermiculite manufacturing, and thereof its cosmetic pack manufacturing with using its functional property}Nano-sized particle Vermiculite manufacturing, and approximately its cosmetic pack manufacturing with using its functional property

일반적으로 팩의 종류로는 고분자 화합물을 이용한 팩과, 황토나 뻘, 벤토나이트 등을 함유한 팩이 있으며, 가정에서 쉽게 제조 사용되는 곡물 팩과 계란팩, 그리고 부직포 등을 이용한 마스크 팩 등이 주로 사용되어지고 있는데, 이 matrix 등은 모두가 수분을 다량 함유하여 피부에 보습효과를 주고 이로 인하여 피부를 부드럽게 하는 효과를 준다.In general, pack types include packs made of polymer compounds and packs containing ocher, clay, bentonite, and the like. Grain packs, egg packs, and mask packs made of non-woven fabrics are easily used at home. This matrix, etc., all contain a large amount of water to moisturize the skin and thereby softens the skin.

그 중 몇몇 종류의 팩이 제품화되어 시판되고 있으며, 그중 최근에 인기를 얻고 있는 제품으로 머드 팩과 황토 팩, 벤토나이트를 이용한 팩 등이 있다. 이들 제품은 광물의 일반적인 특징으로 다량의 미생물이 존재하는 재료들(황토, 뻘, 고령토)이고, 피부와의 흡착력이 떨어져 피부에 충분한 보습 효과를 주지 못할 뿐 아니라, 건조후에 피부에서 이탈되어 호흡 시 체내로 흡입될 우려가 아주 많아 심리적으로 좋은 느낌을 주지 못하고 위생적인 면에서도 부정적이었다.Several kinds of packs are commercialized and commercially available. Among them, mud packs, ocher packs, and bentonite packs are recently gaining popularity. These products are a general feature of minerals and are materials that contain a large amount of microorganisms (ocher, clay, kaolin), and they do not give sufficient moisture to the skin due to their poor adsorption to the skin. There was a high risk of inhalation into the body did not feel good psychologically and hygiene was negative.

본 발명은 나노 입자의 Vermiculite 를 이용해 미용 팩의 새로운 matrix 를 개발함과 동시에 보습 효과뿐만 아니라 미백, 주름제거, 자외선 차단 등 기능성을 부가함으로써 개개인이 가지는 피부에 대한 불만을 해소에 일조를 하고자한다.The present invention aims to solve the individual's dissatisfaction with the skin by adding functionalities such as whitening, wrinkle removal and UV protection as well as moisturizing effect while developing a new matrix of cosmetic packs using Vermiculite of nanoparticles.

뿐만 아니라 본 나노 입자의 Vermiculite 는 천연 광물을 900℃ 이상의 고온에서 멸균, 박리, 팽창시켜 다공성 화합물로 만들었고, 이를 최신 분쇄 방법을 이용하여 나노화(200∼300nm)하였다.In addition, Vermiculite of the nanoparticles were sterilized, peeled, and expanded natural minerals at a high temperature of 900 ° C. or higher to form a porous compound, which was then nanoscaled (200 to 300 nm) using the latest grinding method.

순수한 물을 첨가한 상태에서 알루미나 ball-mill 을 이용해 15 일간 분쇄 후 숙성과정을 거친 후, 다시 고온 열풍건조로 Vermiculite 가 가지는 특유의 Gold 펄을 유지 시켰으며, 미세한 입자의 분진을 없애기 위하여 다시금 입자를 재 조합하여 0.1mm의 입상을 만들어 내었다.After pulverizing with alumina ball-mill for 15 days with pure water, the aging process was carried out, and then the hot gold was used to maintain Vermiculite's unique gold pearl. The particles were again removed to remove fine particles. Recombination gave a granule of 0.1 mm.

본 발명은 천연 Vermiculite 함유된 광물질 중 원적외선을 방사하는 실리카와 마그네슘 등의 기능성 원소의 특성을 이용하고, 박리 팽창과정에 만들어진 다공질 속에 기능성 화장품 재료를 결합시켜 기능성 화장품으로 인정을 받고자 한다.The present invention is intended to be recognized as a functional cosmetic by using the properties of functional elements such as silica and magnesium that emit far-infrared rays among natural Vermiculite-containing minerals, and by combining the functional cosmetic material in the porous made during the peeling expansion process.

또한 특유의 황금 빛 광택을 내는 표면을 만들어내어 신비로움과, 피부와의 흡착력을 증진시킨 신 개념의 팩을 만드는 의도가 있는 발명이다.It is also an invention with the intention of creating a pack of new concepts that create a unique golden luster surface and promote mystery and adsorption to the skin.

본 발명은 천연 Vermiculite 가 가지는 편상 구조로 인하여 분쇄의 어려움을 극복하기 위하여, 900℃이상에서 순간 박리 팽창시켜 미분화를 성공하였고, 천연 콜라겐을 이용하여 다공질 속의 수분과 콜라겐의 치환을 유도하였으며 이로 인하여 피부와의 흡착력을 배가시켜, 분진이 발생하지 않으며, 세안 시 물에 잘 씻어지는특성을 본 발명에서 이루었다.In order to overcome the difficulty of crushing due to the flaky structure of natural Vermiculite, it succeeded in micronization by instantaneous swelling and expansion at 900 ℃ or higher, and induced the substitution of water and collagen in the porous by using natural collagen. By doubling the adsorption power of the, dust does not occur, the characteristics of washing in the water at the time of washing was achieved in the present invention.

뿐만 아니라 건조 후 피부에 부착된 Vermiculite 의 색상은 금빛을 내는데 보는 이의 신비로움을 만족시켜준다.In addition, the color of Vermiculite adheres to the skin after drying to satisfy the mystery of the viewer.

본 발명의 목적은 Vermiculite의 초 미분화를 통하여 NT 기술을 인정 받고 단위 면적을 최대한 증가시켜,.Vermiculite가 가지고 있는 pore 속에 일반적으로 물에 대한 용해도나 분산력이 떨어지는 분자량이 큰 기능성 물질을 다량 함유시켜 유수한 기능성을 가지는 미용화장품 제조에 그 목적을 둔다.The object of the present invention is to recognize NT technology through ultra-differentiation of Vermiculite and to increase the unit area as much as possible.In general, the pores of Vermiculite contain a large amount of functional material having a high molecular weight, which has low solubility or dispersibility in water. Its purpose is to manufacture cosmetics with functionality.

원재료 수집에서 첫째 천연상태의 Vermiculite 를 채광하여 불순물을 분리하고, 이를 사용되어질 수 있는 입자를 따로 구분한다.In the raw material collection, the first natural vermiculite is mined to separate impurities and the particles that can be used are separated.

SiO2, Al2O2, Fe2O3, MgO, CaO, TiO2, Na2O 등이 주성분인 Vermiculite 는 결정격자 층 사이에 3 가지의 결정 수를 가지고 있어 고온 처리 시 박리팽창하며 이러한 물리적 특성을 이용하여 순수한 Vermiculite를 선별 해 낼 수 있다.Vermiculite, which is composed mainly of SiO 2 , Al 2 O 2 , Fe 2 O 3 , MgO, CaO, TiO 2 , and Na 2 O, has three types of crystals between the crystal lattice layers, resulting in exfoliation and expansion at high temperatures. The properties can be used to sort out pure vermiculite.

이렇게 얻어진 Vermiculite 의 편들은 비중이 0.2∼0.4 g/cc 정도이다. 이러한 낮은 비중과 편상으로 뭉쳐지는 물리적은 특성 때문에 현재까지 첨단 소재로 활용 되어지지 못하였다.The Vermiculite pieces thus obtained have a specific gravity of about 0.2 to 0.4 g / cc. Due to such low specific gravity and physical properties that are combined with flaps, it has not been used as an advanced material to date.

본 발명에서는 이러한 특성을 지니는 건조된 Vermiculite에 무게 비로 3.5배에 달하는 순수와 함께 숙성시키고, 이를 Boll mill 을 이용하여 360 시간 미분하여, 200∼300nm의 입도를 가지는 Vermiculite 용액을 제조에 성공하였다.In the present invention, the dried Vermiculite having this characteristic was aged with 3.5 times the pure water by weight ratio, and finely differentiated for 360 hours using a Boll mill, a successful Vermiculite solution having a particle size of 200 ~ 300nm.

제조된 Vermiculite 용액의 특성으로는 미분된 입자와 고유 편상의 펄이 혼합된 상태에서 보여주는 아름다운 금빛 펄을 확인 할 수 있고, 이 용액을 450℃에서 열풍건조하여 고운 powder 를 만드는데 성공 하였다.The characteristics of the prepared Vermiculite solution showed a beautiful golden pearl showing finely mixed particles and intrinsic flaky pearls. The solution was successfully dried to hot air at 450 ℃ to make fine powder.

생성된 powder 를 다시 재가공하여 0.05∼0.1nm 의 입자를 만들었고, 이를 화장품 원재료로 사용 하였다.The produced powder was reprocessed to produce particles of 0.05 to 0.1 nm, which were used as raw materials for cosmetics.

만들어진 matrix 와 함께 화장품의 특성을 살려줄 첨가 재료들은 시중에 유통되는 안전성이 입증된 천연 재료들로만 사용하였고, 특히 콜라겐의 경우 동물성 콜라겐을 사용하지 않고 해양성 콜라겐 펩타이드를 공급 받아 사용하였다.In addition to the matrix, the additives that make use of the cosmetics' properties are used only with natural materials that have been proven to be safe in the market. Especially, collagen was supplied with marine collagen peptides without using animal collagen.

레티놀 성분은 일반 화장품 재료를 사용치 않고 순도가 높은 Sigma-Aldrich 사의 99.999％의 함량을 지지는 시약을 사용 약 15 (wt％) 함량으로 첨가하였고, 이들의 기능성 물질들은 각각 따로 사용되었으며 새로운 Vermiculite Powedr Matrix(VPM)에 골고루 분산 바인딩 되었다.The retinol component was added at a content of about 15 (wt%) using a reagent that supports 99.999% content of high-purity Sigma-Aldrich, without using general cosmetic ingredients, and their functional substances were used separately and the new Vermiculite Powedr Dispersion was bound evenly to the matrix (VPM).

미백기능성 재료인 이산화 티탄(TiO2)의 경우는 신 Vermiculite Powder Matrix 속에 1.19％ 이상 함유되어 있음을 확인 하여 따로 첨가 하지 않았다.Titanium dioxide (TiO 2 ), a whitening functional material, was found to be contained in the new Vermiculite Powder Matrix at 1.19% or more, and was not added separately.

신경 안정화 기능을 가지는 aroma 는 천연물에서 추출한 레몬향과, 페파민트, 로즈마리 향을 주로 사용하였다.Aroma with nerve stabilizing function mainly uses lemon, peppermint and rosemary flavors extracted from natural products.

이렇게 만들어진 가칭 콜라겐 골드 팩과, 레티놀 골드 팩은 기존의 황토 팩이나, 머드 팩, 벤토나이트 팩의 단점인 분진 발생과 뻘이나 흙이라는 고정 관념을 완전히 탈피시킨 최첨단 Wall-being 팩으로 손색이 없었다.The tentative collagen gold pack and the retinol gold pack are the most advanced wall-being packs that completely break the stereotypes such as dust generation and soil or dirt, which are disadvantages of conventional ocher packs, mud packs and bentonite packs.

상기 기술한 내용의 첨가제 및 제품의 최적 함량 비는 다음 table 에 나타내었다.The optimum content ratios of the additives and products described above are shown in the following table.

그간 소비자들이 스스로 제조하거나 자가 처방으로 사용하던 것을 하나의 제품으로 제조하여 우수한 품질로 배합되고 피부에 과민 반응이 없는 함량으로 제조하여 공급하므로 사용이 간편하고 용이하다.In the meantime, it is easy and easy to use because it is manufactured by one product that is manufactured by oneself or used by self-preparation in one product, and is formulated and supplied in an excellent quality and does not have hypersensitivity to skin.

또한 제품에 필요한 재료를 모두 정량 배합하여 제조하여, 보관상의 문제점이나 사용 시 손수 물과 혼합 사용하지 않아도 될 수 있도록 제조되어 미관상이나 사용상에 어려움이 없다.In addition, it is manufactured so that all materials necessary for the product are formulated and formulated, so that it is not necessary to mix and use with hand water during storage problems or use, so there is no difficulty in appearance or use.

Claims (1)

첨단 화장품 소재로 인식되지 못하던 Vermiculite를 최첨단 분쇄 기술을 이용하여 얻은 Vermiculite Powder Matrix를 사용하여 여기에 기능성 화장품 소재를 첨가하여, 기능성이 뛰어난 화장용 팩을 개발하였고, 이들의 함량은 table 1과 같고 이를 배합하여 gel타입의 용액으로 만들었다. 제조된 gel타입의 용액으로 미용을 위해 안면 부위 및 신체 특정부위에 도포용으로 사용하는 것을 특징으로 하는나노 입자의 Vermicu-lite의 제조와 이의 특성을 이용한 기능성 미용 팩의 제조방법. Vermiculite, which was not recognized as a high-tech cosmetic material, was added to the functional cosmetic material by using Vermiculite Powder Matrix obtained through the use of state-of-the-art grinding technology. The mixture was made into a gel type solution. Preparation of a Vermicu-lite nanoparticles, characterized in that it is used for application to the facial and body specific parts for the cosmetic gel-type solution prepared by the method and a method of manufacturing a functional cosmetic pack using its properties.
KR1020040046335A 2004-06-21 2004-06-21 Nano-sized particle Vermiculite manufacturing, and thereof its cosmetic pack manufacturing with using its functional property KR20040071087A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116035957A (en) * 2023-02-16 2023-05-02 塔里木大学 Method for preparing clean moisturizing facial mask by using vermiculite and camel hump as raw materials

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003066016A1 (en) * 2002-02-08 2003-08-14 The Procter & Gamble Company Rinse-off skin conditioning compositions
KR20040022420A (en) * 2001-04-18 2004-03-12 킴벌리-클라크 월드와이드, 인크. Skin Cleansing Composition Incorporating Anionic Particles
KR20040027600A (en) * 2004-02-13 2004-04-01 김만수 Vermiculite pack of which its high heating and fine processing powder with some melted materials in the ionized cleaning solution, thereof its manufacturing method.

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20040022420A (en) * 2001-04-18 2004-03-12 킴벌리-클라크 월드와이드, 인크. Skin Cleansing Composition Incorporating Anionic Particles
WO2003066016A1 (en) * 2002-02-08 2003-08-14 The Procter & Gamble Company Rinse-off skin conditioning compositions
KR20040027600A (en) * 2004-02-13 2004-04-01 김만수 Vermiculite pack of which its high heating and fine processing powder with some melted materials in the ionized cleaning solution, thereof its manufacturing method.

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116035957A (en) * 2023-02-16 2023-05-02 塔里木大学 Method for preparing clean moisturizing facial mask by using vermiculite and camel hump as raw materials

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