JPS55128591A - Manufacture of phosphorothiolate - Google Patents
Manufacture of phosphorothiolateInfo
- Publication number
- JPS55128591A JPS55128591A JP3619479A JP3619479A JPS55128591A JP S55128591 A JPS55128591 A JP S55128591A JP 3619479 A JP3619479 A JP 3619479A JP 3619479 A JP3619479 A JP 3619479A JP S55128591 A JPS55128591 A JP S55128591A
- Authority
- JP
- Japan
- Prior art keywords
- group
- phosphorothiolates
- substituted
- straight
- chain
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
PURPOSE: To obtain phosphorothiolates as agrochemicals simply and in high yields, by electrolytically oxidizing a mixture of a disubstituted disulfide and disubstituted phosphite in the presence of a halide as a catalyst in an organic solvent.
CONSTITUTION: Phosphorothiolates of the formula III can be quantitatively obtained by electrolytically oxidizing a mixture of compounds of the formulae I and II [R is a 1W5C straight-chain or branched alkyl group, a 5W6C alicyclic group, (substituted) phenyl group, or benzyl group, or a 1W5C alkoxycarbonylalkyl group, and R' is 1W5C straight-chain or branched alkyl group or (substituted) phenyl group] in the presence of an inorganic or organic halide, e.g., chloride, bromide, iodide, etc., together with a supporting salt, e.g., amine, ammonium salt, perchlorate, etc., in an organic solvent, e.g., nitrile such as acetonitrile, at 0W100°C, preferably 10W50°C, using an electrode of platinum, stainless steel, carbon, etc.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP3619479A JPS55128591A (en) | 1979-03-29 | 1979-03-29 | Manufacture of phosphorothiolate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP3619479A JPS55128591A (en) | 1979-03-29 | 1979-03-29 | Manufacture of phosphorothiolate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS55128591A true JPS55128591A (en) | 1980-10-04 |
| JPS5643387B2 JPS5643387B2 (en) | 1981-10-12 |
Family
ID=12462906
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP3619479A Granted JPS55128591A (en) | 1979-03-29 | 1979-03-29 | Manufacture of phosphorothiolate |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS55128591A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022158702A1 (en) * | 2021-01-21 | 2022-07-28 | 삼성에스디아이 주식회사 | Additive, and lithium secondary battery electrolyte and lithium battery which comprise same |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP4290412A3 (en) | 2018-09-05 | 2024-01-03 | Sartorius Stedim Data Analytics AB | Computer-implemented method, computer program product and system for data analysis |
-
1979
- 1979-03-29 JP JP3619479A patent/JPS55128591A/en active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022158702A1 (en) * | 2021-01-21 | 2022-07-28 | 삼성에스디아이 주식회사 | Additive, and lithium secondary battery electrolyte and lithium battery which comprise same |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5643387B2 (en) | 1981-10-12 |
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