JPS57168147A - Analysis of ratio of optical isomer - Google Patents
Analysis of ratio of optical isomerInfo
- Publication number
- JPS57168147A JPS57168147A JP5405681A JP5405681A JPS57168147A JP S57168147 A JPS57168147 A JP S57168147A JP 5405681 A JP5405681 A JP 5405681A JP 5405681 A JP5405681 A JP 5405681A JP S57168147 A JPS57168147 A JP S57168147A
- Authority
- JP
- Japan
- Prior art keywords
- compound
- ratio
- lewis base
- functional group
- optical isomer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R33/00—Arrangements or instruments for measuring magnetic variables
- G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
- G01R33/44—Arrangements or instruments for measuring magnetic variables involving magnetic resonance using nuclear magnetic resonance [NMR]
- G01R33/46—NMR spectroscopy
Landscapes
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- High Energy & Nuclear Physics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE:To measure accurately and simply with high resolution the ratio of an optical isomer in a compound that contains a functional group of Lewis base by nuclear magnetic resonance method with the addition of a compound that has other functional group of Lewis base under the existence of a specific optical activity shift reagent. CONSTITUTION:When the ratio of an optical isomer of a compound that has functional groups of Lewis base such as OH, SH, NH2, CN, etc. is analysed by nuclear magnetic resonance method, using a shift reagent of optical activity as represented by the formula, a compound of alcohol, amine or others that has a functional group of Lewis base which is different from said object compound to be measured as the third component. With this set-up the ratio of optical isomers such as alpha-cyano-3-pheoxybenzil alcohol, etc. which are not sufficiently separable or inseparable can be analysed simply with high resolution.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP5405681A JPS57168147A (en) | 1981-04-09 | 1981-04-09 | Analysis of ratio of optical isomer |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP5405681A JPS57168147A (en) | 1981-04-09 | 1981-04-09 | Analysis of ratio of optical isomer |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS57168147A true JPS57168147A (en) | 1982-10-16 |
Family
ID=12959951
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP5405681A Pending JPS57168147A (en) | 1981-04-09 | 1981-04-09 | Analysis of ratio of optical isomer |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS57168147A (en) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9855038B2 (en) | 2005-07-26 | 2018-01-02 | Ethicon Llc | Surgical stapling and cutting device |
US9934920B2 (en) | 2006-05-19 | 2018-04-03 | Ethicon Endo-Surgery, Inc. | Force switch |
US10314592B2 (en) | 2006-05-19 | 2019-06-11 | Ethicon Llc | Electrically self-powered surgical instrument with cryptographic identification of interchangeable part |
US10314583B2 (en) | 2005-07-26 | 2019-06-11 | Ethicon Llc | Electrically self-powered surgical instrument with manual release |
US10675022B2 (en) | 2006-05-19 | 2020-06-09 | Ethicon Llc | Electrical surgical instrument with optimal tissue compression |
-
1981
- 1981-04-09 JP JP5405681A patent/JPS57168147A/en active Pending
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9855038B2 (en) | 2005-07-26 | 2018-01-02 | Ethicon Llc | Surgical stapling and cutting device |
US10314583B2 (en) | 2005-07-26 | 2019-06-11 | Ethicon Llc | Electrically self-powered surgical instrument with manual release |
US11172930B2 (en) | 2005-07-26 | 2021-11-16 | Cilag Gmbh International | Electrically self-powered surgical instrument with manual release |
US11234695B2 (en) | 2005-07-26 | 2022-02-01 | Cilag Gmbh International | Surgical stapling and cutting device |
US9934920B2 (en) | 2006-05-19 | 2018-04-03 | Ethicon Endo-Surgery, Inc. | Force switch |
US10217582B2 (en) | 2006-05-19 | 2019-02-26 | Ethicon Endo-Surgery, Inc. | Force switch |
US10314592B2 (en) | 2006-05-19 | 2019-06-11 | Ethicon Llc | Electrically self-powered surgical instrument with cryptographic identification of interchangeable part |
US10586669B2 (en) | 2006-05-19 | 2020-03-10 | Ethicon-Endo Surgery, Inc. | Force switch |
US10675022B2 (en) | 2006-05-19 | 2020-06-09 | Ethicon Llc | Electrical surgical instrument with optimal tissue compression |
US11172931B2 (en) | 2006-05-19 | 2021-11-16 | Cilag Gmbh International | Electrically self-powered surgical instrument with cryptographic identification of interchangeable part |
US11183349B2 (en) | 2006-05-19 | 2021-11-23 | Ethicon Endo-Surgery, Inc | Force switch |
US11759203B2 (en) | 2006-05-19 | 2023-09-19 | Cilag Gmbh International | Electrical surgical instrument with minimum closure distance for staple firing control |
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