KR20020085937A - Gibberrelic acid paste manufacturing method - Google Patents

Gibberrelic acid paste manufacturing method Download PDF

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KR20020085937A
KR20020085937A KR1020010025469A KR20010025469A KR20020085937A KR 20020085937 A KR20020085937 A KR 20020085937A KR 1020010025469 A KR1020010025469 A KR 1020010025469A KR 20010025469 A KR20010025469 A KR 20010025469A KR 20020085937 A KR20020085937 A KR 20020085937A
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acid
lanolin
ethyl alcohol
mixture
coating agent
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KR1020010025469A
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Korean (ko)
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김인수
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주식회사천우물산
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Publication of KR20020085937A publication Critical patent/KR20020085937A/en

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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N45/00Biocides, pest repellants or attractants, or plant growth regulators, containing compounds having three or more carbocyclic rings condensed among themselves, at least one ring not being a six-membered ring
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A01N25/04Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/30Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Environmental Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Zoology (AREA)
  • Plant Pathology (AREA)
  • Toxicology (AREA)
  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Fats And Perfumes (AREA)
  • Cosmetics (AREA)

Abstract

PURPOSE: A method for producing a gibberellin acid coating agent is provided, which is coated on the stalk of fruits to shorten fruit maturation period and to increase of fruit size, thereby harvesting fruits early. CONSTITUTION: The method for producing a gibberellin acid coating agent comprises mixing 3.59g of gibberellin acid 3 with 10g of ethyl alcohol; adding 5g of a surfactant into the mixture; adding 81.44g of lanolin as a weight increasing agent and a resin into the mixture; and stirring the mixture at 50 to 60 deg. C under vacuum condition to extract ethyl alcohol. Alternatively, the gibberellin acid coating agent is produced by powdering 3.56g of gibberellin acid 3 with an air mill; adding 96.44g of lanolin into the powdered gibberellin acid 3; and high speed rotating the mixture using a stirrer.

Description

지베레린 에시드 도포제의 제조방법{Gibberrelic acid paste manufacturing method}Gibberrelic acid paste manufacturing method {Gibberrelic acid paste manufacturing method}

본 발명은 과실(배)의 숙기 및 비대를 촉진시켜 조기에 수확하기 위하여 과실의 과경부위에 도포하는 지베레린 도포제의 제조방법에 관한 것으로서, 이를 좀 더 구체적으로 설명하면, 과실(배)의 숙기 및 비대를 촉진시키는 지베레린 에시드 3에 증량제 및 담체인 라놀린을 균일하게 분포시키기 위한 것으로서 용매로 에틸알콜을 사용하여 용해시킨 후 이 용액에서 알콜성분을 추출하는 방법과 순수교반기를 이용하여 지베레린 에시드를 교반시키는 방법으로 제조하는 것이다.The present invention relates to a method for producing a gibberellin coating agent applied to the fruit area of the fruit in order to promote ripening and enlargement of the fruit (pear) early harvesting, more specifically, the ripening of the fruit (pear) And uniform distribution of lanolin, an extender and a carrier, in gibbererin acid 3, which promotes hypertrophy, by dissolving ethyl alcohol as a solvent, and then extracting an alcohol component from the solution and using a pure stirrer. It is prepared by the method of stirring lean acid.

일반적으로 과실(배)의 숙기 및 비대를 촉진하기 위한 성장촉진제로서 지베레린 에시드가 널리 사용되고 있으나 이의 제품은 전량 외국에서 수입하여 과수농가에 보급하고 있어 외화낭비를 초래하고 있어 이의 국산화가 시급히 요구되고 있는 실정에 있으나 현재까지 이를 제조할 수 있는 기술은 전혀 제안된 바 없는 것이다.Generally, gibberelin acid is widely used as a growth accelerator to promote ripening and enlargement of fruits (pears), but all of its products are imported from foreign countries and distributed to fruit farms, which causes waste of foreign currency. However, there is no technology that can be manufactured so far has been proposed.

본 발명자는 상기의 문제점을 해결하기 위하여 연구를 거듭한 결과, 본 발명의 제조방법을 제안하기에 이른 것으로서, 본 발명의 목적은 간단한 공정으로 지베레린 에시드가 라놀린에 균일하게 분포되도록 하는 기술을 제안하여 지베레린 도포제의 국산화를 가능하게 하는데 그 목적이 있는 것이다.As a result of repeated studies to solve the above problems, the present inventors have come to propose a manufacturing method of the present invention, and an object of the present invention is to provide a technique for uniformly distributing gibberelin acid to lanolin in a simple process. The purpose of this study is to enable localization of gibberellin coatings.

상기의 목적을 달성하기 위한 본 발명의 전체적인 제조공정은 2가지 방법이 있다.There are two methods for the overall manufacturing process of the present invention for achieving the above object.

그 하나의 제조방법으로서 중량비로 3.59g의 지베레린 에시드 3에 에틸알콜 10g를 혼합하여 용해시키는 용해공정과 ; 상기 용해공정에 의해 용해된 원재에 유화제인 계면활성제를 5g첨가하여 유화시킨 후 증량제 및 담체인 액상의 라놀린을 81.44g를 첨가하여 섭씨 50∼60℃에서 진공교반시켜 에틸알콜을 추출하는 교반공정으로 제조하는 것이다.As one manufacturing method, the dissolution process of mixing and dissolving 10 g of ethyl alcohol in 3.59 g of gibberellic acid 3 by weight ratio; By adding 5g of the surfactant as an emulsifier to the raw material dissolved by the dissolution step to emulsify, 81.44g of liquid lanolin as an extender and a carrier are added, followed by vacuum stirring at 50-60 ° C to extract ethyl alcohol. To manufacture.

또 다른 제조방법으로서 중량비로 3.56g의 지베레린 에시드 3을 에어밀로 분말화하는 분쇄공정과 ; 분쇄된 지베레린 에이드 3에 라놀린 96.44g을 혼합하여 순수교반기를 이용하여 고속으로 회전시켜 각 성분을 혼합하는 교반공정을 제조하는 것이다.Another manufacturing method is a pulverizing step of powdering 3.56 g of gibberelin acid 3 by weight with an air mill; 96.44 g of lanolin is mixed with pulverized gibberelin aldehyde 3 and rotated at high speed using a pure stirrer to prepare a stirring process for mixing each component.

이하, 본 발명의 일실시에 및 이로부터 얻게 되는 특유의 효과 등에 대하여 상세히 설명하면 하기와 같다.Hereinafter, one embodiment of the present invention and the specific effects obtained therefrom will be described in detail.

<실시예 1><Example 1>

본 발명에 의해 제조되는 지베레린 에이드 도포제에 이용되는 물질은 하기의 (표1)에서와 같이 과실(배)의 숙기 및 비대를 촉진시키는 지베레린 에시드 3과 용매로서 에틸알콜 및 유화역할을 하는 계면활성제 와 증량제 및 담체인 라놀린으로 구성되는 것이다.The material used for the gibberelene ide coating agent prepared according to the present invention is ethyl alcohol and emulsifying role as gibbererin acid 3 and a solvent to promote ripening and hypertrophy of fruit (pear), as shown in Table 1 below. It consists of a surfactant, an extender and a carrier lanolin.

<지베레린 도포제 100g 제조기준><Manufacturing Standards for 100g of Gibberellin Coatings> Material NameMaterial Name Purity of TechPurity of tech Target ContentTarget Content WeightWeight GA3GA3 90%90% 3.2%3.2% 3.56g3.56 g EtOHEtOH -- 10%10% 10g10 g 계면활성제Surfactants -- 5%5% 5g5 g LanolineLanoline -- RestRest 81.44g81.44 g TotalTotal -- 100%100% 100g100 g

상기 지베레린 에이드 도포제에 대한 제조공정은 먼저 중량비로 3.56g의 지베레린 에시드 3에 용매인 에틸알콜을 10g를 첨가하여 혼합시키는 용해공정을 행하게 된다.The manufacturing process for the gibberelin amide coating agent is first subjected to a dissolution step of mixing by adding 10g of ethyl alcohol as a solvent to 3.56g of gibbererel acid 3 in weight ratio.

그리고 상기의 용해공정을 마친 용액은 교반공정을 거치게 되는 것으로서, 이의 교반공정은 계면활성제인 유화제를 5g 첨가하여 유화시킨 상태에서 증량제 및 담체인 라놀린 81.44g를 첨가하여 섭씨 50∼60℃의 온도에서 진공교반을 행하게 된다.And the solution after the dissolution step is to go through a stirring step, the stirring step of the emulsifier was added by adding 5g of emulsifier surfactant in the emulsified state and added 81.44g lanolin as a carrier and carrier at a temperature of 50 ~ 60 ℃ Vacuum stirring is performed.

상기 진공교반을 1시간 정도 진행하는 과정에서 상기 용매로 이용한 알콜이 전량 추출되면 별도로 마련한 튜브에 주입하여 완제품을 제조하게 되는 것이다.If the entire amount of alcohol used as the solvent is extracted in the course of the vacuum stirring for about 1 hour to prepare a finished product by injecting into a separately prepared tube.

상기의 방법에 의하여 용매로 사용한 알콜은 주성분인 지베레린 에시드 3을 용해시키는 역할을 하게 되는 것이며, 또 진공교반의 시간을 1시간 정도로 설정하여 에틸알콜을 추출하는 이유는 에틸알콜이 지베레린 에시드 3을 천천히 분해시키는 성질이 있기 때문이다.The alcohol used as a solvent by the above method serves to dissolve Gibberelin Acid 3, which is a main component, and the reason for extracting ethyl alcohol by setting the vacuum stirring time to about 1 hour is that ethyl alcohol is gibbererin This is because the acid 3 is slowly decomposed.

그리고 용해공정이 완료된 후 유화제를 사용하는 이유는 에틸알콜과 라놀린이 잘 섞이지 않기 때문에 이를 사용하여 라놀린과 에틸알콜을 유화시킴으로써 에틸알콜에 녹아있는 주성분인 지베레린에시드 3이 잘 섞이도록 하기 위한 것이다.The reason why the emulsifier is used after the dissolution process is completed is that the ethyl alcohol and lanolin are not mixed well, so that the emulsifier is used to emulsify lanolin and ethyl alcohol so that the gibbererin acid 3, the main component dissolved in ethyl alcohol, is mixed well. .

<실시예 2><Example 2>

본 발명의 또 다른 실시예로서 상기 실시예에서 사용한 유화제를 사용하지 않고 순수교반기(homogenizer)로 교반하는 방법으로서, 이의 제조방법을 살펴보면 본 실시예에 사용되는 물질은 하기의 (표2)에서와 같이 중량비로 지베레린 에시드 3을 3.56g 및 액상의 라놀린 96.44g으로 구성되는 것이다.As another embodiment of the present invention as a method of stirring with a pure agitator (homogenizer) without using the emulsifier used in the above embodiment, looking at the production method thereof is used in the following Example 2 Likewise, it is composed of 3.56g of gibberelin acid 3 and 96.44g of liquid lanolin in weight ratio.

<지베레린 도포제 100g 제조기준><Manufacturing Standards for 100g of Gibberellin Coatings> Material NameMaterial Name Purity of TechPurity of tech Target ContentTarget Content WeightWeight GA3GA3 90%90% 3.2%3.2% 3.56g3.56 g LanolineLanoline -- RestRest 96.44g96.44 g TotalTotal -- 100%100% 100g100 g

상기의 물질 중 지베레린 에시드 3을 에어밀(Air Mill)로 분말화하는 분쇄공정을 행하게 된다.Among the above materials, a pulverization process is performed to powder Gibberelin acid 3 into an air mill.

그리고 분쇄공정이 완료된 원제에 액체상태의 라놀린 96.44g을 혼합한 후 라놀린과 원제인 지베레린 에시드 3이 균일하게 분산 될 수 있도록 하기 위하여 순수교반기를 이용하여 30분 정도 교반공정을 거치게 되는 것이다.Then, 96.44 g of lanolin in liquid form is mixed with the raw material after the pulverization process is completed, and agitation process is performed for 30 minutes using a pure stirrer to uniformly disperse lanolin and the original agent, gibbererlic acid 3.

상기 교반공정을 거친 용액은 별도로 마련된 용기인 튜브에 주입하여 제품을 완성하게 되는 것으로서 상기의 분쇄공정에 있어서, 에어밀로 분쇄하는 이유는 원제의 입도가 균일하지 못하여 제품상태에서 주성분의 분산이 잘 되지 않기 때문에 이를 방지하기 위함이고, 또 순수교반기로 교반공정을 행하는 이유는 증량제 및 담체인 라놀린에 원제인 지베레인 에시드 3을 골고루 분산시키기 위한 것이다.The solution after the stirring process is injected into a tube, which is a separately prepared container, to complete the product. In the above crushing process, the reason for pulverizing with an air mill is that the particle size of the raw material is not uniform, so that the main component is not well dispersed in the product state. This is to prevent this, and the reason for carrying out the stirring step with a pure stirrer is to evenly disperse Gibberane Acid 3, which is the original agent, in the lanolin as the extender and carrier.

상기와 같이 본 발명은 에틸알콜을 사용하거나 순수교반기를 이용하여 원제인 지베레린 에시드 3을 증량제에 균일하게 분포시켜서 제조하므로서 과실(배)의 비대 및 숙기를 촉진시켜 배 생산량 증대와 숙기 촉진으로 당도를 증가시킬 수 있다.As described above, the present invention is prepared by uniformly distributing the original agent, gibberelin acid 3, using an ethyl alcohol or a pure stirrer in the extender, thereby promoting the enlargement and ripening of the fruit (pear) and increasing the pear production and promoting ripening. It can increase the sugar content.

Claims (2)

중량비로 3.59g의 지베레린 에시드 3에 에틸알콜 10g를 혼합하여 용해시키는 용해공정과 ; 상기 용해공정에 의해 용해된 원재에 유화제인 계면활성제를 5g첨가하여 유화시킨 후 증량제 및 담체인 액상의 라놀린을 81.44g를 첨가하여 섭씨 50∼60℃에서 진공교반시켜 에틸알콜을 추출하는 교반공정으로 제조하는 것을 특징으로 하는 지베레린 도포제의 제조방법.A dissolution step of mixing and dissolving 10 g of ethyl alcohol in 3.59 g of gibberelin acid 3 by weight ratio; By adding 5g of the surfactant as an emulsifier to the raw material dissolved by the dissolution step to emulsify, 81.44g of liquid lanolin as an extender and a carrier are added, followed by vacuum stirring at 50-60 ° C to extract ethyl alcohol. Method for producing a gibberellin coating agent, characterized in that the manufacturing. 중량비로 3.56g의 지베레린 에시드 3을 에어밀로 분말화하는 분쇄공정과 ; 분쇄된 지베레린 에이드 3에 라놀린 96.44g을 혼합하여 순수교반기를 이용하여 고속으로 회전시켜 각 성분을 혼합하는 교반공정을 제조하는 것을 특징으로 하는 지베레린 도포제의 제조방법.A pulverizing step of powdering 3.56 g of gibberelin acid 3 by weight with an air mill; A method for producing a gibberellin coating agent, characterized in that a mixture of 96.44 g of lanolin is mixed with pulverized gibberelin amide 3 and rotated at a high speed using a pure stirrer to mix each component.
KR1020010025469A 2001-05-10 2001-05-10 Gibberrelic acid paste manufacturing method KR20020085937A (en)

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KR100812114B1 (en) * 2007-03-09 2008-03-12 윤채혁 Gibberelin agents containing plant-derived carrier and a method for preparation thereof

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