JP3817169B2 - Thermocrystallization apparatus for thermoplastic polymer chips - Google Patents

Thermocrystallization apparatus for thermoplastic polymer chips Download PDF

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Publication number
JP3817169B2
JP3817169B2 JP2001381388A JP2001381388A JP3817169B2 JP 3817169 B2 JP3817169 B2 JP 3817169B2 JP 2001381388 A JP2001381388 A JP 2001381388A JP 2001381388 A JP2001381388 A JP 2001381388A JP 3817169 B2 JP3817169 B2 JP 3817169B2
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Prior art keywords
tank
partition wall
thermoplastic polymer
hot air
side mesh
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JP2001381388A
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JP2003181831A (en
Inventor
役男 佐藤
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有限会社佐藤化成工業所
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Priority to JP2001381388A priority Critical patent/JP3817169B2/en
Priority to CNB021565430A priority patent/CN100441386C/en
Publication of JP2003181831A publication Critical patent/JP2003181831A/en
Priority to HK04102514.9A priority patent/HK1059600A1/en
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Description

【0001】
【発明の属する技術分野】
本発明は、ポリアミド、ポリエステル等の熱可塑性重合体チップを加熱してこれを結晶化する加熱結晶化装置に関し、特にポリエステルチップを予熱または加熱して予備結晶化する加熱結晶化装置に関する。
【0002】
【従来の技術】
そもそも、溶融重合後のカツテイング等により無結晶化表面が形成されたポリアミド、ポリエステル等の熱可塑性重合体チップを乾燥又は固相重合する作業を行なうときに、通常90℃ないし130℃以上の温度をかけるとチップ相互に融着が起きる。この融着は2〜3粒のチップの塊から、いわおこしのような大きな塊の場合があり、いずれの場合でも以後の工程でトラブルを惹起して好ましくない。
【0003】
従前、このような融着現象を解消するために、本発明者は、底部内に円錐形のスクリーンセパレータを有する撹袢翼付き加熱結晶化装置(登録実用新案公報3050004号)を提案した。この加熱結晶化装置は、確かにチップ相互に融着が生じないようする上で効果があって、汎用されるに至っている。
【0004】
しかしながら、この加熱結晶化装置にも、つぎのような問題点があった。
(1)スクリーンセパレータの処理面が傾斜していて目詰まりが起こり易い。
(2)目詰まりしたスクリーンセパレータのメンテナンスには大掛かりな分解作業等が必要で大変であった。
(3)目詰まり(凝固)が進むにつれて熱量不足が徐々に進行するので、これに従って処理時間を徐々に長くして行く必要があった。
(4)上記(3)で述べたように熱量不足が徐々に進行するために結晶化不良の発生時点の把握が難しく、これによる不測のトラブルも起き易い。
(5)上記(4)で述べたように不測のトラブル発生が起き易いので、バッチ方式ではない連続使用には必ずしも向いているとは言えない。
【0005】
【発明が解決しようとする課題】
本発明の目的は、上記の諸問題を解消するための工夫を施した熱可塑性重合体チップの加熱結晶化装置を新規に提供することにある。
【0006】
【課題を解決するための手段】
上記目的を達成するために本発明に係る熱可塑性重合体チップの加熱結晶化装置は、筒状タンクの上部に結晶化前ペレットの投入口を有し、底部に結晶化済みペレットの排出口を有し、且つ内部に上下方向に多段の撹袢翼群を有する熱可塑性重合体チップの加熱結晶化装置であって、タンクの底部内に漏斗形状を呈する金属板製の仕切り壁を装入して同タンクの底壁と仕切り壁の間に当該仕切り壁を囲繞する空間を形成し、この空間内に熱風を供給するための熱風供給装置をタンクに連結すると共に仕切り壁の深い所に上記排出口へ結晶化済みペレットを送出する送出管を連結し、この送出管の壁面に同管内と上記空間を連通状態とするための沢山の小孔を有する底部側メッシュ部を設け、上記仕切り壁の上方に、上記タンクの筒状胴壁内側に開口する熱風吹出口を設け、この熱風吹出口の開口面に同口内とタンク内を連通状態とするための沢山の小孔を有する胴部側メッシュ部を設け、上記胴部側メッシュ部は傾斜しないように形成されるとともに、上記胴部側メッシュ部の外側に当該胴部側メッシュ部をメンテナンスするための開放用蓋を設けたものである。
【0007】
【実施例】
図1および図2に示す第1実施例は、外面を保温材13により被包した漏斗形底14付きの円筒形タンク1を構成し、このタンク1の上部に結晶化前ペレットの投入口2および熱風排出口17を設け、また漏斗形底14の下端に結晶化済みペレットの排出口3を設けると共にタンク1の漏斗形底14の内側に同底14よりも僅かに浅い漏斗形状を呈するステンレス板製の仕切り壁5を装入して同漏斗形底14と仕切り壁5の間に当該仕切り壁5を囲繞する空間7を形成し、この空間7に当該空間7内に熱風を供給するための熱風供給口6を開設して同口6に熱風供給装置(図示せず)を連結したものである。
【0008】
さらに、同第1実施例は、仕切り壁5の深い所に排出口3へ結晶化済みペレットを送出する送出管8を連結し、この送出管8の壁面に同管8内と上記空間7を連通状態とするための沢山の小孔を有する底部側メッシュ部9を設けると共に上記空間7の上縁に連続してタンク1の筒状胴壁内側に開口する縦長の熱風吹出口10aの3個を等間隔配置で設け、これ等各熱風吹出口10aの開口面に同口10a内とタンク1内を連通状態とするための沢山の小孔を有する胴部側メッシュ部11aを設けたものである。
【0009】
また、同第1実施例は、胴部側メッシュ部11aの外側に当該胴部側メッシュ部11aをメンテナンスするための開放用蓋18を設けたものである。このようにしたので、胴部側メッシュ部11aの目詰まりを解消する等のメンテナンスは、当該開放用蓋18を外して、楽に、タンク1の外側から行なうことができて便利である。
【0010】
さらに、同第1実施例は、タンク1の天壁の中心に攪拌用モータ(図示せず)により回転する回転軸15をその下端が仕切り壁5の底口16の近くまで達する位置として串通し、この回転軸15にタンク1内および仕切り壁5内に存する結晶化中ペレット(以下、単に結晶化中ペレットという。)を上方に戻し乍ら攪拌する多数枚の攪拌用羽根4を取付けたものである。
【0011】
図3および図4に示す第2実施例は、空間7の上縁を上方に延長して筒状の延長部19に連設し、この延長部19の上端全周にタンク1の胴壁内側に開口するリング状熱風吹出口10bを設け、このリング状熱風吹出口10bの開口面に同口10b内とタンク1内を連通状態とするための沢山の小孔を有する胴部側メッシュ部11bを設けてあるものである。そして、その他の部位は上記第1実施例と同様の構成としたものであるので、同じ部位には同一の符号を付してその詳細の説明は省略する。
【0012】
なお、上記実施例は、漏斗形底14に空間7内および底部側メッシュ部9のための点検用窓20を設け、また図には示していないが排出口2にシャッターを、またタンク1の筒状胴壁に内部点検用蓋およびペレット量ゲージ窓等を設けてある。
【0013】
上記の実施例は、先ず、熱風供給口6から熱風を供給して全体を暖め且つ攪拌用羽根4を回転させたのち投入口2を介して例えばポリエチレンテレフタレートの結晶化前ペレットとカラーリング用マスターバッチとステアリン酸カルシウム等を各定量まで投入すると共に熱風供給装置の制御盤(図示せず)で温度調節を行い、温度が安定した状態を一定時間まで予め得ているデータに基いて続け、結晶化前ペレットの結晶化の完了をペレットゲージ窓で確認した時点でカラーリング用マスターバッチ混入結晶化済みペレットを排出口3から成形機(図示せず)等に供給したり、袋詰めしたりする等の用法で供するものであって、ペレット結晶化処理をバッチ方式でも連続方式でもできるものである。
【0014】
上記用法等で用いる場合、熱風供給口6から供給された熱風は、熱風吹出口10a、10bおよび胴部側メッシュ部11a、11bを介してタンク1内に入って同タンク1内のペレットを結晶化する機能と、底部側メッシュ部10a、10bを経て仕切り壁5内に入り且つ空間7内で仕切り壁5を加熱して同仕切り壁5内に存するペレットを結晶化する機能とを行う。
【0015】
上記機能をなす場合、仕切り壁5には目(小孔)がないので上記従来例のスクリーンセパレータのような目詰まりによる問題点を発生する危惧のないものであり、また胴部側メッシュ部11a、11bがタンク1の筒状胴壁に設けて傾斜しないようにしてあるので目詰まりが起き難くいものである。
【0016】
【発明の効果】
従って、本発明によれば、上記スクリーンセパレータを採用した従来例で生じていたような種々の問題を充分に回避でき、常に一定で安定したチップを供給できる加熱結晶化装置を提供できる。さらには、目詰まりが起き難くいので、装置の運転を停止して行なわなければならないタンク内の清掃の回数を顕著に少なくでき、これによって作業効率向上と安全の確保という面においても極めて大きな効果を得ることができる。また、メンテナンスは開放用蓋を開くことで容易にできて使い易く便利である。
【図面の簡単な説明】
【図1】本発明の第1実施例を示す正面断面図である。
【図2】同じく、平面断面図である。
【図3】本発明の第2実施例を示す正面断面図である。
【図4】同じく、平面断面図である。
【符号の説明】
1 タンク
2 投入口
3 排出口
4 攪拌用羽根
5 仕切り壁
6 熱風供給口
7 空間
8 送出管
9 底部側メッシュ部
10a、10b 熱風吹出口
11a、11b 胴部側メッシュ部
13 保温材
14 漏斗形底
15 回転軸
16 底口
17 熱風排出口
18 開放用蓋
19 延長部
20 点検用窓
[0001]
BACKGROUND OF THE INVENTION
The present invention relates to a heat crystallization apparatus that heats and crystallizes a thermoplastic polymer chip such as polyamide or polyester, and more particularly to a heat crystallization apparatus that preheats or heats a polyester chip to perform precrystallization.
[0002]
[Prior art]
In the first place, when a thermoplastic polymer chip such as polyamide or polyester having a non-crystallized surface formed by cutting or the like after melt polymerization is dried or solid-phase polymerized, the temperature is usually 90 ° C to 130 ° C or higher. When applied, fusion occurs between the chips. This fusion may be a large lump such as a wrinkle from a lump of 2 to 3 chips. In any case, troubles are caused in subsequent steps, which is not preferable.
[0003]
In the past, in order to eliminate such a fusion phenomenon, the present inventor has proposed a heated crystallization apparatus with a stirring blade (Registered Utility Model Publication No. 3050004) having a conical screen separator in the bottom. This heat crystallization apparatus is effective in preventing fusion between chips, and has been widely used.
[0004]
However, this heat crystallization apparatus also has the following problems.
(1) The processing surface of the screen separator is inclined and clogging is likely to occur.
(2) Maintenance of the clogged screen separator required a large disassembly work and was difficult.
(3) Since the heat shortage gradually proceeds as clogging (solidification) proceeds, it was necessary to gradually increase the treatment time accordingly.
(4) As described in (3) above, since the shortage of heat proceeds gradually, it is difficult to grasp the time of occurrence of crystallization failure, and unexpected troubles are likely to occur.
(5) Since unexpected troubles are likely to occur as described in (4) above, it is not necessarily suitable for continuous use other than the batch method.
[0005]
[Problems to be solved by the invention]
An object of the present invention is to newly provide a heat crystallization apparatus for a thermoplastic polymer chip which has been devised to solve the above problems.
[0006]
[Means for Solving the Problems]
In order to achieve the above object, the thermoplastic polymer chip heating and crystallization apparatus according to the present invention has a pre-crystallization pellet inlet at the top of a cylindrical tank and a crystallized pellet outlet at the bottom. A thermoplastic polymer chip crystallization apparatus having a plurality of stirring blade groups in the vertical direction inside, and having a partition wall made of a metal plate having a funnel shape in the bottom of the tank. A space surrounding the partition wall is formed between the bottom wall and the partition wall of the tank, and a hot air supply device for supplying hot air into the space is connected to the tank and the exhaust is disposed deep in the partition wall. A delivery pipe for delivering the crystallized pellets to the outlet is connected, and a bottom side mesh portion having many small holes for communicating the inside of the pipe with the space is provided on the wall of the delivery pipe . upward, cylindrical body wall inside the tank An opening for hot air outlet provided, the barrel-side mesh portion having a lot of small holes for communicating state with the mouth and the tank opening surface of the hot air outlet provided, the barrel-side mesh portion inclined In addition, an opening lid for maintaining the trunk side mesh portion is provided outside the trunk side mesh portion.
[0007]
【Example】
In the first embodiment shown in FIGS. 1 and 2, a cylindrical tank 1 with a funnel-shaped bottom 14 whose outer surface is encapsulated by a heat insulating material 13 is constructed, and an inlet 2 for pellets before crystallization is formed on the upper portion of the tank 1. And a hot air discharge port 17, a crystallized pellet discharge port 3 at the lower end of the funnel-shaped bottom 14, and a funnel shape slightly shallower than the bottom 14 inside the funnel-shaped bottom 14 of the tank 1. In order to insert a partition wall 5 made of a plate to form a space 7 surrounding the partition wall 5 between the funnel-shaped bottom 14 and the partition wall 5, and to supply hot air to the space 7 in the space 7 The hot air supply port 6 is opened and a hot air supply device (not shown) is connected to the same.
[0008]
Further, in the first embodiment, a delivery pipe 8 for sending the crystallized pellets to the discharge port 3 is connected to the deep part of the partition wall 5, and the inside of the pipe 8 and the space 7 are connected to the wall of the delivery pipe 8. Three vertical hot air outlets 10a that are provided on the inner side of the cylindrical body wall of the tank 1 are provided on the inside of the cylindrical body wall of the tank 1 while providing the bottom side mesh portion 9 having many small holes for communication. Are provided at equal intervals, and the body side mesh portion 11a having a large number of small holes for communicating the inside of the same port 10a and the inside of the tank 1 is provided on the opening surface of each hot air outlet 10a. is there.
[0009]
In the first embodiment, an opening lid 18 is provided on the outside of the body side mesh part 11a for maintenance of the body side mesh part 11a. Since it did in this way, maintenance, such as eliminating the clogging of the trunk side mesh portion 11a, can be easily performed from the outside of the tank 1 with the opening lid 18 removed, which is convenient.
[0010]
Further, in the first embodiment, the rotary shaft 15 rotated by a stirring motor (not shown) is centered on the top wall of the tank 1 so that the lower end thereof reaches the vicinity of the bottom port 16 of the partition wall 5. The rotating shaft 15 is provided with a plurality of stirring blades 4 for stirring while returning the crystallization pellets (hereinafter simply referred to as crystallization pellets) in the tank 1 and the partition wall 5 to the upper side. It is.
[0011]
In the second embodiment shown in FIGS. 3 and 4, the upper edge of the space 7 is extended upward and is connected to a cylindrical extension 19. A ring-shaped hot air outlet 10b is provided at the opening, and a trunk-side mesh portion 11b having a large number of small holes on the opening surface of the ring-shaped hot air outlet 10b for connecting the inside of the mouth 10b and the tank 1 to each other. Is provided. Since the other parts have the same configuration as that of the first embodiment, the same parts are denoted by the same reference numerals and detailed description thereof is omitted.
[0012]
In the above embodiment, an inspection window 20 for the inside of the space 7 and the bottom mesh portion 9 is provided in the funnel-shaped bottom 14, and although not shown in the figure, a shutter is provided at the discharge port 2, and the tank 1. An internal inspection lid, a pellet amount gauge window, and the like are provided on the cylindrical body wall.
[0013]
In the above-described embodiment, first, hot air is supplied from the hot air supply port 6 to warm the whole and the stirring blade 4 is rotated, and then, for example, a pre-crystallization pellet of polyethylene terephthalate and a coloring master through the input port 2. The batch and calcium stearate etc. are charged up to each amount, and the temperature is adjusted with the control panel (not shown) of the hot air supply device, and a stable temperature state is continued based on the data obtained in advance for a certain period of time for crystallization. When the completion of crystallization of the previous pellets is confirmed through the pellet gauge window, the crystallized pellets mixed with the coloring master batch are supplied to the molding machine (not shown) or the like from the discharge port 3 or packed in a bag. The pellet crystallization treatment can be performed either batchwise or continuously.
[0014]
When used in the above-mentioned usage etc., the hot air supplied from the hot air supply port 6 enters the tank 1 through the hot air outlets 10a and 10b and the body side mesh portions 11a and 11b and crystallizes the pellets in the tank 1 And the function of entering the partition wall 5 through the bottom mesh portions 10a and 10b and heating the partition wall 5 in the space 7 to crystallize the pellets present in the partition wall 5.
[0015]
In the case of performing the above function, the partition wall 5 has no eyes (small holes), so there is no risk of causing problems due to clogging as in the conventional screen separator, and the body side mesh portion 11a. 11b are provided on the cylindrical body wall of the tank 1 so as not to be inclined, so that clogging is unlikely to occur.
[0016]
【The invention's effect】
Therefore, according to the present invention, it is possible to provide a heat crystallization apparatus that can sufficiently avoid various problems such as those caused in the conventional example employing the screen separator and can always supply a constant and stable chip. In addition, since clogging is unlikely to occur, the number of tank cleanings that must be carried out after stopping the operation of the tank can be remarkably reduced, which is extremely effective in improving work efficiency and ensuring safety. Can be obtained. In addition, maintenance can be easily performed by opening the opening lid, which is convenient and convenient to use.
[Brief description of the drawings]
FIG. 1 is a front sectional view showing a first embodiment of the present invention.
FIG. 2 is also a plan sectional view.
FIG. 3 is a front sectional view showing a second embodiment of the present invention.
FIG. 4 is a plan sectional view of the same.
[Explanation of symbols]
DESCRIPTION OF SYMBOLS 1 Tank 2 Inlet 3 Outlet 4 Stirring blade 5 Partition wall 6 Hot air supply port 7 Space 8 Delivery pipe 9 Bottom side mesh part 10a, 10b Hot air outlet 11a, 11b Trunk side mesh part 13 Heat insulating material 14 Funnel-shaped bottom 15 Rotating shaft 16 Bottom port 17 Hot air outlet 18 Opening lid 19 Extension part 20 Inspection window

Claims (2)

筒状タンクの上部に結晶化前ペレットの投入口を有し、底部に結晶化済みペレットの排出口を有し、且つ内部に上下方向に多段の撹袢翼群を有する熱可塑性重合体チップの加熱結晶化装置であって、タンクの底部内に漏斗形状を呈する金属板製の仕切り壁を装入して同タンクの底壁と仕切り壁の間に当該仕切り壁を囲繞する空間を形成し、この空間内に熱風を供給するための熱風供給装置をタンクに連結すると共に仕切り壁の深い所に上記排出口へ結晶化済みペレットを送出する送出管を連結し、この送出管の壁面に同管内と上記空間を連通状態とするための沢山の小孔を有する底部側メッシュ部を設け、上記仕切り壁の上方に、上記タンクの筒状胴壁内側に開口する熱風吹出口を設け、この熱風吹出口の開口面に同口内とタンク内を連通状態とするための沢山の小孔を有する胴部側メッシュ部を設け、上記胴部側メッシュ部は傾斜しないように形成されていることを特徴とする熱可塑性重合体チップの加熱結晶化装置。A thermoplastic polymer chip having an inlet for pellets before crystallization at the top of a cylindrical tank, an outlet for discharging crystallized pellets at the bottom, and a multistage stirring blade group in the vertical direction inside It is a heat crystallization device, and a space surrounding the partition wall is formed between the bottom wall and the partition wall of the tank by inserting a partition wall made of a metal plate having a funnel shape in the bottom of the tank, A hot air supply device for supplying hot air into the space is connected to the tank, and a delivery pipe for sending the crystallized pellets to the discharge port is connected to the deep part of the partition wall, and the inside of the pipe is connected to the wall of the delivery pipe. And a bottom side mesh portion having many small holes for communicating with the space, and a hot air outlet opening to the inside of the cylindrical body wall of the tank is provided above the partition wall. The inside of the outlet and the tank communicate with the opening surface of the outlet And the body portion-side mesh portion having a lot of small holes for providing the heating crystallization apparatus of the thermoplastic polymer chips the barrel side mesh portion is characterized in that it is formed so as not to tilt. 請求項1に係る熱可塑性重合体チップの加熱結晶化装置について、胴部側メッシュ部の外側に当該胴部側メッシュ部をメンテナンスするための開放用蓋を設けたことを特徴とする熱可塑性重合体チップの加熱結晶化装置。  The thermoplastic polymer crystallization apparatus for a thermoplastic polymer chip according to claim 1, wherein an opening lid for maintaining the trunk side mesh portion is provided outside the trunk side mesh portion. Combined chip heat crystallization equipment.
JP2001381388A 2001-12-14 2001-12-14 Thermocrystallization apparatus for thermoplastic polymer chips Expired - Fee Related JP3817169B2 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
JP2001381388A JP3817169B2 (en) 2001-12-14 2001-12-14 Thermocrystallization apparatus for thermoplastic polymer chips
CNB021565430A CN100441386C (en) 2001-12-14 2002-12-12 Heating crystallizing device for thermoplastic polymer fragment
HK04102514.9A HK1059600A1 (en) 2001-12-14 2004-04-08 Heating-crystallizing device for thermoplastic polymer chip

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US7329723B2 (en) 2003-09-18 2008-02-12 Eastman Chemical Company Thermal crystallization of polyester pellets in liquid
CA2482056A1 (en) 2003-10-10 2005-04-10 Eastman Chemical Company Thermal crystallization of a molten polyester polymer in a fluid
US20060047102A1 (en) 2004-09-02 2006-03-02 Stephen Weinhold Spheroidal polyester polymer particles
DE102005008115A1 (en) * 2005-02-21 2006-08-31 Mann + Hummel Protec Gmbh Process for crystallizing an amorphous plastic granulate
US7875184B2 (en) 2005-09-22 2011-01-25 Eastman Chemical Company Crystallized pellet/liquid separator
JP5857783B2 (en) * 2012-02-17 2016-02-10 株式会社リコー Nozzle, image forming apparatus, and powder derivation method
CN106273054B (en) * 2016-08-31 2018-08-10 无锡优萌模塑制造有限公司 A kind of feed pre-processing device of injection molding machine
CN107694142A (en) * 2017-11-09 2018-02-16 东莞市和津塑料机械有限公司 Efficient PET crystallizers and its method for crystallising
CN108126213B (en) * 2018-01-23 2020-07-14 青岛市即墨区人民医院 Medical scalpel disinfection cabinet
CN109049425B (en) * 2018-08-29 2021-04-06 合肥千聚环保科技有限公司 Waste plastic crushing apparatus convenient for environmental protection

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