JPH07178323A - Method for backwashing ceramic membrane - Google Patents

Method for backwashing ceramic membrane

Info

Publication number
JPH07178323A
JPH07178323A JP32565393A JP32565393A JPH07178323A JP H07178323 A JPH07178323 A JP H07178323A JP 32565393 A JP32565393 A JP 32565393A JP 32565393 A JP32565393 A JP 32565393A JP H07178323 A JPH07178323 A JP H07178323A
Authority
JP
Japan
Prior art keywords
raw water
pressure
membrane
water side
valve
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP32565393A
Other languages
Japanese (ja)
Other versions
JP2763262B2 (en
Inventor
Hitoshi Yonekawa
均 米川
Tokuji Kubo
篤司 久保
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NGK Insulators Ltd
Original Assignee
NGK Insulators Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NGK Insulators Ltd filed Critical NGK Insulators Ltd
Priority to JP5325653A priority Critical patent/JP2763262B2/en
Publication of JPH07178323A publication Critical patent/JPH07178323A/en
Application granted granted Critical
Publication of JP2763262B2 publication Critical patent/JP2763262B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Abstract

PURPOSE:To provide a sufficient effective membrane differential pressure and to effectively backwash a ceramic membrane in a short time by closing the membrane on the raw water side, exerting a high pressure from the filtration side to equalize the pressures on the raw water side and filtration side of the membrane and then releasing the pressure on the raw water side at a time. CONSTITUTION:When backwashing is needed, a raw water feed valve 3, a waste backwashing water valve 9, etc., are closed to close the raw water side. High-pressure air is added to a pressure tank 5 under these conditions by opening a high-pressure air feed valve 6, hence a pressure is exerted on the filtration side of a ceramic membrane 2, the pressure is transmitted to the closed raw water side, and the pressures on the raw water side and filtration side of the membrane 2 are equalized. While the valve 6 is opened and the valve 9 is rapidly opened, the pressure on the raw water side is lowered at once, and a large effective membrane differential pressure is generated. Accordingly, the deposits on the membrane surface are successively peeled off the surface, passed through the valve 9 along with the filtered water flowing out of the tank 5 and discharged.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は、セラミック膜の逆洗方
法に関するものであり、特に管状型またはモノリス型の
セラミック膜の逆洗方法に関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for backwashing a ceramic membrane, and more particularly to a method for backwashing a tubular or monolithic ceramic membrane.

【0002】[0002]

【従来の技術】一般に膜モジュールによるろ過を継続す
ると、ろ過によって分離された物質が次第に膜面上に蓄
積し、ろ過抵抗が増大する。このため、ろ過側から原水
側へろ過水を高速度で逆流させ、膜表面の蓄積物を剥離
させる逆洗(逆圧洗浄)を行う必要がある。
2. Description of the Related Art Generally, when filtration by a membrane module is continued, substances separated by filtration gradually accumulate on the membrane surface, and filtration resistance increases. For this reason, it is necessary to carry out backwashing (backpressure washing) in which filtered water is allowed to flow back from the filtration side to the raw water side at a high speed to remove accumulated substances on the membrane surface.

【0003】このような逆洗方法としては、ろ過水を貯
留したタンクから逆洗専用のポンプを用いて膜モジュー
ルにろ過水を透過させるポンプ方式の逆洗方法が一般的
に使用されている。またろ過水の一部を加圧タンクに導
入して圧縮空気等により加圧し、膜モジュールにろ過水
を逆流させるエアー加圧方式も使用されている。
As such a backwashing method, a pump type backwashing method is generally used in which filtered water is passed from a tank storing filtered water to a membrane module by using a dedicated pump for backwashing. In addition, an air pressurization method is also used in which a part of the filtered water is introduced into a pressure tank and pressurized with compressed air or the like to cause the filtered water to flow back to the membrane module.

【0004】[0004]

【発明が解決しようとする課題】しかし図3に示すよう
に、このような従来の逆洗方法では、ろ過水側圧力を高
めるとそれに連れて原水側圧力も高まるため、両者の差
圧である有効膜差圧の値を十分に大きく取ることは困難
であり、従って膜表面の蓄積物を十分に剥離させるため
に比較的長い逆洗時間を必要とするという問題があっ
た。本発明は上記した従来の問題点を解決し、有効膜差
圧を十分に取って短時間で効果的な逆洗を行うことがで
きるセラミック膜の逆洗方法を提供するためになされた
ものである。
However, as shown in FIG. 3, in such a conventional backwashing method, when the pressure on the filtered water side is increased, the pressure on the raw water side is also increased, which is the pressure difference between the two. It is difficult to make the value of the effective transmembrane pressure difference sufficiently large, and therefore, there has been a problem that a relatively long backwash time is required in order to sufficiently release the accumulated material on the membrane surface. The present invention has been made to solve the above-mentioned conventional problems, and to provide a backwashing method for a ceramic membrane capable of performing effective backwashing in a short time while sufficiently taking an effective transmembrane pressure difference. is there.

【0005】[0005]

【課題を解決するための手段】上記の課題を解決するた
めになされた本発明は、管状型またはモノリス型のセラ
ミック膜によるろ過を停止し、原水側のバルブを閉じて
原水側を閉鎖状態としたのち、ろ過側より高圧を加えて
セラミック膜の原水側とろ過側とを等圧に保持し、その
後に原水側のバルブを急速に開き原水側の圧力を一度に
開放して逆洗することを特徴とするものである。また、
原水側の圧力開放時に原水側の上流からリンス水を流
し、剥離物質を系外に放出するようにすると更に好まし
い。
SUMMARY OF THE INVENTION The present invention, which has been made to solve the above problems, stops filtration by a tubular or monolithic ceramic membrane and closes the raw water side valve to close the raw water side. After that, apply high pressure from the filtration side to keep the raw water side and the filtration side of the ceramic membrane at equal pressure, and then quickly open the valve on the raw water side to release the pressure on the raw water side at once and backwash. It is characterized by. Also,
It is further preferable that the rinse water is made to flow from the upstream side of the raw water side when the pressure on the raw water side is released so that the stripping substance is released to the outside of the system.

【0006】[0006]

【作用】本発明のセラミック膜の逆洗方法によれば、原
水側を閉鎖状態としてろ過側より高圧を加え、セラミッ
ク膜の原水側とろ過側とを等圧に保持した後に原水側の
圧力を一度に開放するので、原水側の圧力は高圧状態か
ら一挙に低下し、この瞬間に大きい有効膜差圧が発生す
る。このため、わずかなろ過水によって膜表面の蓄積物
を短時間で十分に剥離させることができる。また、膜表
面に加えられる高圧により膜表面の蓄積物が圧密化され
るので、逆洗により排出された剥離物質の沈降性が良好
となる利点もある。以下に本発明の実施例を示す。
According to the method of backwashing the ceramic membrane of the present invention, the raw water side is closed and a high pressure is applied from the filtration side. Since they are opened at once, the pressure on the raw water side is suddenly reduced from the high pressure state, and a large effective transmembrane pressure is generated at this moment. For this reason, it is possible to sufficiently peel off the accumulated material on the membrane surface in a short time with a small amount of filtered water. Further, since the accumulated material on the surface of the film is consolidated by the high pressure applied to the surface of the film, there is also an advantage that the settling property of the peeling substance discharged by the backwash becomes good. Examples of the present invention will be shown below.

【0007】[0007]

【実施例】図1において1は膜モジュールであり、その
内部にはモノリス型(マルチチャンネル型)のセラミッ
ク膜2が設けられている。実施例のセラミック膜2は細
孔径が0.1 μm のMF膜で、外径30mmの円筒状セラミッ
ク体の内部に直径3mmのチャンネルが37本形成されたも
のである。なおセラミック膜2は管状型のものでもよい
が、平面状のセラミック膜2や有機膜は高圧を加えると
破損するおそれがあるので、本発明の逆洗方法を適用す
ることは好ましくない。
1 is a membrane module in which a monolithic (multi-channel) ceramic membrane 2 is provided. The ceramic membrane 2 of the example is an MF membrane having a pore diameter of 0.1 μm, and 37 channels having a diameter of 3 mm are formed inside a cylindrical ceramic body having an outer diameter of 30 mm. The ceramic membrane 2 may be of a tubular type, but the flat ceramic membrane 2 and the organic membrane may be damaged when high pressure is applied, and therefore it is not preferable to apply the backwashing method of the present invention.

【0008】通常のろ過状態においては、原水は原水側
のバルブである原水供給バルブ3を通じて膜モジュール
1の下部に供給されてモノリス型のセラミック膜2によ
りろ過され、ろ過水はろ過水バルブ4を介して取り出さ
れている。5は膜モジュール1とろ過水バルブ4との間
に設けられた加圧タンクであり、高圧空気供給バルブ6
と放圧用バルブ7とが設けられている。また膜モジュー
ル1の上部にはリンス水供給バルブ8が、下部には原水
側のバルブである逆洗排水バルブ9が設けられている。
In a normal filtration state, raw water is supplied to the lower part of the membrane module 1 through a raw water supply valve 3 which is a valve on the raw water side, and is filtered by a monolithic ceramic membrane 2. The filtered water flows through a filtered water valve 4. Have been taken out through. 5 is a pressure tank provided between the membrane module 1 and the filtered water valve 4, and a high pressure air supply valve 6
And a pressure release valve 7 are provided. Further, a rinse water supply valve 8 is provided in the upper part of the membrane module 1, and a backwash drain valve 9 which is a valve on the raw water side is provided in the lower part.

【0009】ろ過を継続して膜表面の蓄積物が増加し、
逆洗が必要となったときには、次の通り逆洗を行う。ま
ずろ過を停止し、原水側の原水供給バルブ3及び逆洗排
水バルブ9を閉じて原水側を閉鎖状態とする。またろ過
水バルブ4、放圧用バルブ7、リンス水供給バルブ8も
全て閉じる。この状態で高圧空気供給バルブ6を開いて
例えば300kPaの高圧空気を加圧タンク5に加える。その
結果、セラミック膜2のろ過側に圧力が加えられるとと
もに閉鎖状態にある原水側にもこの圧力が伝播し、図2
のグラフに示すようにセラミック膜2の原水側とろ過側
とが等圧に保持される。この保持時間は2〜3秒程度で
十分である。
Continuation of filtration increases the accumulation on the membrane surface,
When backwashing becomes necessary, backwashing is performed as follows. First, the filtration is stopped, and the raw water supply valve 3 and the backwash drain valve 9 on the raw water side are closed to close the raw water side. Further, the filtered water valve 4, the pressure release valve 7, and the rinse water supply valve 8 are all closed. In this state, the high pressure air supply valve 6 is opened and high pressure air of, for example, 300 kPa is added to the pressurized tank 5. As a result, pressure is applied to the filtration side of the ceramic membrane 2, and this pressure also propagates to the raw water side in the closed state.
As shown in the graph, the raw water side and the filtration side of the ceramic membrane 2 are kept at equal pressure. This holding time of about 2 to 3 seconds is sufficient.

【0010】次に高圧空気供給バルブ6を開いたまま、
原水側のバルブである逆洗排水バルブ9を急速に開き、
原水側の圧力を一度に開放する。このとき図2に示すよ
うに原水側の圧力は一挙に低下し、大きい有効膜差圧が
発生する。従って膜表面の蓄積物はほとんど順次に膜表
面から剥離し、加圧タンク5内から流出するろ過水とと
もに逆洗排水バルブ9を通過して排出される。
Next, with the high pressure air supply valve 6 open,
Open the backwash drain valve 9 on the raw water side,
Release the pressure on the raw water side at once. At this time, as shown in FIG. 2, the pressure on the raw water side is reduced at once and a large effective transmembrane pressure is generated. Therefore, the accumulated substances on the membrane surface are almost sequentially peeled off from the membrane surface, and are discharged together with the filtered water flowing out from the pressurized tank 5 through the backwash drain valve 9.

【0011】この加圧逆洗工程のみによっても逆洗が可
能であるが、実施例では加圧逆洗工程を数秒継続した
後、高圧空気供給バルブ6を閉じ、ろ過側の加圧を停止
するとともに、リンス水供給バルブ8を開いて原水側の
上流からリンス水を流す。これにより剥離物質はリンス
水とともに系外に放出されることとなる。
Although backwashing can be performed only by this pressure backwashing step, in the embodiment, after the pressure backwashing step is continued for several seconds, the high pressure air supply valve 6 is closed and the pressure on the filtration side is stopped. At the same time, the rinse water supply valve 8 is opened to flow the rinse water from the upstream side of the raw water side. As a result, the stripping substance is released out of the system together with the rinse water.

【0012】[0012]

【発明の効果】以上に説明したように、本発明のセラミ
ック膜の逆洗方法はセラミック膜の原水側とろ過側とに
高圧を加えて等圧に保持したうえ、原水側のバルブを急
速に開いて原水側の圧力を一度に開放することにより十
分な有効膜差圧を発生させることができるので、膜表面
から瞬時に蓄積物を剥離させることができ、短時間で効
果的な逆洗を行うことができる。また高圧を加えた際に
膜表面の蓄積物が圧密化され、剥離物質の沈降性を高め
られる利点もある。
As described above, according to the method of backwashing a ceramic membrane of the present invention, a high pressure is applied to the raw water side and the filtration side of the ceramic membrane to maintain the pressure equal, and the valve on the raw water side is rapidly changed. By opening and releasing the pressure on the raw water side at once, a sufficient effective transmembrane pressure can be generated, so that accumulated substances can be instantly separated from the membrane surface, and effective backwashing can be performed in a short time. It can be carried out. Further, there is also an advantage that when a high pressure is applied, the accumulated material on the film surface is consolidated and the sedimentation property of the exfoliated substance can be enhanced.

【図面の簡単な説明】[Brief description of drawings]

【図1】実施例の装置の配管系統図である。FIG. 1 is a piping system diagram of an apparatus according to an embodiment.

【図2】本発明の実施例おける逆洗時の圧力変化を示す
グラフである。
FIG. 2 is a graph showing pressure changes during backwashing in an example of the present invention.

【図3】従来法における逆洗時の圧力変化を示すグラフ
である。
FIG. 3 is a graph showing a pressure change during backwashing in a conventional method.

【符号の説明】[Explanation of symbols]

1 膜モジュール、2 セラミック膜、3 原水供給バ
ルブ、4 ろ過水バルブ、5 加圧タンク、6 高圧空
気供給バルブ、7 放圧用バルブ、8 リンス水供給バ
ルブ、9 逆洗排水バルブ
1 membrane module, 2 ceramic membrane, 3 raw water supply valve, 4 filtered water valve, 5 pressurized tank, 6 high pressure air supply valve, 7 pressure release valve, 8 rinse water supply valve, 9 backwash drain valve

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】 セラミック膜を用いて固液分離する際に
管状型またはモノリス型のセラミック膜によるろ過を停
止し、原水側のバルブを閉じて原水側を閉鎖状態とした
のち、ろ過側より高圧を加えてセラミック膜の原水側と
ろ過側とを等圧に保持し、その後に原水側の一端のバル
ブを急速に開き原水側の圧力を一度に開放して逆洗する
ことを特徴とするセラミック膜の逆洗方法。
1. When solid-liquid separation is performed using a ceramic membrane, filtration with a tubular or monolithic ceramic membrane is stopped, the raw water side valve is closed to close the raw water side, and then the high pressure is applied from the filtration side. A ceramic membrane characterized in that the raw water side and the filtration side of the ceramic membrane are held at equal pressure, and then the valve at one end on the raw water side is rapidly opened to release the pressure on the raw water side at once and backwash. How to backwash the membrane.
【請求項2】 原水側の圧力開放時に原水側の他端か
ら、剥離物を系外に除外するためのリンス水を流し、剥
離物質を系外に放出する請求項1に記載のセラミック膜
の逆洗方法。
2. The ceramic membrane according to claim 1, wherein when the pressure on the raw water side is released, rinse water for excluding the exfoliated material from the system is flowed from the other end on the raw water side to release the exfoliated substance to the outside of the system. Backwash method.
JP5325653A 1993-12-24 1993-12-24 Backwashing method of ceramic membrane Expired - Lifetime JP2763262B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP5325653A JP2763262B2 (en) 1993-12-24 1993-12-24 Backwashing method of ceramic membrane

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP5325653A JP2763262B2 (en) 1993-12-24 1993-12-24 Backwashing method of ceramic membrane

Publications (2)

Publication Number Publication Date
JPH07178323A true JPH07178323A (en) 1995-07-18
JP2763262B2 JP2763262B2 (en) 1998-06-11

Family

ID=18179225

Family Applications (1)

Application Number Title Priority Date Filing Date
JP5325653A Expired - Lifetime JP2763262B2 (en) 1993-12-24 1993-12-24 Backwashing method of ceramic membrane

Country Status (1)

Country Link
JP (1) JP2763262B2 (en)

Cited By (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001023076A1 (en) * 1999-09-29 2001-04-05 Zenon Environmental Inc. Ultrafiltration and microfiltration module and system
JP2007111576A (en) * 2005-10-18 2007-05-10 Ngk Insulators Ltd Back-washing method of membrane module
JP2009220018A (en) * 2008-03-17 2009-10-01 Metawater Co Ltd Method and device for cleaning membrane
JP2011183320A (en) * 2010-03-09 2011-09-22 Metawater Co Ltd Backwashing method for membrane filter
JP2014147919A (en) * 2013-02-04 2014-08-21 Metawater Co Ltd Membrane filtration system
US8840783B2 (en) 2007-05-29 2014-09-23 Evoqua Water Technologies Llc Water treatment membrane cleaning with pulsed airlift pump
US8858796B2 (en) 2005-08-22 2014-10-14 Evoqua Water Technologies Llc Assembly for water filtration using a tube manifold to minimise backwash
US8956464B2 (en) 2009-06-11 2015-02-17 Evoqua Water Technologies Llc Method of cleaning membranes
US9022224B2 (en) 2010-09-24 2015-05-05 Evoqua Water Technologies Llc Fluid control manifold for membrane filtration system
US9023206B2 (en) 2008-07-24 2015-05-05 Evoqua Water Technologies Llc Frame system for membrane filtration modules
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US9675938B2 (en) 2005-04-29 2017-06-13 Evoqua Water Technologies Llc Chemical clean for membrane filter
US9764288B2 (en) 2007-04-04 2017-09-19 Evoqua Water Technologies Llc Membrane module protection
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US9925499B2 (en) 2011-09-30 2018-03-27 Evoqua Water Technologies Llc Isolation valve with seal for end cap of a filtration system
US9962865B2 (en) 2012-09-26 2018-05-08 Evoqua Water Technologies Llc Membrane potting methods
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US10322375B2 (en) 2015-07-14 2019-06-18 Evoqua Water Technologies Llc Aeration device for filtration system
US10427102B2 (en) 2013-10-02 2019-10-01 Evoqua Water Technologies Llc Method and device for repairing a membrane filtration module
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JPH05184885A (en) * 1991-03-26 1993-07-27 Lyonnaise Des Eaux Dumez Sa Method for cleaning meso-porous tubular membrane of ultrafiltration

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH05184885A (en) * 1991-03-26 1993-07-27 Lyonnaise Des Eaux Dumez Sa Method for cleaning meso-porous tubular membrane of ultrafiltration

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US6814861B2 (en) 1999-09-29 2004-11-09 Zenon Environmental, Inc. Ultrafiltration and microfiltration module and system
US7070695B2 (en) 1999-09-29 2006-07-04 Zenon Environmental Inc. Ultrafiltration and microfiltration module and system
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US9675938B2 (en) 2005-04-29 2017-06-13 Evoqua Water Technologies Llc Chemical clean for membrane filter
US8858796B2 (en) 2005-08-22 2014-10-14 Evoqua Water Technologies Llc Assembly for water filtration using a tube manifold to minimise backwash
US8894858B1 (en) 2005-08-22 2014-11-25 Evoqua Water Technologies Llc Method and assembly for water filtration using a tube manifold to minimize backwash
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US9764288B2 (en) 2007-04-04 2017-09-19 Evoqua Water Technologies Llc Membrane module protection
US8840783B2 (en) 2007-05-29 2014-09-23 Evoqua Water Technologies Llc Water treatment membrane cleaning with pulsed airlift pump
US10507431B2 (en) 2007-05-29 2019-12-17 Evoqua Water Technologies Llc Membrane cleaning with pulsed airlift pump
US9206057B2 (en) 2007-05-29 2015-12-08 Evoqua Water Technologies Llc Membrane cleaning with pulsed airlift pump
US9573824B2 (en) 2007-05-29 2017-02-21 Evoqua Water Technologies Llc Membrane cleaning with pulsed airlift pump
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US9023206B2 (en) 2008-07-24 2015-05-05 Evoqua Water Technologies Llc Frame system for membrane filtration modules
US8956464B2 (en) 2009-06-11 2015-02-17 Evoqua Water Technologies Llc Method of cleaning membranes
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US9914097B2 (en) 2010-04-30 2018-03-13 Evoqua Water Technologies Llc Fluid flow distribution device
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